This article focuses on various vacuum heat treating processes for additively manufactured parts, namely annealing and stress relieving, solid-solution annealing, and solution treating and aging. It addresses several practical concerns involved in using vacuum heat treatment, including temperature measurement, unvented cavities, loose powder, and direct contact of metals in the high-temperature vacuum. The article provides a short discussion on sintering and evaporation of metals in vacuum furnaces.

Alloy 7040 is a variation of 7050, where Zr additions prevent recrystallization of hot-worked products during solution heat treatment without the quench sensitivity from additions of Cr. This datasheet provides information on composition limits and fabrication characteristics of aluminum alloys 7040 and 7140 and processing effects on mechanical properties of aluminum alloy 7040-T7651 high-strength plate.

This article summarizes a typical solution and aging heat treatments of 2xxx (Al-Cu), 6xxx (Al-Mg-Si), and 7xxx (Al-Zn-Mg) wrought alloys. It discusses the general aging characteristics and the effects of reheating of aluminum alloys. Typical examples of hardness and conductivity values for various aluminum alloy tempers are listed in a table. The article also describes the age hardening of Al-Cu (Mg) alloys, Al-Mg-Si alloys, and Zn-Mg-(Cu) aluminum alloys.

Heat treatment of aluminum alloys frequently refers to the heat treatable aluminum alloys that can be strengthened by solution treatment, quenching, and subsequent hardening. This article introduces the general metallurgy of strengthening aluminum alloys by heat treatment. It discusses various heat treatable alloying elements, such as copper, chromium, iron, magnesium, silicon, zinc, and lithium. The article describes the age-hardening treatments and generalized precipitation sequence for aluminum alloys. It reviews the solution heat treatment in terms of solution heating time and temperature, as well as high-temperature oxidation. The article also discusses quench sensitivity, vacancy loss, grain-boundary precipitates, and quench delay for the heat treatment of aluminum. It concludes with a discussion on the deformation of aluminum alloys prior to aging.

The fundamental objective of quenching is to preserve, as nearly as possible, a metastable solid solution formed at the solution heat treating temperature, by rapidly cooling to some lower temperature, usually near room temperature. This article provides an overview of the factors used to determine a suitable cooling rate and the appropriate quenching process to develop a suitable cooling rate. It discusses the three distinct stages of quenching: vapor stage, boiling stage, and convection stage. The article reviews the factors that affect the rate of cooling in production operations. It discusses the quenchants that are used in quenching aluminum alloys, namely, hot or cold water and polyalkylene glycol. The article also describes the racking practices for controlling distortion and the level of residual stresses induced during the quench.

The strength of aluminum castings can be improved significantly by heat treatments, which control the size, shape, and distribution of the impurity elements in the casting. This article presents a discussion on the heat treatment of aluminum alloy castings, with a focus on the fundamental technical aspects involved in each process step. The intent is to convey a good understanding of the fundamental aspects of heat treatment. Typical heat treatments of aluminum casting alloys are presented in a table. The article describes the solution heat treatment, quenching, and preaging of Al-Si-Mg alloys, as well as the solution heat treatment and artificial aging of Al-Si-Cu-Mg casting alloys.

This article provides a detailed discussion on the heat treatment processes for titanium and titanium alloys. These processes are age hardening, solution treatment, aging, and annealing. The article illustrates the characteristics of equilibrium phase diagrams that are important for understanding the heat treatment of titanium alloys. It explains the types of metastable phases encountered in titanium alloys. The article also provides information on the equilibrium phase relationships and properties of titanium alloys.

This article presents a detailed discussion on typical thermal treatment practices for hardening of various aluminum casting alloys. These practices are solution treatment, quenching or cooling, preaging, and artificial aging at an elevated temperature. The aluminum casting alloys considered here are: Al-Cu and Al-Cu-Mg (2xx) alloys, Al-Zn-Mg (7xx) alloys, Al-Si-Mg alloys, Al-Si-Cu, and Al-Si-Cu-Mg alloys.

This article discusses the various heat treating processes, namely, solid-solution hardening, solution treating, solution aging and dispersion hardening, for low-melting-point alloys such as lead alloys, tin-rich alloys, and zinc alloys. Heat treating of tin-rich alloys has been practiced for bearing alloys, pewterware, and organ pipe alloys. The article reviews the principles underlying these applications.

Cast nickel-base alloys are used extensively in corrosive-media and high-temperature applications. This article briefly reviews the common types of heat treatments of nickel alloy castings: homogenization, stress relieving, in-process annealing, full annealing, solution annealing, quenching, coating diffusion, and precipitation. It describes the three general strengthening mechanisms, namely, solid-solution hardening, age hardening, and carbide precipitation. The article summarizes the typical heat treatment of the general families of nickel-base castings used in industrial applications. It focuses on the solution treatment and age hardening of cast nickel-base superalloys and the heat treatment of cast solid-solution alloys for corrosion-resisting applications. The article also discusses the typical types of atmospheres used in annealing or solution treating: exothermic, endothermic, dry hydrogen, dry argon, and vacuum.

This article describes the heat treatment of wrought solid-solution and precipitation-hardening alloys with a focus on the major families of wrought nickel alloys. It also provides information on the heat treatment of some representative solid-solution alloys in the Monel (Ni-Cu), Inconel (Ni-Cr-Mo), Hastelloy (Ni-Mo-Cr), and Incoloy (Ni-Fe-Cr) families of alloys. The heat treatment processes for gamma prime nickel alloys, gamma prime nickel-iron superalloys, and gamma double-prime nickel-iron superalloys are also included. The article also provides information on age-hardenable alloys, and the effects of cold work on aging response and grain growth with examples.

The most widely accepted alloy and temper designation system for aluminum and its alloys is maintained by the Aluminum Association and recognized by the American National Standards Institute (ANSI) as the American National Standard Alloy and Temper Designation Systems for Aluminum (ANSI H35.1). This article provides a detailed discussion on the alloy and temper designation system for aluminum and its alloys. The Aluminum Association alloy designations are grouped as wrought and cast alloys. Lengthy tables provide information on alloying elements in wrought aluminum and aluminum alloys; nominal composition of aluminum alloy castings; typical mechanical properties of wrought and cast aluminum alloys in various temper conditions; and cross references to former and current cast aluminum alloy designations.

This article provides information on nickel alloying elements, and the heat treatment processes of various nickel alloys for applications requiring corrosion resistance and/or high-temperature strength. These processes are homogenization, annealing, solution annealing, solution treating, stabilization treatment, age hardening, stress relieving, and stress equalizing. Discussion of furnaces, fixtures, and atmospheres is included. Nickel alloys used for the heat treatment processes include corrosion-resistant nickel alloys, heat-resistant nickel alloys, nickel-beryllium alloys, special-purpose alloys such as nitinol shape memory alloys, low-expansion alloys, electrical-resistance alloys and soft magnetic alloys. Finally, the article focuses on heat treatment modeling for selecting the appropriate heat treatment process.

Annealing is an essential treatment in the fabrication of metal parts and semiproducts. This article discusses the processes involved in annealing, namely, recovery, recrystallization, and grain coarsening. It lists the heat treatment conditions of processed aluminum alloys. It provides information on the types of heat treatment, which include preheating, full anneal, stabilization, and stoving. The article describes the steps involved for achieving the age-hardening effect and the strongest hardening effect in aluminum. The steps to increase the strength of aluminum alloys by extremely fine, dispersed second-phase particles are: solution heat treatment, quenching, and age hardening. Finally, the article also discusses the process parameters of annealing, including the effect of strain, effect of temperature, effect of heating rate, and the effect of alloy elements, and the effect of annealing on anisotropy.

This article provides a detailed discussion on heat treatment of titanium alloys such as alpha alloys, alpha-beta alloys, and beta and near-beta alloys. Common processes include stress-relief, annealing, solution treating, aging, quenching, and age hardening. It provides information on the effects of alloying elements on alpha/beta transformation. The article also discusses the heat treating procedures, and the furnaces used for heat treating titanium and titanium alloys.

This article focuses on the aging characteristics of solution and precipitation heat treated aluminum alloy systems and their corresponding types. It includes information on aluminum-copper systems, aluminum-copper-magnesium systems, aluminum-magnesium-silicon systems, aluminum-zinc-magnesium systems, aluminum-zinc-magnesium-copper systems, and aluminum-lithium alloys.

Precipitation hardening is a hardening mechanism found in various steels and alloy systems, such as nickel-, cobalt-, titanium-, copper-, and iron-base alloys. This article provides a brief description of precipitation hardening process, furnace equipment, surface-related problems, and protective atmospheres used in heat treatment of iron-base precipitation-hardenable (PH) superalloys. It focuses on various factors to be considered in heat treating of PH stainless steels: cleaning prior to heat treatment, furnace atmospheres, time-temperature cycles, variations in cycles, and scale removal after heat treatment. The article describes the mechanical properties, solution treatment, and aging treatment for many martensitic PH alloys, including: Alloy 17-4 PH, Alloy 13-8 Mo, Alloy 15-5 PH, Custom 450, and Custom 455; as well as semiaustenitic PH stainless steels such as Alloy 17-7 PH, Alloy PH 15-7 Mo, AM-350, Pyromet 350, AM-355, and Pyromet 355; austenitic PH stainless steel, A-286; cast PH stainless steels; and iron-nickel PH superalloys.

This article provides an overview of heat treatment processes, namely, solution heat treatment, quenching, natural aging, and artificial aging. It contains a table that lists the various heat treatment tempers commonly practiced for nonferrous castings. The article describes microstructural changes that occur due to the heat treatment of cast alloys.

Heat treating of stainless steel produces changes in physical condition, mechanical properties, and residual stress level and restores maximum corrosion resistance when that property has been adversely affected by previous fabrication or heating. This article focuses on annealing of different types of stainless steels such as austenitic, ferritic, duplex, martensitic, and precipitation-hardening, and on the heat treatment of superalloys and refractory metals. It discusses the recommended procedures for solution annealing, austenite conditioning, transformation cooling, and age tempering of precipitation-hardening stainless steels. The article also lists general recommendations for the annealing temperatures of tantalum, niobium, molybdenum, tungsten, and their alloys.

This article addresses the general welding characteristics common to both solid-solution-strengthened and precipitation-hardened nickel-, iron-, and cobalt alloys.