This article presents fractographs of pure irons that show evidence of overload, fatigue, and embrittlement. Woody fracture, microvoid coalescence, cleavage, and stress rupture are seen in the overload failure images. A large inclusion is seen in the fatigue fractograph. Embrittlement images show an impact fracture with intergranular rupture and transcrystalline cleavage.

This article discusses several examples of fatigue load histories that intentionally create artificial fracture-surface markings during testing such that they are measurable by post-test quantitative fractography (QF). It reviews a number of methods for providing fatigue fracture-surface markers to aid QF of fatigue crack growth (FCG). These methods are based on load changes, including reordering the basic load histories and/or adding loads to them. The article also provides some guidelines for obtaining recognizable FCG markers for a variety of load histories and crack-growth regimes for coupons, components, and, particularly, full-scale fatigue tests.

This article examines residual stresses in quenched and surface-hardened steels by focusing on its theoretical background, formation mechanisms of residual stress, effects of tempering and cryogenic cooling on residual stress, effects of residual stress on the service performance of components, and measurement, computation, and relaxation of residual stress.

Quenching is one of the most important heat treating processes, because it is so closely related to dimensional control requirements and control of residual stresses. This article provides an overview of the fundamental material- and process-related parameters of quenching on residual stress, distortion control, and cracking. This overview is followed by various selected case histories of failures attributed to the quenching process.

Structure-property relationships for metal additive manufacturing (AM) using solidification-based AM processes (e.g., powder-bed fusion and directed-energy deposition) are the focus of this article. Static strength and ductility properties in AM materials are impacted heavily by the microstructure but are also affected by porosity and surface roughness. Fatigue failure in AM materials is also influenced by porosity, surface roughness, microstructure, and residual stress due to applied manufacturing processing parameters. Post-processing treatments can further influence fatigue failure in AM materials.

This article provides an overview of different modeling approaches used to capture the phenomena present in the additive manufacturing (AM) process. Inherent to the thermomechanical processing that occurs in AM for metals is the development of residual stresses and distortions. The article then provides an overview of thermal modeling. It presents a discussion on solid mechanics simulation and microstructure simulation.

This article surveys common additive manufacturing (AM) data-acquisition methods, covering preprocess materials characterization in the lab, machine calibration in the field, in-process monitoring during a build, and the postprocess part inspections and tests. The focus is to identify acquisition-related metadata for AM data sets to improve data usability and reusability. Also included in the article are exemplar metadata definitions for a data set acquired from light-scattering-based particle size analysis.

This article discusses several alternative mechanical test approaches that can be applied to additive manufacturing (AM) materials, both for smaller-scale assessments and for specimens that have been extracted from an AM component. This includes small punch testing, shear punch testing, and small ring testing.

This article addresses some established protocols for characterizing thermoplastics and whether they are homogeneous resins, alloyed, or blended compositions or highly modified thermoplastic composites. It begins with a discussion on characterizing mechanical, rheological, and thermal properties of polymer. This is followed by a section describing molecular weight determination using viscosity measurements. Next, the article discusses the use of cone and plate and parallel plate geometries in melt rheology. It then reviews the processes involved in the analysis of thermoplastic resins by chromatography. Finally, the article covers three operations of thermoanalysis, namely differential scanning calorimetry, thermogravimetric analysis, and thermomechanical testing.

This article discusses the most common thermal analysis methods for thermosetting resins. These include differential scanning calorimetry, thermomechanical analysis, thermogravimetric analysis, and dynamic mechanical analysis. The article also discusses the characterization of uncured thermosetting resins as well as the curing process. Then, the techniques to characterize the physical properties of cured thermosets and composites are presented. Several examples of stress-strain curves are shown for thermosets and thermoplastic polymers.

Rheology is defined as the study of the flow and deformation of matter. This article begins with an examination of flow behavior. It describes the geometries and methods employed for rheological testing of polymers in their molten state. It also discusses materials that are predominantly in the solid state and the methods employed for solids testing. Examples of unidirectional and dynamic oscillatory testing are provided for different mechanical behaviors.

This article briefly introduces some commonly used methods for mechanical testing. It describes the test methods and provides comparative data for the mechanical property tests. In addition, creep testing and dynamic mechanical analyses of viscoelastic plastics are also briefly described. The article discusses the processes involved in the short-term and long-term tensile testing of plastics. Information on the strength/modulus and deflection tests, impact toughness, hardness testing, and fatigue testing of plastics is also provided. The article describes tension testing of elastomers and fibers. It covers two basic methods to test the mechanical properties of fibers, namely the single-filament tension test and the tensile test of a yarn or a group of fibers.

This article describes the viscoelastic behavior of plastics in their solid state only, from the standpoint of the material deforming without fracturing. The consequences of viscoelasticity on the mechanical properties of plastics are described, especially in terms of time-dependencies, as well as the dependence of the viscoelastic character of a plastic on chemical, physical, and compositional variables. By examining the viscoelastic behavior of plastics, the information obtained are then applied in situations in which it may be important to anticipate the long-term properties of a material. This includes assessing the extent of stress decay in materials that are pre-stressed, the noise and vibration transmission characteristics of a material, the amount of heat build-up in a material subjected to cyclic deformation, and the extent a material can recover from any prior deformation. Several qualitative graphs are presented, which highlights the possible differences in the viscoelastic behavior that can exist among plastics.

This article reviews the impact response of plastic components and the various methods used to evaluate it.. It describes the effects of loading rate on polymer deformation and the influence of temperature and strain rate on failure mode. It discusses the advantages and limitations of standard impact tests, the use of puncture tests for assessing material behavior under extreme strain, and the application of fracture mechanics for analyzing impact failures. It also develops and demonstrates the theory involved in the design and analysis of thin-walled, injection-molded plastic components.

This article provides some new developments in elevated-temperature and life assessments. It is aimed at providing an overview of the damage mechanisms of concern, with a focus on creep, and the methodologies for design and in-service assessment of components operating at elevated temperatures. The article describes the stages of the creep curve, discusses processes involved in the extrapolation of creep data, and summarizes notable creep constitutive models and continuum damage mechanics models. It demonstrates the effects of stress relaxation and redistribution on the remaining life and discusses the Monkman-Grant relationship and multiaxiality. The article further provides information on high-temperature metallurgical changes and high-temperature hydrogen attack and the steps involved in the remaining-life prediction of high-temperature components. It presents case studies on heater tube creep testing and remaining-life assessment, and pressure vessel time-dependent stress analysis showing the effect of stress relaxation at hot spots.

Welded connections are a common location for failures for many reasons, as explained in this article. This article looks at such failures from a holistic perspective. It discusses the interaction of manufacturing-related cracking and service failures and primarily deals with failures that occur in service due to stresses caused by externally applied loads. The purpose of this article is to enable a failure analyst to identify the causative factors that lead to welded connection failure and to identify the corrective actions needed to overcome such failures in the future. Additionally, the reader will learn from the mistakes of others and use principles that will avoid the occurrence of similar failures in the future. The topics covered include failure analysis fundamentals, welded connections failure analysis, welded connections and discontinuities, and fatigue. In addition, several case studies that demonstrate how a holistic approach to failure analysis is necessary are presented.