This article discusses the importance of the care and handling of fracture specimens and what to look for during the preliminary field or laboratory observation and collection, the preservation of specimens, and the cleaning and preparation of fracture specimens for additional analyses. The preservation of nonmetallic specimens, medical devices, oversized components, light alloys, nondestructively tested components, and materials that are part of legal proceedings is addressed.

Vat polymerization (VP) is an additive manufacturing (AM), or three-dimensional (3-D) printing process in which 3-D objects are produced by hardening a liquid polymer into the desired shape. With the introduction of new materials and improvements in material properties, VP offers a good alternative for AM for low-volume production. This overview of the VP process begins with an introduction to two main processes of VP, namely stereolithography apparatus and digital light processing, and then moves on to discuss the characteristics of the feedstocks used as well as their selection criteria. The article then covers safety issues associated with feedstock handling and the manufacturing constraints related to part orientation and design, providing some key tips for VP support structures. This is followed by a discussion on postprocessing/finishing of VP parts. A brief concluding section considers some special topics related to AM process.

This article describes post-processing techniques for machining, finishing, heat treating, and deburring used to remove additive manufacturing (AM) metallic workpieces from a base plate and subsequent techniques to enhance printed workpieces. The AM processes include powder bed fusion, binder jetting, and direct energy deposition. The discussion provides information on powder removal, powder recycling and conditioning, part removal, and part enhancement. The mechanism, applications, advantages, and limitations of mechanical, radiation, and chemical-finishing processes as well as the properties of the resulting material are also covered.

Etching aluminum can be a pretreatment step for anodizing, chemical conversion coating, metal-to-rubber bonding, and a host of other processes. Chemical etching, using either alkaline or acid solutions, produces a matte finish on aluminum products. This article describes the alkaline etching and acid etching of aluminum. Alkaline etching reduces or eliminates surface scratches, nicks, extrusion die lines, and other imperfections. Acid etching can be done without heavy smut problems, particularly on aluminum die castings. Hydrochloric, hydrofluoric, nitric, phosphoric, chromic, and sulfuric acids are used in acid etching. The article presents a flow chart of the operations used in acid etching.

Adhesive bonding is a proven technology in the manufacture of automotive assemblies, helping carmakers achieve weight reduction goals without compromising body stiffness, crash performance, and noise-vibration-handling characteristics. This article discusses the advantages and limitations of adhesive-bonded aluminum joints and the procedures used to produce them. It addresses surface preparation, the addition of interfacial coatings and primers, and the application of thermoplastic and thermosetting resins. The article examines the nature and role of the various layers that constitute the joint and explains how each contributes to performance. It also discusses adhesive selection factors, joint design, and testing procedures.

Aluminum components are often plated with other metals to mitigate the effects of corrosion and wear, improve application performance, and extend service life. This article discusses some of the more common aluminum plating processes, including electroplating, immersion plating, and electroless plating, and describes various plating materials and the types of applications in which they are used. It provides critical processing details such as temperatures, ratios, ranges, times, and rates. The article explains how to prepare aluminum components for electroplating, discussing surface roughening, anodizing, and immersion procedures along with expected results.

This article discusses the properties of aluminum surface and the applications of aluminum alloys. It explains the effects of trace elements on aluminum alloys. The article considers microstructural development of aluminum in terms of the surface and explains how it will impact corrosion resistance and surface treatment. It describes the thermodynamics of equilibrium oxidation processes and non-equilibrium corrosion processes. The article provides a discussion on aluminum oxidation under atmospheric and dynamic conditions. It presents the potential/pH (Pourbaix) diagram for aluminum under atmospheric and dynamic conditions. The article also explains the polarization effects during the formation of stable aluminum oxide under dynamic conditions. It concludes with information on the designation system for aluminum finishes.

The resistance welding processes commonly employed for joining aluminum are resistance spot welding, resistance seam welding, resistance roll welding, upset and flash welding for butt joining welding, and high-frequency resistance welding. This article discusses the general factors affecting resistance welding: electrical and thermal conductivities, rising temperature, plastic range, shrinkage, and surface oxide. It reviews the weldability of base materials such as Alclad alloys and aluminum metal-matrix composites. The article describes the joint design and welding procedures for resistance spot welding, as well as the joint type, equipment, and welding procedures for seam and roll spot welding. It concludes with information on flash welding, high-frequency welding, and cross-wire welding.

Although aluminum alloys are inherently corrosion resistant, there are many operating environments where they require additional protection. This article describes the conditions under which aluminum is prone to corrode and explains how to prevent it through the addition of conversion coatings and paints. It addresses some of the more common corrosion mechanisms, including corrosion driven by pH extremes, pitting corrosion, crevice corrosion, galvanic corrosion, and filiform corrosion. The article also describes in-plant as well as field application procedures for cleaning and coating, and discusses the advantages and limitations of the various materials and chemicals used.

The necessary precursor to a proper and durable finish is the preparation of the active aluminum surface to receive the desired protective finish that will allow it to have a long and attractive service life. This article helps those who work with aluminum in the many varieties of applications of such products. It describes the two main categories of cleaning that can be used with most any metal, namely, mechanical cleaning and chemical cleaning. The article provides a discussion on the laboratory evaluation of cleaners, field testing of cleaners, and cleaner types and procedures. It also describes the special cleaning procedures for aluminum alloys, such as steam cleaning and rotary wire-brush cleaning. The article reviews the use of temporary coatings and the use of maintenance coatings on aluminum. It provides information on the handling and storage procedures of aluminum alloys and the cleaning of specific applications of aluminum.

Chemical brightening (bright dipping) and electrolytic brightening (electropolishing) are essentially selective-dissolution processes, in which the high points of a rough surface of aluminum are attacked more rapidly than the depressions, and the peaks and valleys are smoothed to produce a bright and beautiful finish. This article discusses the metallurgical factors, optical factors, and applications of the chemical and electrolytic brightening. It compares the chemical brightening and electrolytic brightening, and presents the advantages of the chemical and electrolytic brightening processes in terms of performance and economy. The article describes the phosphoric-nitric acid baths and phosphoric-sulfuric acid baths used for chemical brightening. Solution compositions and operating conditions for three commercial electropolishing processes, as well as for suitable post-treatments, are presented in a table.

Mechanical finishes usually can be applied to aluminum using the same equipment used for other metals. This article describes the two types of grinding used in mechanical finishing: abrasive belt grinding and abrasive wheel grinding. It reviews the binders and fluid carriers used in buffing, and discusses satin finishing and barrel finishing. It also describes lapping and honing techniques that are of special interest in treating aluminum parts that have received hard anodic coatings. Honing recommendations for aluminum alloys are presented in a table.

Liquid penetrant inspection is a nondestructive method of revealing discontinuities that are open to the surfaces of solid and essentially nonporous materials. This article provides information on physical principles, evolution, description, and processing parameters of liquid penetrant inspection as well as materials used. It discusses some of the more generally used types of equipment used in penetrant inspection and their requirements. The article describes various penetrant methods and their selection criteria and provides information on precleaning and postcleaning of workpieces before and after penetrant inspection. The quality assurance and maintenance of penetrant inspection materials are also discussed. The article concludes with information on specifications and standards applicable to penetrant inspection.

This article describes two variations of carbon-base coatings: diamondlike carbon (DLC) coatings and polycrystalline diamond (PCD) coatings. It discusses the basics of a few deposition methods as they apply to industrially relevant coatings. The methods include deposition of tungsten-containing hydrogenated amorphous carbon films, deposition of tetrahedral amorphous carbon films, and deposition of silicon-incorporated hydrogenated amorphous carbon films. The most common deposition technologies for diamond films are also discussed. The article provides information on surface preparation for DLC and diamond deposition. It also provides a discussion on the coating composition and structure, mechanical and tribological properties, and applications of DLC and diamond coatings. The quality control techniques for DLC and diamond coatings are specified to meet customer requirements and ensure repeatable quality.

This article is concerned with gear tooth failures influenced by friction, lubrication, and wear, and especially those failure modes that occur in wind-turbine components. It provides a detailed discussion on wear (including adhesion, abrasion, polishing, fretting, and electrical discharge), scuffing, and Hertzian fatigue (including macropitting and micropitting). Details for obtaining high lubricant specific film thickness are presented. The article describes the selection criteria for lubricants, such as oil, grease, adhesive open gear lubricant, and solid lubricants. It discusses the applications of oil and gear lubricants and the types of standardized gear tests. The article presents some recommendations for selecting lubricants and lubricant viscosity for enclosed gear. It provides some examples of failure modes that commonly occur on gears and bearings in wind turbine gearboxes.

This article discusses the fundamentals of electroplating processes, including pre-electroplating and surface-preparation processes. It illustrates the four layers of a plating system, namely, top or finish coat, undercoat, strike or flash, and base material layers. The article describes various plating methods, such as pulse electroplating, electroless plating, brush plating, and jet plating. It reviews the types of electrodeposited coatings, including hard coatings and soft coatings. The article also details the materials available for electroplating, including electroplated chromium, electroplated nickel, electroless (autocatalytic) nickel, electroless nickel composite coatings, electroplated gold, and platinum group coatings. These are specifically tailored toward plated coatings for friction, lubrication, and wear technology. The article concludes with a discussion on the common issues encountered with electroplating.

This article discusses the classification of wear based on the presence or absence of effective lubricants, namely, lubricated and nonlubricated wear. Variations in ambient temperature, atmosphere, load, and sliding speed, as well as variations in material bulk composition, microstructure, surface treatment, and surface finish of steel are also considered. The article discusses the types, wear testing, wear evaluation, and hardness evaluation of abrasive wear. It describes the selection criteria of steels for wear resistance. The article also describes the importance of hardness and microstructure as factors in resistance to wear. It provides a discussion on the resistance of various materials to wear in specific applications. The wear resistance of austenitic manganese steels is also discussed. The article discusses the applications of phosphate coatings, wear-resistant coatings, and ion implantation. It concludes with information on interaction of wear and corrosion.

This article discusses the application of friction stir processing (FSP) and friction surfacing for tribological components. It describes the three critical aspects involved in the application of FSP for near-surface material modifications intended for tribological applications. These include tools, processing parameters, and machines. The article also discusses the equipment and processing parameters for friction surfacing. It describes various hybrid stir processing techniques that involve preheating of the workpiece material, especially relatively hard and high-strength ones. The article presents a partial list of surface-modification methods based on FSP. The partial list includes surface hardening, surface composites, and additive coating. The article also provides information on generation of residual stresses in metallic materials and alloys form different variants of FSP.

This article describes the technology of thermal spraying with regard to tribological applications. It introduces the basics of tribology and presents the fundamentals of thermal spraying and the relevant process variants and suitable materials. Specific application areas are described regarding the different forms of elementary movement in the corresponding tribological system. The article provides an overview of thermal spray coatings and possible uses for friction and wear control, besides operating as corrosion protection and a thermal barrier. The article provides examples that illustrate how tribological performance can be improved.