This article surveys common additive manufacturing (AM) data-acquisition methods, covering preprocess materials characterization in the lab, machine calibration in the field, in-process monitoring during a build, and the postprocess part inspections and tests. The focus is to identify acquisition-related metadata for AM data sets to improve data usability and reusability. Also included in the article are exemplar metadata definitions for a data set acquired from light-scattering-based particle size analysis.

Rheology is defined as the study of the flow and deformation of matter. This article begins with an examination of flow behavior. It describes the geometries and methods employed for rheological testing of polymers in their molten state. It also discusses materials that are predominantly in the solid state and the methods employed for solids testing. Examples of unidirectional and dynamic oscillatory testing are provided for different mechanical behaviors.

During metal powder production, powder and/or dust handling, compaction, and part finishing operations, many safety and environmental risks exist. This article is a detailed account of the types of safety hazards that can exist and the issues that occur during metal powder handling, as well as recommendations and strategies that can be employed to both prevent and protect against damaging effects from powder exposure, fire and/or explosions, or environmental impact events.

This article provides an overview of the general methods of metal powder production. It details the primary methods for particle sizing used in additive manufacturing: sieving, laser diffraction and scattering, and digital image analysis. Methods of interpreting and understanding particle size distribution (PSD) data are presented, with an emphasis on the differences between count- and volume-based PSDs. The article then outlines practices for both qualitative and quantitative assessment of particle morphology.

Powder-bed additive manufacturing (AM) processes are some of the most commonly used techniques, necessitating the accurate measurement of powder flowability properties. This article discusses some powder flow tests that occur in powder-bed AM machines. These include the Hall/Carney flow test, bulk/tap density, rheometer, and the revolving or rotating drum technique. The three categories of powder properties that are available from rheometer experiments are discussed: bulk, dynamic flow, and shear properties. The article also describes the basic principles and applications of micro-X-ray computed tomography in studying powder porosity characteristics nondestructively.

This article uses metal and alloy powders as examples to briefly discuss how to perform the characterization of powders. It begins by reviewing some of the techniques involved in the sampling of powders to ensure accurate characterization. This is followed by a discussion on the important properties to characterize powders, namely the particle size, surface area, density, porosity, particle hardness, compressibility, green strength, and flowability. For characterization of powders, both individual particles and bulk powders are used to evaluate their physical and chemical properties. The article also discusses the important characteristics and compositions of powder as well as impurities that directly affect powder properties. It ends with a description of the ignition and dust-explosion characteristics of organic and metal powders.

This article summarizes sampling of powders, which includes the sampling of stored material and flowing streams, sample reduction and evaluation, and weight of sample required. It also summarizes the classification of powders. Classifiers are divided into two categories: counterflow equilibrium and crossflow separation. Classification methods are used to exclude certain powder sizes from a powder distribution and to obtain particular powder distributions. For example, sieving methods are used to obtain particular powder distributions and to obtain narrow size ranges of a powder. The article summarizes the sieving methods for powders. The sieving methods include hand sieving, machine sieving, manual wet sieving, air jet sieving, sonic sifter, wet sieving by machine, the Seishin robot sifter, automated systems, and ultrasonic machine sieving. The article outlines the sieve types and the process variables of the sieving process. An appendix reviews dispersion of powders in liquids.

Milling of materials, whether hard and brittle or soft and ductile, is of prime interest and of economic importance to the powder metallurgy (PM) industry. This article discusses the principles of milling, milling parameters, and the powder characteristics required for the process. It discusses the changes in powder particle morphology that occur during milling of metal powders produced by various processes such as microforging, fracturing, agglomeration, and deagglomeration. The article also provides useful information on milling equipment such as tumbler ball mills, vibratory ball mills, attrition mills, and hammer and rod mills.

This article focuses on the theory, advantages, and limitations of various methods used for the determination of surface area, density, and porosity of powder. These include gas adsorption, permeametry, pycnometry, and mercury porosimetry. Information on various equipment used in these processes are also provided.

Particle image analysis of metal powders can be easily performed with optical macroscopes and microscopes. This article provides examples of the particle image analysis on powders used in the powder metallurgy industry.

Various powder production processes allow precise control of the chemical composition and physical characteristics of powders and allow tailoring of specific attributes for targeted applications. Metal powders are produced by either mechanical methods or chemical methods. The commonly used mechanical methods include water and gas atomization, milling, mechanical alloying, and electrolysis. Some chemical methods include reduction of oxides. This article provides information on the reliable techniques for powder characterization and testing to evaluate the chemical and physical properties of metal powders, both as individual particles and in bulk forms.

Superalloys are predominantly nickel-base alloys that are strengthened by solid-solution elements including molybdenum, tungsten, cobalt, and by precipitation of a Ni 3 (Al, Ti) type compound designated as gamma prime and/or a metastable Ni 3 Nb precipitate designated as gamma double prime. This article provides a discussion on the conventional processing, compositions, characteristics, mechanical properties, and applications of powder metallurgy (PM) superalloys. The conventional processing of PM superalloys involves production of spherical prealloyed powder, screening to a suitable maximum particle size, blending the powder to homogenize powder size distribution, loading powder into containers, vacuum outgassing and sealing the containers, and consolidating the powder to full density. PM superalloys include Rene 95, IN-100, LC Astroloy, Udimet 720, N18, ME16, RR1000, Rene 88DT, PA101, MERL 76, AF2-1DA, Inconel 706, AF115, and KM4. The article reviews specialized PM superalloy processes and technical issues in the usage of PM superalloys.

Particle size and size distribution have a significant effect on the behavior of metal powders during their processing. This article provides an overview of the sample preparation process for particle size measurement, which is a key step in the measurement of particle size distributions. Common particle size measuring techniques discussed in this article include sieve analysis, quantitative image analysis, laser diffraction, sedimentation methods, aerodynamic time-of-flight method, electrical zone sensing, and photon correlation spectroscopy. The advantages and disadvantages of these methods are reviewed.

The raw materials used in thermal spray processes are a critical parameter in the finished coating because the variations in their size, morphology, chemistry, and phase composition can significantly impact coating properties. Therefore, it is important to test and characterize the raw materials. This article discusses various characterization methods for powders. Topics discussed include: methods for determining particle size and/or size distribution; powder and coating stoichiometry; particle chemistry; and phase analysis by x-ray diffraction. This article discusses the characterization of thermal spray powders which involves the determination of particle size and/or size distribution and phase analysis by x-ray diffraction. It provides information on preferential volatilization and rapid solidification that influence compositional differences. Wet chemical methods, spectographic analysis, and atomic absorption spectrometry are also discussed.

This article discusses three types of powder-feeder systems that are commonly used throughout the thermal spray (TS) industry: gravity-based devices, rotating wheel devices, and fluidized-bed systems. It provides information on the various mechanical methods for producing powders, namely, crushing, milling, attriting, and machining. The article describes two prime methods of agglomeration. One method uses a binder by way of agglutination, while the other relies on a sintering operation. The article discusses the technology and principles of the processes that relate to thermal spraying, and offers an understanding for choosing particular feedstock materials that are classified based on the thermal spray process, material morphology, chemical nature of the material, and applications. Sieving, the most common method of separating powders into their size fractions, is also reviewed. The article also provides information on the topical areas and precautions to be undertaken to protect the operator from safety hazards.

This article describes the results obtained by Volmer, Weber, Farkas, Becker, and Doring, which constitute the classical nucleation theory. These results are the predictions of the precipitate size distribution, steady-state nucleation rate, and incubation time. The article reviews a nucleating system as a homogeneous phase using the classical nucleation theory, along with heterophase fluctuations that led to the formation of precipitates. It discusses the gas cluster dynamics using the kinetic approach to describe nucleation. The article presents key parameters, such as cluster condensation and evaporation rates, to describe the time evolution of the system. The predictions and extensions of the classical nucleation theory are discussed. The article also provides the limitations of classical nucleation theories in cluster dynamics.

This article provides an overview of the thixocasting process and discusses the concepts that are important to the practical application of this technology. The thixocasting process involves two casting processes. The first casting process is required to make the feedstock that must be reheated to achieve the structures necessary for casting. The second casting process combines billet sawing, reheating, and the actual injecting of material into the mold. The article focuses on these processes and provides information on rheological tests. It discusses some key design concepts used in thixocasting. The article illustrates the differences between a conventional high-pressure die-casting injection profile and the thixocasting injection profile used to produce the same part.

Thermal analysis provides a powerful tool for researchers and engineers in determining both unknown and reproducible behavioral properties of polymer molecules. This article covers the thermal analysis and thermal properties of engineering plastics with respect to chemical composition, chain configuration, conformation of the base polymers, processing of the base polymers with or without additives; and the response to chemical, physical, and mechanical stresses of base polymers as unfilled, shaped articles or as components of composite structures. It also describes thermal analysis techniques, including differential scanning calorimetry, thermogravimetric analysis, thermomechanical analysis, and rheological analysis. This article also summarizes the basic thermal properties used in the application of engineering plastics, such as thermal conductivity, temperature resistance, thermal expansion, specific heat, and the determination of glass transition temperatures. It concludes with a discussion of the thermal and related properties of nine thermostat resin systems divided into three groups by low, medium, and high service temperature capabilities.

This article describes the structure of coatings produced by plasma spraying, vapor deposition, and electrodeposition processes. The main techniques used for microstructure assessment are introduced. The relationship between the microstructure and property is also discussed. The experimental techniques for microstructural characterization include metallographic technique, X-ray diffraction, electron, microscopies, and porosimetry.