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Cássio Barbosa, Jôneo Lopes do Nascimento, José Luiz Fernandes, Ibrahim de Cerqueira Abud
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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.rail.c9001531
EISBN: 978-1-62708-231-0
..., and ductility are mainly determined by the carbon content of wheel steels. The fatigue crack growth resistance is insensitive to composition and microstructure, while the fatigue crack initiation life increases with the decrease of austenite grain size and pearlite colony size. The dynamic fracture toughness...
Abstract
In this study, the failure modes of cartwheel and mechanical properties of materials have been analyzed. The results show that rim cracking is always initiated from stringer-type alumina cluster and driven by a combination effect of mechanical and thermal load. The strength, toughness, and ductility are mainly determined by the carbon content of wheel steels. The fatigue crack growth resistance is insensitive to composition and microstructure, while the fatigue crack initiation life increases with the decrease of austenite grain size and pearlite colony size. The dynamic fracture toughness, KID, is obviously lower than static fracture toughness, KIC, and has the same trend as KIC. The ratio of KID/sigma YD is the most reasonable parameter to evaluate the fracture resistance of wheel steels with different composition and yield strength. Decreasing carbon content is beneficial to the performance of cartwheel.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001776
EISBN: 978-1-62708-241-9
... surface showing cleavage of brittle fracture Fig. 3 SEM micrograph of fractured surface showing precipitation of carbides in the austenite matrix and the formation of microcracks Fig. 4 Optical micrograph of failed crusher jaw showing large carbide deposits at grain boundaries...
Abstract
In this article, we report the outcome of an investigation made to uncover the premature fracture of crusher jaws produced in a local foundry. A crusher jaw that had failed while in service was studied through metallographic techniques to determine the cause of the failure. Our investigation revealed that the reason for the fracture was the presence of large carbides at the grain boundaries and in the grain matrix. This led to the formation of microcracks that propagated along the grain boundaries under in-service working forces. It is also believed that the precipitation of carbides at the grain boundaries may have occurred because of improper heat treatment, but not because of a deficiency in composition.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001780
EISBN: 978-1-62708-241-9
... 51.5 Fracture toughness data, Ref. [<xref rid="c9001780-ref23" ref-type="bibr">23</xref>] Table 6 Fracture toughness data, Ref. [ 23 ] Added element content (wt.%) Tempering temperature ( o C) K IC (ksi-√inch) (multiple samples) 0 100 91, 83 200 129, 126 400 140...
Abstract
A number of failures involving carbon and alloy steels were analyzed to assess the effects of inclusions and their influence on mechanical properties. Inclusions, including brittle oxides and more ductile manganese sulfides (MnS), affect fatigue endurance limit, fatigue crack propagation rates, fracture toughness, notch toughness, and transverse tensile properties, and do so in an anisotropic manner with respect to rolling direction. Significant property anisotropy has been documented in the failures investigated, providing evidence that designers failed to account for it. Typical fracture morphologies observed in such cases and metallographic appearances of MnS-containing materials are illustrated.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c0045903
EISBN: 978-1-62708-223-5
... for the replacement unit to lessen the possibility of such gross inclusion segregation and to improve the fracture toughness of the cylinder. Casing (material) Extruders Nonmetallic inclusions Xray analysis ASTM A235-55 Corrosion fatigue The energy-dispersive x-ray analyzer, in conjunction...
Abstract
A 230 mm (9 in.) thick casing, fabricated from ASTM 235-55 low-carbon steel, of a 450 Mg (500 ton) extrusion press failed after 27 years of service. Initial visual examination revealed an area that exhibited multiple origins and classic beach marks radiating out approximately 75 mm (3 in.) from the origin along the wall of a hydraulic-oil bleed hole. Investigation with a SEM showed corrosion pits along the bleed hole wall, but oxidation and corrosion prevented review of microfractographic details. Vacuum epoxy encapsulation, sectioning of the bleed hole, and metallographic examination revealed a basic microstructure of pearlite and ferrite with bands of slightly finer pearlite, with a large concentration of inclusion stringers in the area of the fracture origin. Further investigation using an energy-dispersive x-ray analyzer showed high concentrations of sulfur and manganese. Thus, the failure appeared to have resulted from corrosion-assisted fatigue, and the inclusion concentration in the fracture-initiated area indicated that the chemical-composition limits for sulfur and manganese would have greatly exceeded material specifications. A higher quality steel was recommended for the replacement unit to lessen the possibility of such gross inclusion segregation and to improve the fracture toughness of the cylinder.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003572
EISBN: 978-1-62708-180-1
..., aspect ratio, distribution, orientation, combination with fillers, and the quality of bonding with the matrix), and operating conditions. Fibers are far more wear resistant than the matrix and hence control the wear of composite. Continuous fiber-reinforced composites with a thermoset-polymer matrix...
Abstract
This article reviews the abrasive and adhesive wear failure of several types of reinforced polymers, including particulate-reinforced polymers, short-fiber reinforced polymers (SFRP), continuous unidirectional fiber reinforced polymers (FRP), particulate-filled composites, mixed composites (SFRP and particulate-filled), unidirectional FRP composites, and fabric reinforced composites. Friction and wear performance of the composites, correlation of performance with various materials properties, and studies on wear-of failure mechanisms by scanning electron microscopy are discussed for each of these types.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001055
EISBN: 978-1-62708-214-3
... fractographic, metallographic, chemical, and mechanical property (tension and impact toughness) analyses were conducted. On the basis of the tests and observations, it was concluded that the failure was the combined result of poor notch toughness (impact) properties of the steel, high stresses in the joint area...
Abstract
The repeated failure of a welded ASTM A283 grade D pipe that was part of a 6 km (4 mi) line drawing and conducting river water to a water treatment plant was investigated. Failure analysis was conducted on sections of pipe from the third failure. Visual, macrofractographic, SEM fractographic, metallographic, chemical, and mechanical property (tension and impact toughness) analyses were conducted. On the basis of the tests and observations, it was concluded that the failure was the combined result of poor notch toughness (impact) properties of the steel, high stresses in the joint area, a possible stress raiser at the intersection of the spiral weld and girth weld, and sudden impact loading, probably due to water hammer. Use of a semi- or fully killed steel with a minimum Charpy V-notch impact value of 20 J (15 ft·lbf) at 0 deg C (32 deg F) was recommended for future water lines. Certified test results from the steel mill, procedure qualification tests of the welding, and design changes to reduce water hammer were also recommended.
Book Chapter
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001819
EISBN: 978-1-62708-241-9
.... 9 Fracture surface (cleavage). Arrows: holes with inclusion particles Fig. 10 Same aspect as in Fig. 9 with more detail Fig. 11 EDS spectrum: particles Fig. 12 EDS spectrum: matrix Fig. 1 ( a ) Fractured centrifugal pump axis. ( b ) Fracture surface...
Abstract
The shafts on two centrifugal pumps failed during use in a petroleum refinery. Light optical microscopy and scanning electron microscopy were used to analyze the damaged materials to determine the cause of failure. The results showed that one shaft, made of duplex stainless steel, failed by fatigue fracture, and the other, made of 316 austenitic stainless steel, experienced a similar fracture, which was promoted by the presence of nonmetallic inclusion particles.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001787
EISBN: 978-1-62708-241-9
... drilling bit. Huang et al. [ 14 ] have found that the microstructure of the advanced drilling bit is composed of tempered martensite, tempered martensite with bainite and bainite as the carburized layer, the transitive layer, and the matrix. High-strength carburized layer and high-toughness matrix can...
Abstract
A masonry type drill bit, designed for impact drilling in rock, fractured after a short time in service. Samples of the failed bit were analyzed using optical and scanning electron microscopy, quantitative metallography, and chemical analysis. The composition was found to be that of 18CrNi3Mo steel. Investigators also found evidence of inclusions and prior austenite grain size, although it was determined that neither played a role in the failure. Rather, according to test data, the failure occurred because of stress concentration (due to geometric discontinuities along the tooth profiles) and the cumulative effect of torque and force loading (the byproduct of continuous twisting and axial impact). Cracks readily initiate under these conditions then propagate quickly through what was found to be networks of tempered martensite, thus resulting in premature failure.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001534
EISBN: 978-1-62708-220-4
... root (lack of penetration). Component failure had started from this weld defect. The hydrogen absorbed during welding facilitated crack initiation from this weld defect during storage of the component after welding. Poor weld toughness at the low operating temperature facilitated crack growth during...
Abstract
A detailed failure analysis was conducted on an ammonia refrigerant condenser tube component that failed catastrophically during its initial hours of operation. Evidence collected clearly demonstrated that the weld between a pipe and a dished end contained a sharp unfused region at its root (lack of penetration). Component failure had started from this weld defect. The hydrogen absorbed during welding facilitated crack initiation from this weld defect during storage of the component after welding. Poor weld toughness at the low operating temperature facilitated crack growth during startup, culminating in catastrophic failure as soon as the crack exceeded critical length.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001784
EISBN: 978-1-62708-241-9
... constituents Fig. 11 X-ray map of the region shown in Fig. 9 indicating concentration of oxygen in Fe rich part of the matrix Fig. 12 EDS spectrum of a high quality 13/16 in. wrench socket showing alloying elements such as Ni and Cr that were not present in the failed socket Fig...
Abstract
A 13/16-in. hex socket failed while in use. Analysis (hardness testing, optical and scanning electron microscopy, and EDS) revealed that the socket was made of low carbon steel formed in a powder metallurgy process. A number of flaws were found including nonuniform wall thickness, poor geometric design with sharp corners as stress raisers, and incomplete sintering evidenced by unsintered particles. These were determined to be the primary cause of failure, although inclusions on the fracture surface containing S and Al may have played a role as well.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c9001544
EISBN: 978-1-62708-219-8
... the material met chemical and mechanical property requirements, tests showed it had low fracture toughness and critical-sized flaws oriented normal to the principal stress in the failed junction piece. Fabrication procedures resulted in high residual stresses and a metallurgical notch at the radius...
Abstract
A large crack developed at a girder-truss joint area of the Fremont bridge in Portland, OR, on 28 Oct 1971. It occurred during a positioning procedure involving a junction piece welded to a girder, starting as a brittle fracture and terminating in plastic hinges in the girder web welds. The arch rib top plate, as it met the main girder, formed a composite beam of A588/A36 composition. Investigation showed the original design of the failed component called for an angle of high geometric stress concentration (90 deg with no radius) in a region of substantial transverse weld joints. While the material met chemical and mechanical property requirements, tests showed it had low fracture toughness and critical-sized flaws oriented normal to the principal stress in the failed junction piece. Fabrication procedures resulted in high residual stresses and a metallurgical notch at the radius in the junction piece. Stresses induced during jacking (the procedure used to raise bridge components into position) applied the stresses in the critical radius that triggered the cracking.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001031
EISBN: 978-1-62708-214-3
.... 85×. Microprobe Analysis Microprobe analysis was used to determine the morphology and composition of the matrix and phases. Typical microstructure of NARloy-Z was observed away from the banded region ( Fig. 3 ). The second-phase intermetallic located at the grain boundaries had...
Abstract
Pinhole defects were found in a main combustion chamber made from NARloy-Z after an unexpectedly short time in service. Analysis indicated that the throat section of the liner had been exposed to very severe environmental conditions of high temperature and high oxygen content, which caused ductility loss and grain-boundary separation. The excessive oxygen content in the liner was attributed to diffusion from an oxygen-rich environment that had resulted from nonuniform mixing of propellants. The internal oxygen embrittled the alloy and reduced its thermal conductivity, which resulted in a higher hot-gas wall temperature and associated degradation of mechanical properties.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003543
EISBN: 978-1-62708-180-1
..., ductility, and toughness of metallic materials. These factors must also be considered in the evaluation and prevention of overload failures. Therefore, throughout this article, the term overload failure is intended to imply fracture due to stresses exceeding the capacity of the material, whether...
Abstract
Overload failures refer to the ductile or brittle fracture of a material when stresses exceed the load-bearing capacity of a material. This article reviews some mechanistic aspects of ductile and brittle crack propagation, including a discussion on mixed-mode cracking, which may also occur when an overload failure is caused by a combination of ductile and brittle cracking mechanisms. It describes the general aspects of fracture modes and mechanisms. The article discusses some of the material, mechanical, and environmental factors that may be involved in determining the root cause of an overload failure. It also presents examples of thermally and environmentally induced embrittlement effects that can alter the overload fracture behavior of metals.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006778
EISBN: 978-1-62708-295-2
... characteristics can act singly or combine synergistically to reduce the strength, ductility, and toughness of metallic materials. These factors must also be considered in the evaluation and prevention of overload failures. Therefore, throughout this article, the term overload failure implies fracture due...
Abstract
This article aims to identify and illustrate the types of overload failures, which are categorized as failures due to insufficient material strength and underdesign, failures due to stress concentration and material defects, and failures due to material alteration. It describes the general aspects of fracture modes and mechanisms. The article briefly reviews some mechanistic aspects of ductile and brittle crack propagation, including discussion on mixed-mode cracking. Factors associated with overload failures are discussed, and, where appropriate, preventive steps for reducing the likelihood of overload fractures are included. The article focuses primarily on the contribution of embrittlement to overload failure. The embrittling phenomena are described and differentiated by their causes, effects, and remedial methods, so that failure characteristics can be directly compared during practical failure investigation. The article describes the effects of mechanical loading on a part in service and provides information on laboratory fracture examination.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001845
EISBN: 978-1-62708-241-9
... the compositions of the flakes; the results determined that the flakes primarily consisted of Cu (~99.1%) and O (0.8–1.0%) elements. It was deduced that the flakes in the fracture were free from Si and Ni elements, which are the basic elements of the matrix material. According to the aforementioned analysis...
Abstract
Two clamps that support overhead power lines in an electrified rail system fractured within six months of being installed. The clamps are made of CuNiSi alloy, a type of precipitation-strengthening nickel-silicon bronze. To identify the root cause of failure, the rail operator led an investigation that included fractographic and microstructural analysis, hardness testing, inductively coupled plasma spectroscopy, and finite-element analysis. The fracture was shown to be brittle in nature and covered with oxide flakes, but no other flaws relevant to the failure were observed. The investigation results suggest that the root cause of failure was a forging lap that occurred during manufacturing. Precracks induced by the forging defect and the influence of preload stress (due to bolt torque) caused the premature failure.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001535
EISBN: 978-1-62708-232-7
... carbide ( Ref 5 ), second-intermediate roll steel composition is leaner in carbon content for enhanced toughness. It has been reported ( Ref 6 ) that toughness for intermediate rolls is more important than wear resistance because the driven second-intermediate rolls have to withstand substantial shear...
Abstract
Although a precise understanding of roll failure genesis is complex, the microstructure of a broken roll can often unravel intrinsic deficiencies in material quality responsible for its failure. This is especially relevant in circumstances when, even under a similar mill-operating environment, the failure involves a particular roll or a specific batch of rolls. This paper provides a microstructural insight into the cause of premature breakage of a second-intermediate Sendzimir mill drive roll used at a stainless steel sheet rolling plant under the Steel Authority of India Limited. Microstructural issues influencing roll quality, such as characteristics of carbides, tempered martensite, retained austenite, etc., have been extensively studied through optical and scanning electron microscopy, electron-probe microanalysis, image analysis, and x-ray diffractometry. These are discussed to elucidate specific microstructural inadequacies that accentuated the failure. The study reveals that even through retained austenite content is low (6.29 vol%) and martensite is non-acicular, the roll breakage is a consequence of intergranular cracking caused by improper carbide morphology and distribution.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001768
EISBN: 978-1-62708-241-9
... plate Heel (Corner) 478 581 27.04 Edge 428 562 28.61 Specified (ASTM A572 Grade 50) 340 min. 450 min. 17 min Charpy impact toughness of the cracked splice plate Table 4 Charpy impact toughness of the cracked splice plate Sample type Location Sample size (mm) Test...
Abstract
A steel splice plate in a power transmission line tower cracked while in service. Metallographic analysis indicated the presence of a white hard martensite layer near the crack, which occurred in the heel of the plate. Mechanical property tests revealed localized hardening in the area of the crack, supporting the metallurgical findings. A substantial deterioration of the Charpy impact toughness of the material in the heel region was also observed which is believed to have caused the initiation and propagation of the cracks leading to the failure.
Book Chapter
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006790
EISBN: 978-1-62708-295-2
... ksi) structure coexists in a relatively soft ferrite or pearlite (HV of approximately 1.0 to 2.9 GPa, or 145 to 420 ksi) matrix. This results in a composite HV for the alloy of between 4.9 and 5.9 GPa (710 and 855 ksi). However, in spite of the relatively high hardness of the composite structure...
Abstract
Engineered components fail predominantly in four major ways: fracture, corrosion, wear, and undesirable deformation (i.e., distortion). Typical fracture mechanisms feature rapid crack growth by ductile or brittle cracking; more progressive (subcritical) forms involve crack growth by fatigue, creep, or environmentally-assisted cracking. Corrosion and wear are another form of progressive material alteration or removal that can lead to failure or obsolescence. This article primarily covers the topic of abrasive wear failures, covering the general classification of wear. It also discusses methods that may apply to any form of wear mechanism, because it is important to identify all mechanisms or combinations of wear mechanisms during failure analysis. The article concludes by presenting several examples of abrasive wear.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.matlhand.c0089676
EISBN: 978-1-62708-224-2
... wear resistance by forming chromium carbides. Examination with a hand magnet indicated that the entire link was magnetically responsive. When properly heat treated, austenitic manganese steel is a tough, nonmagnetic alloy; however, composition changes that occur at the surface during heating may...
Abstract
Chain link, a part of a mechanism for transferring hot or cold steel blooms into and out of a reheating furnace, broke after approximately four months of service. The link was cast from 2% Cr austenitic manganese steel and was subjected to repeated heating to temperatures of 455 to 595 deg C (850 to 1100 deg F). Examination included visual inspection, macrograph of a nital-etched specimen from an as-received chain link 1.85x, micrographs of a nital-etched specimen from an as-received chain link 100x/600x, normal microstructure of as-cast standard austenitic manganese steel 100x, micrograph of a nital-etched specimen that had been austenitized 20 min at 1095 deg C (2000 deg F) and air cooled 315x, and micrograph of the same specimen after annealing 68 h at 480 deg C (900 deg F) 1000x). Investigation supported the conclusions that the chain link failed in a brittle manner, because the austenitic manganese steel from which it was cast became embrittled after being reheated in the temperature range of 455 to 595 deg C (850 to 1100 deg F) for prolonged periods of time. The alloy was not suitable for this application, because of its metallurgical instability under service conditions.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003560
EISBN: 978-1-62708-180-1
... to 1420 ksi) structure coexists in a relatively soft ferrite or pearlite (HV of approximately 1.0 to 2.9 GPa, or 145 to 420 ksi) matrix. This results in a composite HV for the alloy of between 4.9 and 5.9 GPa (710 and 855 ksi). However, in spite of the relatively high hardness of the composite structure...
Abstract
Wear, a form of surface deterioration, is a factor in a majority of component failures. This article is primarily concerned with abrasive wear mechanisms such as plastic deformation, cutting, and fragmentation which, at their core, stem from a difference in hardness between contacting surfaces. Adhesive wear, the type of wear that occurs between two mutually soluble materials, is also discussed, as is erosive wear, liquid impingement, and cavitation wear. The article also presents a procedure for failure analysis and provides a number of detailed examples, including jaw-type rock crusher wear, electronic circuit board drill wear, grinding plate wear failure analysis, impact wear of disk cutters, and identification of abrasive wear modes in martensitic steels.