The measurement of thermophysical properties of metal alloys, especially at high temperatures, is difficult because of the reactivity of some alloys. This article reviews the methods available for measurement of thermal and other physical properties for liquid, semi-solid, and solid commercial alloys, including adiabatic calorimetry, modulated calorimetry, Calvet calorimetry, single-pan calorimetry, and drop calorimetry. It describes differential scanning calorimetry and differential temperature analysis for measuring transition temperatures such as phase transformation or glass transition temperatures. The article schematically illustrates the laser flash apparatus for measuring the thermal diffusivity of solids and oscillation viscometer for measurements of the viscosity of metals. A summary of the measurement methods is presented in tables.

Forming processes can be divided into three major categories: bulk forming, sheet-metal forming, and semisolid forming and polymer extrusion. This article introduces each process category with a description of the constitutive models. It outlines the required properties for process modeling and describes the test methods for determining these properties. The article discusses several compression tests used to determine stress-strain curves for bulk forming and tensile tests used to obtain stress-strain curves for sheet-metal forming. The article concludes with information on the measurement of viscosity of semisolid alloy materials by using three types of viscometers: the coaxial cylinder viscometer, the cone-and-plate viscometer, and the capillary viscometer.