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Powder processing
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Series: ASM Handbook
Volume: 24A
Publisher: ASM International
Published: 30 June 2023
DOI: 10.31399/asm.hb.v24A.a0007021
EISBN: 978-1-62708-439-0
Abstract
This article provides an overview of the supply chain for metallic additively manufactured materials, with an emphasis on spherical alloy powders. The article describes powder production processes as well as the various metal alloys that can be produced using powder AM techniques. It also reviews the basic characteristics of powder feedstocks and the management of metallic powders.
Series: ASM Handbook
Volume: 24
Publisher: ASM International
Published: 15 June 2020
DOI: 10.31399/asm.hb.v24.9781627082907
EISBN: 978-1-62708-290-7
Series: ASM Handbook
Volume: 24
Publisher: ASM International
Published: 15 June 2020
DOI: 10.31399/asm.hb.v24.a0006567
EISBN: 978-1-62708-290-7
Abstract
This article provides an overview of the general methods of metal powder production. It details the primary methods for particle sizing used in additive manufacturing: sieving, laser diffraction and scattering, and digital image analysis. Methods of interpreting and understanding particle size distribution (PSD) data are presented, with an emphasis on the differences between count- and volume-based PSDs. The article then outlines practices for both qualitative and quantitative assessment of particle morphology.
Book
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.9781627081757
EISBN: 978-1-62708-175-7
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006042
EISBN: 978-1-62708-175-7
Abstract
This article discusses metal powder processing via hot isostatic pressing (HIP) and HIP cladding when metal powders are being employed in the cladding process. It traces the history of the process and details the equipment, pressing cycle, and densification mechanisms for HIP. The article describes the available process routes for fabricating products using HIP and the steps involved in the production of a part via direct HIP of encapsulated gas-atomized spherical powder. It concludes with information on the microstructures of 316L stainless steel HIP powder metallurgy valve body and a list of the mechanical properties of several powder metallurgy alloys.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006078
EISBN: 978-1-62708-175-7
Abstract
This article provides a summary of the conventional technologies used for titanium powder production. It focuses on the various processes for titanium powder production, namely, Hunter, Kroll, Armstrong, MER, TIRO, FFC-Cambridge, Chinuka, and CSIR processes. Employment of titanium powder significantly improves the synthesis of titanium and its alloys.
Book Chapter
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006065
EISBN: 978-1-62708-175-7
Abstract
This article discusses the production of aluminum and aluminum alloy powders with emphasis on the gas atomization method and the atomizing nozzle. It illustrates the particle formation mechanism and details the requisites for particle size distribution, control, and morphology. The article presents information on the mean oxide thickness formed on atomized powders. It also describes the mechanical and physical properties of aluminum and aluminum alloy powders, as well as their applications.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006022
EISBN: 978-1-62708-175-7
Abstract
This article reviews various segments of the powder metallurgy (PM) process from powder production and powder processing through the characterization of the materials and their properties. It covers the processing methods for consolidating metal powders including options for processing to full density. The article outlines the freeform fabrication process, also known as additive manufacturing and describes finishing operations of PM parts. It concludes with information on the applications of PM parts.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006081
EISBN: 978-1-62708-175-7
Abstract
This article briefly reviews the production methods and characteristics of plain carbon and low-alloy water-atomized iron and steel powders, high-porosity iron powder, carbonyl iron powder, and electrolytic iron powder. It emphasizes on atomized powders, because they are the most widely used materials for ferrous powder metallurgy. The article provides information on the properties and applications of these powders. It also includes an overview of diffusion alloying, basics of admixing, and bonded premixes.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006139
EISBN: 978-1-62708-175-7
Abstract
This article describes the fundamentals of various techniques used for the production of copper and copper alloy powders. These include atomization (water, air, and gas), oxide reduction, and electrolysis. The article discusses the effects of electrolyte composition and operating conditions on the characteristics of copper and copper alloy powders.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006111
EISBN: 978-1-62708-175-7
Abstract
This article provides information on the most frequently used atmospheres in commercial sintering of powder metallurgy iron and steel materials. These include endothermic, exothermic, dissociated ammonia, pure hydrogen, and nitrogen-base atmospheres. The article discusses sintering of iron and iron-graphite powder, iron-copper and iron-copper graphite, and alloy steels. The effects of various sinter conditions on the amount of combined carbon formed in the steel are also discussed. The article concludes with information on high-temperature sintering and sinter hardening.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006068
EISBN: 978-1-62708-175-7
Abstract
This article provides information on the process details that differ from general water atomization of metals as they relate to basic and engineering properties that are specific to stainless steel powders. The discussion focuses on the compacting-grade stainless steel powders. The process details include raw materials, melting method, and control of physical and chemical powder characteristics. The article describes the gas atomization of stainless steel powders and processes that are done after water atomization: drying, screening, annealing, and lubricating. It also discusses the two types of quality assurance testing measures for powder metallurgy stainless steels: tests for powder contamination and tests of chemical and physical properties.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006086
EISBN: 978-1-62708-175-7
Abstract
Various powder production processes allow precise control of the chemical composition and physical characteristics of powders and allow tailoring of specific attributes for targeted applications. Metal powders are produced by either mechanical methods or chemical methods. The commonly used mechanical methods include water and gas atomization, milling, mechanical alloying, and electrolysis. Some chemical methods include reduction of oxides. This article provides information on the reliable techniques for powder characterization and testing to evaluate the chemical and physical properties of metal powders, both as individual particles and in bulk forms.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006084
EISBN: 978-1-62708-175-7
Abstract
Atomization is the dominant method for producing metal and prealloyed powders from aluminum, brass, iron, low-alloy steels, stainless steels, tool steels, superalloys, titanium alloys, and other alloys. The general types of atomization processes encompass a number of industrial and research methods. This article describes the key process variables and production factors for the industrial methods: two-fluid, centrifugal, vacuum or soluble-gas, and ultrasonic atomization. It also reviews the effect of atomization methods and process variables on key powder characteristics such as the average particle size, particle size distribution or screen analysis, particle shape, chemical composition, and microstructure.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006087
EISBN: 978-1-62708-175-7
Abstract
This article provides a discussion on the process descriptions, processing conditions, and processing variables of the most common chemical methods for metal powder production. These methods include oxide reduction, precipitation from solution, and thermal decomposition. Methods such as precipitation from salt solution and gas, chemical embrittlement, hydride decomposition, and thermite reactions are also discussed. The article also discusses the methods used to produce powders electrolytically and the types of metal powders produced. The physical and chemical characteristics of these powders are also reviewed.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006122
EISBN: 978-1-62708-175-7
Abstract
This article discusses the methods for producing powder metallurgy (PM) nickel powders, including carbonyl process, hydrometallurgical process, hydrogen reduction process, and atomization process, as well as their applications. It describes three processes for producing nickel alloy powders: water atomization, high-pressure water atomization, and gas atomization. The article also provides information on the applications of PM hot isostatic pressing in the oil and gas industry.
Series: ASM Handbook
Volume: 4D
Publisher: ASM International
Published: 01 October 2014
DOI: 10.31399/asm.hb.v04d.a0005971
EISBN: 978-1-62708-168-9
Abstract
Powder metallurgy (PM) processes include press and sinter hardening, metal injection molding, powder forging, hot isostatic pressing, powder rolling, and spray forming. This article provides an overview of PM processing methods and general considerations of heat treatment of PM parts that are case-hardened to obtain higher hardness, wear, fatigue, and impact properties. It describes the effects of porosity on heat treatment, alloy content on PM hardenability, and starting material on homogenization of PM steels. The article describes the properties, following heat treatment, of low-alloy steels tempered at 175 ºC for one hour, and lists recommended quench and temper parameters to achieve good wear resistance and core strength based on different ranges of porosity.
Series: ASM Handbook
Volume: 23
Publisher: ASM International
Published: 01 June 2012
DOI: 10.31399/asm.hb.v23.a0005669
EISBN: 978-1-62708-198-6
Abstract
This article reviews the concepts considered important for an understanding of the processes used for preparing cobalt-chromium alloy implants, the microstructures resulting from this processing, and the resulting material properties. The review includes solidification of alloys, diffusionless (martensitic) phase transformation as occurs with face-centered cubic to hexagonal close-packed transformation in cobalt-chromium alloys, and stacking faults and twins and their role in this transformation. It also discusses the strengthening mechanisms that are responsible for the mechanical properties of cast and wrought cobalt alloys. The article contains tables that list the commonly used cobalt alloys and their biomedical applications and chemical compositions. It discusses the mechanical and corrosion properties of cobalt alloys, and provides a description of the microstructure of cobalt alloys.
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005225
EISBN: 978-1-62708-187-0
Abstract
Spray casting, also known as spray forming, is a niche casting process for the manufacture of preforms. This article lists commercial examples of alloys manufactured by spray casting and provides sequential steps of the spray casting process. Gas atomization is a chaotic, stochastic process that always produces a wide range of droplet diameters. The article schematically illustrates a typical log-normal droplet diameter probability density distribution on a mass or volume basis obtained by gas atomization. It also explains the changes in solid fraction during the spray casting process as a function of axial distance from the point of droplet atomization. The article concludes with information on the occurrence of macrosegregation and coarsening in spray cast preforms.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003185
EISBN: 978-1-62708-199-3
Abstract
This article focuses on the significant fundamental powder characteristics, which include particle size, particle size distribution, particle shape, and powder purity, followed by an overview of general and individual powder production processes such as mechanical, chemical, electrochemical, atomizing, oxide reduction, and thermal decomposition processes. It also covers the consolidation of powders by pressing and sintering, as well as by high density methods. Further emphasis is provided on the distinguishing features of powders, their manufacturing processes, compacting processes, and consolidated part properties. In addition, a glossary of powder metallurgy terms is included.
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