Metal-framed polycarbonate (PC) ophthalmic lenses shattered from acetone solvent-induced cracking. The lenses exhibited primary and secondary cracks with solvent swelling and crazing. A laboratory accident splashed acetone onto the lenses. The metal frames gripped approximately two-thirds of the lenses' periphery and introduced an unevenly distributed force on the lenses. To prevent future failures, it was recommended to protect PC from service environments with solvents, such as acetone; or from marking pens, adhesives or soaps which contain undesirable solvents; and to not apply excessive stress on ophthalmic lenses in the form of working or residual stresses.

A failure analysis was conducted on a flow-sensing device that had cracked while in service. The polysulfone sensor body cracked radially, adjacent to a molded-in steel insert. This article describes the investigative methods used to conduct the failure analysis. The techniques utilized included scanning electron microscopy, Fourier transform infrared spectroscopy, differential scanning calorimetry, thermomechanical analysis, and melt flow rate determination. It was the conclusion of the investigation that the part failed via brittle fracture, with evidence also indicating low cycle fatigue associated with cyclic temperature changes from normal service. The design of the part and the material selection were significant contributing factors because of stresses induced during molding, physical aging of the amorphous polysulfone resin, and the substantial differential in coefficients of thermal expansion between the polysulfone and the mating steel insert.

A weld in a fuel-line tube broke after 159 h of engine testing. The 6.4-mm (0.25-in.) OD x 0.7-mm (0.028-in.) wall thickness tube and the end adapters were all of type 347 stainless steel. The butt joints between tube and end adapters were made by automated gas tungsten arc (orbital arc) welding. It was found that the tube had failed in the HAZ. Examination of a plastic replica of the fracture surface in a transmission electron microscope established that the crack origin was at the outer surface of the tube. The crack growth was by fatigue; closely spaced fatigue striations were found near the origin, and more widely spaced striations near the inner surface. The quality of the weld and the chemical composition of the tube both conformed to the specifications. However, the fuel-line assembly had vibrated excessively in service. The fuel-line fracture was caused by fatigue induced by severe vibration in service. Additional tube clamps were provided to damp the critical vibrational stresses. No further fuel-line fractures were encountered.

Type 347 stainless steel moderator circuit branch piping in a pressurized hot water reactor was experiencing frequent leakage. Investigation of the problem involved failure analysis of leaking pipe specimens, analytical stress analysis, and determination of “leak-before-break” conditions using fracture mechanics and thermal fatigue simulation tests. Failure analysis indicated that cracking had been initiated by thermal fatigue. Data from the analysis were used in making the leak-before-break predictions. It was determined that the cracks could grow to two-thirds of the circumferential length of the pipe without catastrophic failure. A thin stainless steel sleeve was inserted in the branch pipe to resolve the problem.

Superelastic nitinol wires that fractured under various conditions were examined under a scanning electron microscope in order to characterize the fracture surfaces, produce reference data, and compare the findings with prior published work. The study revealed that nitinol fracture modes and morphologies are generally consistent with those of ductile metals, such as austenitic stainless steel, with one exception: Nitinol exhibits a unique damage mechanism under high bending strain, where damage occurs at the compression side of tight bends or kinks while the tensile side is unaffected. The damage begins as slip line formation due to plastic deformation, which progresses to cracking at high strain levels. The cracks appear to initiate from slip lines and extend in shear (mode II) manner.

This article reviews the mechanical behavior and fracture characteristics that discriminate structural polymers from metals. It provides information on deformation, fracture, and crack propagation as well as the fractography involving the examination and interpretation of fracture surfaces, to determine the cause of failure. The fracture modes such as ductile fractures and brittle fractures are reviewed. The article also presents a detailed account of various fracture surface features. It concludes with several cases of field failure in various polymers that illustrate the applicability of available analytical tools in conjunction with an understanding of failure mechanisms.

This article reviews analytical techniques that are most often used in plastic component failure analysis. The description of the techniques is intended to familiarize the reader with the general principles and benefits of the methodologies, namely Fourier transform infrared spectroscopy, energy-dispersive x-ray spectroscopy, differential scanning calorimetry, thermogravimetric analysis, and dynamic mechanical analysis. The article describes the methods for molecular weight assessment and mechanical testing to evaluate plastics and polymers. The descriptions of the analytical techniques are supplemented by a series of case studies to illustrate the significance of each method. The case studies also include pertinent visual examination results and the corresponding images that aided in the characterization of the failures.

With any polymeric material, chemical exposure may have one or more different effects. Some chemicals act as plasticizers, changing the polymer from one that is hard, stiff, and brittle to one which is softer, more flexible, and sometimes tougher. Often these chemicals can dissolve the polymer if they are present in large enough quantity and if the polymer is not crosslinked. Other chemicals can induce environmental stress cracking (ESC), an effect in which brittle fracture of a polymer will occur at a level of stress well below that required to cause failure in the absence of the ESC reagent. Finally, there are some chemicals that cause actual degradation of the polymer, breaking the macromolecular chains, reducing molecular weight, and diminishing polymer properties as a result. This article examines each of these effects. The discussion also covers the effects of surface embrittlement and temperature on polymer performance.

Important clues about the probable cause of a gun tube explosion were obtained from a fractographic and metallographic examination of the fragments. The size, distribution, and surface markings of fragments may be used to localize the explosion and deduce its intensity. Microstructural features such as voids, adiabatic shear, and structural surface alterations also indicate the explosion intensity and further allow a comparison of the tube structure near and away from the explosion zone. These, and other metallurgical characteristics, are illustrated and discussed for cases of accidental and deliberately caused explosions of large caliber gun tubes.

A forging die in a 250-ton press producing brass valves began to show signs of fatigue after a few thousand hits. By the time it reached 30,000 hits, the die was badly damaged and was submitted for analysis along with one of the last forgings produced. The investigation included visual and macroscopic inspection, metallographic and chemical analysis, SEM imaging, optical profilometry, mechanical property testing, and EDX analysis. The die was made of chromium hot-work tool steel and the forgings were made of CuZn39Pb3 heated to an initial working temperature 700 deg C. The entire surface of the die was covered with fatigue cracks and many fillets had been plastically deformed. Several other types of damage were also observed, including areas of oxidation, corrosion pits, voids, abrasive wear, die adhesion, and thermal fatigue. Fatigue cracking was the primary cause of failure with significant contributions from the other damage mechanisms.

While there are many fracture mechanisms that can lead to the failure of a plastic component, environmental stress cracking (ESC) is recognized as one of the leading causes of plastic failure. This article focuses on unpacking the basic concepts of ESC to provide the engineer with a better understanding of how to evaluate and prevent it. It then presents factors that affect and contribute to the susceptibility of plastic to ESC: material factors, chemical factors, stress, and environmental factors. The article includes the collection of background information to understand the circumstances surrounding the failure, a fractographic evaluation to assess the cracking, and analytical testing to evaluate the material, design, manufacturing, and environmental factors.

The first part of this article focuses on two major forms of machining-related failures, namely machining workpiece (in-process) failures and machined part (in-service) failures. Discussion centers on machining conditions and metallurgical factors contributing to (in-process) workpiece failures, and undesired surface layers and metallurgical factors contributing to (in-service) machined part failures. The second part of the article discusses the effects of microstructure on machining failures and their preventive measures.

A deformed steel tube was received for failure analysis after buckling during a heat-treat operation. The tube was subjected to various metallurgical tests as well as nondestructive testing to confirm the presence of residual stresses. The microstructure of the tube was found to be homogenous and had no banded structure. However, x-ray diffraction analysis confirmed the presence of up to 6% retained austenite which likely caused the tube to buckle during the 910 °C heat treating procedure.

Persistent cracking in a forged 1080 steel turntable rail in a wind tunnel test section was investigated. All cracks were oriented transverse to the axis of the rail, and some had propagated through the flange into the web. Through-flange cracks had been repair welded. A section of the flange containing one through-flange crack was examined using various methods. Results indicated that the cracks had initiated from intergranular quench cracks caused by the use of water as the quenching medium. Brittle propagation of the cracks was promoted by high residual stresses acting in conjunction with applied loads. Repair welding was discontinued to prevent the introduction of additional residual stress., Finite-element analysis was used to show that the rail could tolerate existing cracks. Periodic inspection to monitor the degree of cracking was recommended.

The article commences with an overview of short-term and long-term mechanical properties of polymeric materials. It discusses plasticization, solvation, and swelling in rubber products. The article further describes environmental stress cracking and degradation of polymers. It illustrates how surface degradation of a plain strain tension specimen alters the ductile brittle transition in polyethylene creep rupture. The article concludes with information on the effects of temperature on polymer performance.

Distortion often is observed in the analysis of other types of failures, and consideration of the distortion can be an important part of the analysis. This article first considers that true distortion occurs when it was unexpected and in which the distortion is associated with a functional failure. Then, a more general consideration of distortion in failure analysis is introduced. Several common aspects of failure by distortion are discussed and suitable examples of distortion failures are presented for illustration. The article provides information on methods to compute load limits, errors in the specification of the material, and faulty process and their corrective measures to meet specifications. It discusses the general process of material failure analysis and special types of distortion and deformation failure.

Distortion failure occurs when a structure or component is deformed so that it can no longer support the load it was intended to carry. Every structure has a load limit beyond which it is considered unsafe or unreliable. Estimation of load limits is an important aspect of design and is commonly computed by classical design or limit analysis. This article discusses the common aspects of failure by distortion with suitable examples. Analysis of a distortion failure often must be thorough and rigorous to determine the root cause of failure and to specify proper corrective action. The article summarizes the general process of distortion failure analysis. It also discusses three types of distortion failures that provide useful insights into the problems of analyzing unusual mechanisms of distortion. These include elastic distortion, ratcheting, and inelastic cyclic buckling.

This article describes the underlying fundamentals, applications, the relevance and necessity of performing proper stress analysis in conducting a failure analysis. It presents an introduction to the stress analysis of bodies containing crack-like imperfections and the topic of fracture mechanics. The fracture mechanics approach is an important part of stress analysis at the tips of sharp cracks or discontinuities. The article reviews fracture mechanics concepts, including linear elastic fracture mechanics, elastic-plastic fracture mechanics, and subcritical fracture mechanics. It also provides information on the applications of fracture mechanics in failure analysis.