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M. Mobin, A. U. Malik
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Book Chapter
Feedwater Piping Erosion at a Waste-to-Energy Plant
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001276
EISBN: 978-1-62708-215-0
... Abstract The carbon steel feedwater piping at a waste-to-energy plant was suffering from wall thinning and leaking after being in service for approximately six years. Metallographic examination of ring sections removed front the piping revealed a normal microstructure consisting of pearlite...
Abstract
The carbon steel feedwater piping at a waste-to-energy plant was suffering from wall thinning and leaking after being in service for approximately six years. Metallographic examination of ring sections removed front the piping revealed a normal microstructure consisting of pearlite and ferrite. However, the internal surface on the thicker regions of the rings exhibited significant deposit buildup, where the thinned regions showed none. No significant corrosion or pitting was observed on either the internal or external surface of the piping. The lack of internal deposits on the affected areas and the evidence of flow patterns indicated that the wall thinning and subsequent failure were caused by internal erosion damage. The exact cause of the erosion could not be determined by the appearance of the piping. Probable causes of the erosion include an excessively high velocity flow through the piping, extremely turbulent flow, and/or intrusions (weld backing rings or weld bead protrusions) on the internal surface of the pipes. Increasing the pipe diameter and decreasing the intrusions on the internal surface would help to eliminate the problem.
Book Chapter
Metallurgical Evaluation of a Five Inch Cylindrical Induction Melter
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001598
EISBN: 978-1-62708-232-7
... Abstract The metallurgical condition of a cylindrical induction melter (CIM) vessel was evaluated after approximately 375 h of operation over a two-year span at temperatures between 1400 to 1500 deg C. Wall thinning and significant grain growth was observed in the lower portion of the conical...
Abstract
The metallurgical condition of a cylindrical induction melter (CIM) vessel was evaluated after approximately 375 h of operation over a two-year span at temperatures between 1400 to 1500 deg C. Wall thinning and significant grain growth was observed in the lower portion of the conical section and the drain tube. No through-wall penetrations were found in the cylindrical and conical sections of the CIM vessel and only one leak site was identified in the drain tube. Failure of the drain tube was associated with localized overheating and creep. The observed degradation resulted from cumulative service at elevated temperature. A recommendation was made to implement a support for the conical section of the CIM and to increase the wall thickness of the drain tube. Thus, the possibility of drain tube misalignment in the induction coils and localized over heating will be minimized. In addition, the use of grain stabilized Pt/Rh alloy should be evaluated as a method to prevent grain growth.
Book Chapter
Caustic Corrosion Failure of Back Wall Riser Tube in a High-Pressure Boiler
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001826
EISBN: 978-1-62708-241-9
... testing, energy dispersive x-ray analysis, and inductively coupled plasma mass spectrometry. The tube was made from SA 210A1 carbon steel that had been compromised by wall thinning and the accumulation of fire and water-side scale deposits. Investigators determined that the tube failed due to prolonged...
Abstract
A back wall riser tube in a high pressure boiler failed, interrupting operations in a cogeneration plant. The failure occurred in a tube facing the furnace, causing eight ruptured openings over a 1.8 m section. The investigation consisted of an on-site visual inspection, nondestructive testing, energy dispersive x-ray analysis, and inductively coupled plasma mass spectrometry. The tube was made from SA 210A1 carbon steel that had been compromised by wall thinning and the accumulation of fire and water-side scale deposits. Investigators determined that the tube failed due to prolonged caustic attack that led to ruptures in areas of high stress. The escaping steam eroded the outer surface of the tube causing heavy loss of metal around the rupture points.
Book Chapter
Corrosion Failure of a Chemical Process Piping Cross-Tee Assembly
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001325
EISBN: 978-1-62708-215-0
... failure at this location because the weld was abnormally thin as fabricated. Thus, failure resulted from inadequate deposition of weld metal and subsequent wall thinning from internal corrosion. It was recommended that the cross-tee be replaced with a like component, with more careful attention to weld...
Abstract
A carbon steel piping cross-tee assembly which conveyed hydrogen sulfide (H7S) process gas at 150 to 275 deg C (300 to 585 deg F) with a maximum allowable operating pressure of 3 MPa (450 psig) ruptured at the toe of one of the welds at the cross after several years of service. The failure was initially thought to be the result of thermal fatigue, and the internal surfaces exhibited the “elephant hide” pattern characteristic of thermal fatigue. However metallographic failure analysis found that this pattern was the result of corrosion rather than thermal fatigue. Corrosion caused failure at this location because the weld was abnormally thin as fabricated. Thus, failure resulted from inadequate deposition of weld metal and subsequent wall thinning from internal corrosion. It was recommended that the cross-tee be replaced with a like component, with more careful attention to weld quality.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001333
EISBN: 978-1-62708-215-0
... Abstract A low-carbon steel (St35.8) tube in a phthalic anhydride reactor system failed. Visual and stereomicroscopic examination of fracture surfaces revealed heavy oxide/deposits on the outer surface of the tube, tube wall thinning in the area of the fracture, and discolorations and oxides...
Abstract
A low-carbon steel (St35.8) tube in a phthalic anhydride reactor system failed. Visual and stereomicroscopic examination of fracture surfaces revealed heavy oxide/deposits on the outer surface of the tube, tube wall thinning in the area of the fracture, and discolorations and oxides/deposits on the inner surface. Cross sections from the fracture surface were metallographically examined, and the deposits were analyzed. It was determined that the tube had thinned from the inner surface because of a localized overheating condition (probably resulting from a runaway chemical reaction within the tube) and then fractured, which allowed molten salt to flow into the tube.
Book Chapter
Failure of Inconel 600 Thin-Walled Tubes Due to Nitriding
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001676
EISBN: 978-1-62708-229-7
Abstract
The self-powered flux detectors used in some nuclear reactors are Pt or V-cored co-axial cables with MgO as an insulator and Inconel 600 as the outer sheath material. The detectors are designed to operate in a He atmosphere; to maximize the conduction of heat (generated from the interaction with gamma radiation) and to prevent corrosion. A number of failures have occurred over the years because of a loss of the He cover gas in the assembly. This has resulted in either acid attack on the Inconel 600 sheath in a wet environment or gaseous corrosion in a dry environment. In the latter case, nitriding and embrittlement occurred at temperatures as low as 300 to 400 deg C (determined from an examination of the oxidation of the Zircaloy-2 carrier rod on which the detectors were mounted). Recent results are described and discussed in terms of the oxidation and nitriding kinetics of Zircaloy-2 and Inconel 600, respectively.
Book Chapter
An Investigation of the Development of Defects During Flow Forming of High Strength Thin Wall Steel Tubes
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001601
EISBN: 978-1-62708-235-8
... Abstract Flow forming technology has emerged as a promising, economical metal forming technology due to its ability to provide high strength, high precision, thin walled tubes with excellent surface finish. This paper presents experimental observations of defects developed during flow forming...
Abstract
Flow forming technology has emerged as a promising, economical metal forming technology due to its ability to provide high strength, high precision, thin walled tubes with excellent surface finish. This paper presents experimental observations of defects developed during flow forming of high strength SAE 4130 steel tubes. The major defects observed are fish scaling, premature burst, diametral growth, microcracks, and macrocracks. This paper analyzes the defects and arrives at the causative factors contributing to the various failure modes.
Book Chapter
Coal-Ash Corrosion of a Chromium-Molybdenum Steel Superheater Tube
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c0048331
EISBN: 978-1-62708-229-7
... of the rupture. A red and white deposit was found on the sides and bottom of the tube in the rupture area. The deposit was produced by attack of the steel by the alkali acid sulfate and had thinned the tube wall. It was concluded that rupture of the tube had occurred due to thinning of the wall by coal-ash...
Abstract
The top tube of a horizontal superheater bank in the reheat furnace of a steam generator ruptured after seven years in service. The rupture was found to have occurred in the ferritic steel tubing (2.25Cr-1Mo steel (ASME SA-213, grade T-22)) near the joint where it was welded to austenitic stainless steel tubing (type 321 stainless steel (ASME SA-213, grade TP321H)). The surface temperature of the tube was found to be higher than operating temperature in use earlier. The ferritic steel portion of the tube was found to be longitudinally split and heavily corroded in the region of the rupture. A red and white deposit was found on the sides and bottom of the tube in the rupture area. The deposit was produced by attack of the steel by the alkali acid sulfate and had thinned the tube wall. It was concluded that rupture of the tube had occurred due to thinning of the wall by coal-ash corrosion. The thinned tubes were reinforced by pad welding. Type 304 stainless steel shields were welded to the stainless steel portions of the top reheater tubes and were held in place about the chromium-molybdenum steel portions of the tubes by steel bands.
Image
Published: 01 June 2019
Image
Structure of second crankcase. 100 × a. Unetched. In the thin-walled part w...
Available to Purchase
in Cracked Cast Iron Crankcases
> ASM Failure Analysis Case Histories: Processing Errors and Defects
Published: 01 June 2019
Fig. 6 Structure of second crankcase. 100 × a. Unetched. In the thin-walled part with crack. Structure of second crankcase. 100 × b. Picral. In the thin-walled part with crack.
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Image
in Cracked Cast Iron Crankcases
> ASM Failure Analysis Case Histories: Processing Errors and Defects
Published: 01 June 2019
Image
in Cracked Cast Iron Crankcases
> ASM Failure Analysis Case Histories: Processing Errors and Defects
Published: 01 June 2019
Image
Case of old design. Thin-walled part. Microstructure of crankcase, etch: Pi...
Available to Purchase
in Cracks in Cylinder Blocks and in Cast Iron Cylinder Head
> ASM Failure Analysis Case Histories: Construction, Mining, and Agricultural Equipment
Published: 01 June 2019
Image
Thin-walled part of reinforced case. Microstructure of crankcase, etch: Pic...
Available to Purchase
in Cracks in Cylinder Blocks and in Cast Iron Cylinder Head
> ASM Failure Analysis Case Histories: Construction, Mining, and Agricultural Equipment
Published: 01 June 2019
Book Chapter
Remote Inspection of a 46-Year-Old Buried High-Level Waste Storage Tank
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001639
EISBN: 978-1-62708-229-7
... on specified areas of the tank. No indications of reportable wall loss or pitting were detected. All thickness readings were above minimum design tank-wall thickness, although several small indications of thinning were noted. The crack detection and sizing examinations revealed five previously undetected...
Abstract
This paper describes the remote ultrasonic (UT) examinations of a high-level radioactive waste storage tank at the Savannah River Site in South Carolina. The inspections, carried out by E.R. Holland, R.W. Vande Kamp, and J.B. Elder, were performed from the contaminated, annular space of the 46 year old, inactive, 1.03 million gallon waste storage tank. A steerable, magnetic wheel wall crawler was inserted into the annular space through small (6 in., or 150 mm, diam) holes/risers in the tank top. The crawler carried the equipment used to simultaneously collect data with up to four UT transducers and two cameras. The purpose of this inspection was to verify corrosion models and to investigate the possibility of previously unidentified corrosion sites or mechanisms. The inspections included evaluation of previously identified leak sites, thickness mapping, and crack detection scans on specified areas of the tank. No indications of reportable wall loss or pitting were detected. All thickness readings were above minimum design tank-wall thickness, although several small indications of thinning were noted. The crack detection and sizing examinations revealed five previously undetected indications, four of which were only partially through-wall. The cracks that were examined were found to be slightly longer than expected but still well within the flaw size criteria used to evaluate tank structural integrity.
Book Chapter
Analysis of a Corrosion Failure of an Aboveground Storage Tank
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c0091208
EISBN: 978-1-62708-220-4
... Examination The underside of the floor plates showed extensive localized wall thinning. Figure 1 shows a pit in one of the tank floor plates. While it was expected that the ground under the tank was near operational temperatures, it was determined that the temperatures were below 104 °C (220 °F...
Abstract
A failure of an aboveground storage tank occurred due to external corrosion of the tank floor. The liquid asphalt tank operated at elevated temperatures (approximately 177 deg C, or 350 deg F) and had been in service for six years. Cathodic protection (rectifiers) had been installed since start-up of the tank operation. It was noted, however, that some operational problems with the rectifier may have interrupted its protection. Investigation (visual inspection, on-site examination and testing, EDS analysis of scale deposits, and MIC testing of the soil) supported the conclusion that corrosion may have been caused by an interruption in cathodic protection. The effectiveness of cathodic protection on established microbial deposits is questionable. Recommendations included ultrasonically testing the tank floor and replacing portions based on the remaining wall thickness. Doubling the wall thickness of the floor plates was also recommended.
Image
Published: 01 January 2002
Fig. 8 Thin-lip rupture in a 64-mm (2 1 2 -in.) outside-diameter × 2.7-mm (0.105-in.) wall thickness carbon steel furnace-wall tube that was caused by rapid overheating. Knife-edge wall thinning at longitudinal main rupture is shown in cross section in the inset. Note secondary
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Book Chapter
Premature Failure of a Type 309 Stainless Steel Pan for a Lead Bath
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c0046915
EISBN: 978-1-62708-232-7
..., and etched micrographs using Murakami's reagent) supported the conclusions that thinning of the pan walls at the surface of the molten lead resulted from using coke of high moisture content and from the low fluctuating coke level. Recommendations included reducing the supply of oxygen attacking the grain...
Abstract
Severely reduced wall thickness was encountered at the liquid line of a lead-bath pan that was used in a continuous strip or wire oil-tempering unit. Replacement of the pan was necessary after six months of service. The pan, 6.9 m (22.5 ft) long, 0.6 m (2 ft) wide, and 38 cm (15 in.) deep with a 2.5-cm (1-in.) wall thickness, was a type 309 stainless steel weldment. Operating temperatures of the lead bath in the pan ranged from 805 deg C (1480 deg F) at the entry end to 845 deg C (1550 deg F) at the exit end. Analysis (visual inspection. metallographic analysis, moisture testing, and etched micrographs using Murakami's reagent) supported the conclusions that thinning of the pan walls at the surface of the molten lead resulted from using coke of high moisture content and from the low fluctuating coke level. Recommendations included reducing the supply of oxygen attacking the grain boundaries and the hydrogen that readily promoted decarburization with the use of dry (2 to 3% moisture content) coke. Maintaining a thick layer of coke over the entire surface of molten lead in the pan would exclude atmospheric oxygen from the grain boundaries.
Image
Stainless steel pan (top) for a molten-lead bath that failed as a result of...
Available to Purchase
in Premature Failure of a Type 309 Stainless Steel Pan for a Lead Bath
> ASM Failure Analysis Case Histories: Steelmaking and Thermal Processing Equipment
Published: 01 June 2019
Fig. 1 Stainless steel pan (top) for a molten-lead bath that failed as a result of wall thinning (shaded area) caused by oxidation and decarburization. Overall view of pan and section taken through a second pan (Section A-A) showing the relation of the thinned region to coke level. Dimensions
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Image
Composite photomicrograph showing microstructure of the conical section fro...
Available to Purchase
in Metallurgical Evaluation of a Five Inch Cylindrical Induction Melter
> ASM Failure Analysis Case Histories: Steelmaking and Thermal Processing Equipment
Published: 01 June 2019
Fig. 7 Composite photomicrograph showing microstructure of the conical section from the CIM. Note significant grain growth and the lack of voids throughout the cross section. Molten glass attack is visible on ID surface, but no wall thinning occurred.
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