Milling of materials, whether hard and brittle or soft and ductile, is of prime interest and of economic importance to the powder metallurgy (PM) industry. This article discusses the principles of milling, milling parameters, and the powder characteristics required for the process. It discusses the changes in powder particle morphology that occur during milling of metal powders produced by various processes such as microforging, fracturing, agglomeration, and deagglomeration. The article also provides useful information on milling equipment such as tumbler ball mills, vibratory ball mills, attrition mills, and hammer and rod mills.

Hardness characterizes the resistance of the ceramic to deformation, densification, displacement, and fracture. It is usually measured with conventional microindentation hardness machines using the Knoop or the Vickers diamond indenters. This article discusses the metrology issues of the Knoop and the Vickers hardness in ceramics. It explicates how to estimate fracture toughness from Vickers indentation cracking. The article also provides information on instrumented hardness testing and the Meyer law.