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Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006768
EISBN: 978-1-62708-295-2
... Abstract X-ray diffraction (XRD) residual-stress analysis is an essential tool for failure analysis. This article focuses primarily on what the analyst should know about applying XRD residual-stress measurement techniques to failure analysis. Discussions are extended to the description of ways...
Abstract
X-ray diffraction (XRD) residual-stress analysis is an essential tool for failure analysis. This article focuses primarily on what the analyst should know about applying XRD residual-stress measurement techniques to failure analysis. Discussions are extended to the description of ways in which XRD can be applied to the characterization of residual stresses in a component or assembly and to the subsequent evaluation of corrective actions that alter the residual-stress state of a component for the purposes of preventing, minimizing, or eradicating the contribution of residual stress to premature failures. The article presents a practical approach to sample selection and specimen preparation, measurement location selection, and measurement depth selection; measurement validation is outlined as well. A number of case studies and examples are cited. The article also briefly summarizes the theory of XRD analysis and describes advances in equipment capability.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003528
EISBN: 978-1-62708-180-1
... Abstract This article focuses primarily on what an analyst should know about applying X-ray diffraction (XRD) residual stress measurement techniques to failure analysis. Discussions are extended to the description of ways in which XRD can be applied to the characterization of residual stresses...
Abstract
This article focuses primarily on what an analyst should know about applying X-ray diffraction (XRD) residual stress measurement techniques to failure analysis. Discussions are extended to the description of ways in which XRD can be applied to the characterization of residual stresses in a component or assembly. The article describes the steps required to calibrate instrumentation and to validate stress measurement results. It presents a practical approach to sample selection and specimen preparation, measurement location selection, and measurement depth selection, as well as an outline on measurement validation. The article also provides information on stress-corrosion cracking and corrosion fatigue. The importance of residual stress in fatigue is described with examples. The article explains the effects of heat treatment and manufacturing processes on residual stress. It concludes with a section on the XRD stress measurements in multiphase materials and composites and in locations of stress concentration.
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in X-Ray Diffraction Residual-Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 15 January 2021
Fig. 8 Effect of surface R a on x-ray diffraction stress measurements. (a) X-ray penetration depth is greater than R a . (b) X-ray penetration depth is less than R a . Source: Ref 35
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in X-Ray Diffraction Residual Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 01 January 2002
Fig. 6 X-ray diffraction stress versus applied stress for varying average roughness ( R a ). (a) Samples with R a of 1, 3, and 6 μm. (b) Samples with R a of 1, 40, and 56 μm. (Source: Ref 26 )
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in X-Ray Diffraction Residual Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 01 January 2002
Fig. 9 X-ray diffraction stress versus applied stress on (a) as-received and (b) electropolished surfaces
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in X-Ray Diffraction Residual Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 01 January 2002
Fig. 14 X-ray diffraction residual-stress map showing the introduction of compressive surface residual stresses in the parent material and the reduction, but not elimination, of tensile residual stresses in the weld metal on the unmasked side from shot peening a nickel alloy weldment. Source
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in X-Ray Diffraction Residual Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 01 January 2002
Fig. 28 X-ray diffraction residual stress versus heat treatment temperature for various iron alloys. Specimens were held at temperature for 1 h and furnace cooled.
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in Brittle Fracture of a Cast Iron Valve in Oleum and Sulfuric Acid Service
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1992
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in Failure Analysis of High-Level Radioactive Waste Tank Purge
> Handbook of Case Histories in Failure Analysis
Published: 01 December 2019
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in Failure Analysis of High-Level Radioactive Waste Tank Purge
> Handbook of Case Histories in Failure Analysis
Published: 01 December 2019
Fig. 12 X-ray diffraction (XRD) pattern of oxide in vent pipe adjacent to bottom iron oxide trail
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in The Role of Impact Energy in Failure of Explosive Cladding of Inconel 625 and Steel
> Handbook of Case Histories in Failure Analysis
Published: 01 December 2019
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Published: 15 May 2022
Fig. 37 X-ray diffraction curve of unoriented polyethylene (PE); (a) at 100 °C (212 °F), (b) at 120 °C (250 °F)
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Published: 15 May 2022
Fig. 38 X-ray diffraction curve of two-dimensional ordering in a polymer, short-range ordering. Source: Ref 38
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Published: 15 January 2021
Fig. 10 Typical x-ray diffraction spectral data used to identify rutile TiO 2 . Significant peak positions are noted by d-spacing calculation of the 2θ position. Courtesy of P. Howard, NASA
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in X-Ray Diffraction Residual-Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 15 January 2021
Fig. 6 X-ray diffraction (XRD) stress versus applied stress for varying average roughness ( R a ). (a) Samples with R a of 1, 3, and 6 μm. (b) Samples with R a of 1, 40, and 56 μm. Source: Ref 35
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in X-Ray Diffraction Residual-Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 15 January 2021
Fig. 7 Ratio of measured stress (XRD, x-ray diffraction) and applied stress for varying average roughness, R a . Source: Ref 35
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in X-Ray Diffraction Residual-Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 15 January 2021
Fig. 9 X-ray diffraction stress versus applied stress on (a) as-received and (b) electropolished surfaces
More
Image
in X-Ray Diffraction Residual-Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 15 January 2021
Fig. 14 X-ray diffraction residual-stress map showing the introduction of compressive surface residual stresses in the parent material and the reduction, but not elimination, of tensile residual stresses in the weld metal on the unmasked side from shot peening a nickel alloy weldment. Source
More
Image
in X-Ray Diffraction Residual-Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 15 January 2021
Fig. 21 Theoretical model versus x-ray-diffraction-generated experimental data plots of residual stress versus number of cycles. Source: Ref 53
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in X-Ray Diffraction Residual-Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 15 January 2021
Fig. 28 X-ray diffraction (XRD) residual stress versus heat treatment temperature for various iron alloys. Specimens were held at temperature for 1 h and furnace cooled.
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