Fatigue failure is a critical performance metric for additively manufactured (AM) metal parts, especially those intended for safety-critical structural applications (i.e., applications where part failure causes system failure and injury to users). This article discusses some of the common defects that occur in laser powder bed fusion (L-PBF) components, mitigation strategies, and their impact on fatigue failure. It summarizes the fatigue properties of three commonly studied structural alloys, namely aluminum alloy, titanium alloy, and nickel-base superalloy.

Boronizing is a case hardening process for metals to improve the wear life and galling resistance of metal surfaces. Boronizing can be carried out using several techniques. This article discusses the powder pack cementation process for carrying out boronizing. It describes the structures of boride layers in ferrous materials and boride-layer structures in nickel-base superalloys. The primary reason for boriding metals is to increase wear resistance against abrasion and erosion. The article reviews the wear resistance and coefficient of friction of boride layers, as well as galling resistance of borided surfaces. It concludes with a discussion on boronizing plus physical vapor deposition (PVD) overlay coating.

Cast nickel-base alloys are used extensively in corrosive-media and high-temperature applications. This article briefly reviews the common types of heat treatments of nickel alloy castings: homogenization, stress relieving, in-process annealing, full annealing, solution annealing, quenching, coating diffusion, and precipitation. It describes the three general strengthening mechanisms, namely, solid-solution hardening, age hardening, and carbide precipitation. The article summarizes the typical heat treatment of the general families of nickel-base castings used in industrial applications. It focuses on the solution treatment and age hardening of cast nickel-base superalloys and the heat treatment of cast solid-solution alloys for corrosion-resisting applications. The article also discusses the typical types of atmospheres used in annealing or solution treating: exothermic, endothermic, dry hydrogen, dry argon, and vacuum.

This article describes the heat treatment of wrought solid-solution and precipitation-hardening alloys with a focus on the major families of wrought nickel alloys. It also provides information on the heat treatment of some representative solid-solution alloys in the Monel (Ni-Cu), Inconel (Ni-Cr-Mo), Hastelloy (Ni-Mo-Cr), and Incoloy (Ni-Fe-Cr) families of alloys. The heat treatment processes for gamma prime nickel alloys, gamma prime nickel-iron superalloys, and gamma double-prime nickel-iron superalloys are also included. The article also provides information on age-hardenable alloys, and the effects of cold work on aging response and grain growth with examples.

Superalloys are predominantly nickel-base alloys that are strengthened by solid-solution elements including molybdenum, tungsten, cobalt, and by precipitation of a Ni 3 (Al, Ti) type compound designated as gamma prime and/or a metastable Ni 3 Nb precipitate designated as gamma double prime. This article provides a discussion on the conventional processing, compositions, characteristics, mechanical properties, and applications of powder metallurgy (PM) superalloys. The conventional processing of PM superalloys involves production of spherical prealloyed powder, screening to a suitable maximum particle size, blending the powder to homogenize powder size distribution, loading powder into containers, vacuum outgassing and sealing the containers, and consolidating the powder to full density. PM superalloys include Rene 95, IN-100, LC Astroloy, Udimet 720, N18, ME16, RR1000, Rene 88DT, PA101, MERL 76, AF2-1DA, Inconel 706, AF115, and KM4. The article reviews specialized PM superalloy processes and technical issues in the usage of PM superalloys.

Precipitation hardening is a hardening mechanism found in various steels and alloy systems, such as nickel-, cobalt-, titanium-, copper-, and iron-base alloys. This article provides a brief description of precipitation hardening process, furnace equipment, surface-related problems, and protective atmospheres used in heat treatment of iron-base precipitation-hardenable (PH) superalloys. It focuses on various factors to be considered in heat treating of PH stainless steels: cleaning prior to heat treatment, furnace atmospheres, time-temperature cycles, variations in cycles, and scale removal after heat treatment. The article describes the mechanical properties, solution treatment, and aging treatment for many martensitic PH alloys, including: Alloy 17-4 PH, Alloy 13-8 Mo, Alloy 15-5 PH, Custom 450, and Custom 455; as well as semiaustenitic PH stainless steels such as Alloy 17-7 PH, Alloy PH 15-7 Mo, AM-350, Pyromet 350, AM-355, and Pyromet 355; austenitic PH stainless steel, A-286; cast PH stainless steels; and iron-nickel PH superalloys.

The warm and hot working of metals provide the ability to shape important materials into component shapes that are useful in a variety of applications requiring strength, toughness, and ductility. This article focuses on a variety of metals that can be hot or warm worked, and describes the characteristics and processing considerations of each metal. It discusses forging because it is a versatile metalworking process and performed at cold, warm, and hot working temperatures. The article also presents the applications of steels, stainless steels, aluminum alloys, titanium alloys, superalloys, and copper alloys.

This article discusses special considerations relative to induction heating of stainless steels and nickel-base superalloys. It focuses on the various industrial and high-temperature applications of induction heating to stainless steel and superalloy components, namely, primary melting processes, preheating for primary and secondary forming processes, heat treatments, brazing, and thermal processing for fusion welds. The article also provides information on computational modeling of induction heating processes for super alloys and stainless steels.

Materials resulting from thermal spray processes are often different from their wrought, forged, and cast counterparts. Assessing the usefulness of thermal spray coatings requires understanding, developing, and using appropriate testing and characterization methods that are generally borrowed from other materials science disciplines. This article focuses on commonly used testing and characterization methods: metallography, image analysis, hardness, tensile adhesion testing, corrosion testing, x-ray diffraction, non-destructive testing, and powder characterization. It provides information on how the materials themselves respond to the various test methods. The article focuses on the test methods themselves, including those test parameters that can be varied and the influence of each on the results obtained.

A key differentiator between friction stir welding (FSW) and other friction welding processes is the presence of a nonconsumable tool in FSW, often referred to as a pin tool to differentiate it from other tooling associated with the process. This article discusses materials for friction stir welding (FSW) pin tools, various tool geometries that have been used, designs for specific applications, predicting and measuring tool performance, and other considerations in FSW pin tool design. The tool materials include tool steels, superalloys, refractory metals, carbides and ceramics, and superabrasives.

Solid-state transformations occurring in a weld are highly nonequilibrium in nature and differ distinctly from those experienced during casting, thermomechanical processing, and heat treatment. This article provides a description of the special factors affecting transformation behavior in a weldment. It reviews the heat-affected and fusion zones of single-pass and multi-pass weldments. The article also includes a discussion on the welds in alloy systems, such as stainless steels and aluminum-base, nickel-base, and titanium-base alloys.

This article summarizes the general features of microstructure evolution during the thermomechanical processing (TMP) of nickel-base superalloys and the challenges posed by the modeling of such phenomena. It describes the fundamentals and implementations of various modeling methodologies. These include JMAK (Avrami) models, topological models, and mesoscale physics-based models.

This article discusses the two extremes of solute redistribution, equilibrium solidification and nonequilibrium Gulliver-Scheil solidification, for which solid redistribution of solute within the primary solid phase is the distinguishing parameter. The process and material parameters that control microsegregation are discussed in relation to the manifestations of microsegregation in simple and then increasingly complex alloy systems. The measurement and kinetics of microsegregation are discussed for the binary isomorphous systems: titanium-molybdenum; binary eutectic systems: aluminum-copper and aluminum-silicon; binary peritectic systems: copper-zinc; multicomponent eutectic systems: Al-Si-Cu-Mg; and for systems with both eutectic and peritectic reactions: Fe-C-Cr and nickel-base superalloy.

The vacuum arc remelting (VAR) process is widely used to improve the cleanliness and refine the structure of standard air melted or vacuum induction melted (VIM) ingots. It is also used in the triplex production of superalloys. This article illustrates the VAR process and the capabilities and variables of the process. It also presents a discussion on the melt solidification, resulting structure, and ingot defects. The article concludes with a discussion on the VAR process of superalloy and titanium and titanium alloy.

The corrosion issues in the compressor, combustor and turbine sections of industrial gas turbines used in steam production generally depend on the quality of the fuel, air, and water used in the engine than on the specific industrial application. This article focuses on the forms of corrosion and their preventive measures in the compressor, combustor and turbine sections of a steam turbine. The compressor section mainly suffers from aqueous corrosion; while in case of the combustor and turbine sections, which are made of nickel-base superalloys, high-temperature environmental attack in the form of high-temperature oxidation and hot corrosion are predominant. The effect of high-temperature oxidation and hot corrosion on the mechanical properties of superalloys is also discussed.

This article lists functions of lubricants common to the majority of applications and processes. It discusses the lubricant candidates widely used in forging: conversion coatings with soaps (stearate compounds) and molybdenum disulfide for cold forging; oil-based thick, film oil or polymerbased lubricants and molybdenum disulfide for warm application; graphite suspensions in oil or water for hot forging steels; and glass films for titanium and superalloys hot forgings. The article describes the applications of lubricants in warm extrusion and forging, hot forging of steel, hot forging of aluminum, isothermal and hot die forging, and the extrusion of steel.

A wide range of flow-formed open- and close-ended shapes are currently available in a variety of difficult-to-form materials, including titanium alloys and nickel-base super alloys. This article describes the two basic methods of flow forming that are characterized by the position of the rolls during the forming process. The flow forming methods include staggered-roll flow forming process and in-line flow-forming process. Typical mechanical properties of flow-formed materials in various conditions are summarized in a table. Proper process controls and subsequent product qualification tests are critical to assure optimal performance of the flow-formed tubular component. The article discusses the most commonly required process control parameters and the effects of forming speed and temperature in the flow forming process.

The thermomechanical processing (TMP) of conventional and advanced nickel and titanium-base alloys is aimed at altering or enhancing one or more metallurgical features within the material and component. This article presents a number of examples of the TMP of nickel-base superalloys and titanium alloys. The TMP techniques include retained-strain processing, dual-microstructure processing, and dual-alloy processing. The article also describes the TMP of alpha-beta titanium alloys, including fine-grain processing, hybrid-structure processing, dual-microstructure processing, and dual-alloy processing. It concludes with a discussion on computer simulation of advanced TMP processes.