An AISI D2 tool steel insert from a forming die used in the manufacture of automotive components failed prematurely during production. Results of various analyses and simulation tests indicated fatigue failure resulting from improper heat treatment. The fatigue fracture originated because of a highly stressed condition produced by a sharp corner combined with low toughness from ineffective tempering. It was recommended that 25 other inserts that belonged to the same die be double tempered.

Several surgical tool failures were analyzed to understand why they occur and how to prevent them. The study included drills, catheters, and needles subjected to the rigors of biomedical applications such as corrosive environments, high stresses, sterilization, and improper cleaning procedures. Given the extreme conditions to which surgical tools can be exposed, and the potential for misuse, failures are inevitable and systematic methods for analyzing them are necessary to keep them in check.

The A2 tool steel mandrel, part of a rolling tool used for mechanically joining two tubes was fractured after making five rolled joints. A 6.4 mm diam hole was drilled by EDM through the square end of the hardened mandrel due to difficulty was experienced in withdrawing the tool. The fracture progressed into the threaded section and formed a pyramid-shape fragment after it was initiated at approximately 45 deg through the hole in the square end. An irregular zone of untempered martensite with cracks radiating from the surface of the hole (result of melting around hole) was revealed by metallographic examination. A microstructure of fine tempered martensite containing some carbide particles was exhibited by the core material away from the hole. Brittle fracture characteristics with beach marks were exhibited by the fracture surfaces which is characteristic of a torsional fatigue fracture. As a corrective measure, the hole through the square end of the mandrel was incorporated into the design of the tool and was drilled and reamed before heat treatment and specified hardness of the threaded portion and square end of the mandrel was reduced.

A broken cross-recessed die was examined. Examination of the unetched, polished section for impurities revealed several coarse streaks of slag. The purity did not therefore correspond to the requirements set for a high speed tool steel of the given theoretical quality DMo 5. After etching with 5% nital the polished surface exhibited a pronounced, easily-visible, fibrous structure. Microscopic examination revealed that this etch pattern was produced by marked segregation bands. The very unfavorable structure for a high speed steel tool of these dimensions and subject to such stresses together with the low purity favored the fracture of the tool.

Two A6 tool steel (free machining grade) shafts, parts of a clamping device used for bending 5.7 cm OD tubing on an 8.6 cm radius, failed simultaneously under a maximum clamping force of 54,430 kg. The shaft was imposed with cyclic tensile stresses due to the clamping force and unidirectional bending stresses resulting from the nature of operation. Nonmetallic oxide-sulfide segregation was indicated by microscopic examination of the edge of the fracture surface. Both smooth and granular areas were revealed on visual examination of the fracture. The shaft was subjected to a low overstress as the smooth-textured fatigue zone was relatively large compared with the crystalline textured coarse final-fracture zone. The fatigue crack was nucleated by the nonmetallic inclusion that intersected the surface and initiated in the 0.25 mm radius fillet at a change in section due to stress concentration. To minimize this stress concentration, a larger radius fillet shaft at the critical change in section was suggested as corrective measure.

During natural gas drilling in the EMS region in 1956, considerable numbers of longitudinal cracks and transverse fractures occurred in the connecting pieces of the bore rods. The connectors were screwed onto the rods by means of a fine thread and tightly joined with it by shrinkage at 530 deg C. The connectors were made of SAE 4140 Cr-Mo steel. The material for the rod pipes was Fe-0.4C-1Mn steel. Structural stresses played a role in the cracking. Iron sulfide formed on the fracture planes and flake-like stress cracks occurred in the steel. The hydrogen sulfide content of the gas was the cause of damage. Hydrogen liberated by reaction with the iron caused the formation of iron sulfide after penetration of the steel, which had an explosive effect during molecular separation under high pressure. This in turn caused the crack formation in conjunction with the external and residual stresses.

A failed H-11 tool steel pylon attachment stud was found during a routine walk-around inspection. The stud exhibited gross localized corrosion pitting at several different areas on its surface. Light general rust was also evident. Severe pitting occurred near the fracture location. The fracture face contained evidence of intergranular SCC as well as ductile dimples. The protective coating was found to be an inorganic water-base aluminide coating having a coating thickness of 7.5 to 13 micron (0.3 to 0.5 mil). The coating was of a nonuniform mottled nature. It was concluded that the failure of the pylon attachment stud was caused by general corrosion followed by SCC. The stud was not adequately protected against corrosion by the coating. It was recommended that the coating be applied to a thickness of 38 to 75 micron (1.5 to 3 mil) to provide long-time corrosion resistance. The coating must be either burnished or cured at 540 deg C (1000 deg F) to provide cathodic protection to the steel. Other coatings, such as cadmium or aluminum, were also recommended if a thinner coating is needed.

The safety valve on a steam turbogenerator was set to open when the steam pressure reaches 2400 kPa (348 psi). The pressure had not exceeded 1790 kPa (260 psi) when the safety-valve spring shattered into 12 pieces. The steam temperature in the line varied from about 330 to 400 deg C (625 to 750 deg F). Because the spring was enclosed and mounted above the valve, its temperature was probably slightly lower. The 195 mm (7 in.) OD x 305 mm (12 in.) long spring was made from a 35 mm (1 in.) diam rod of H21 hot-work tool steel. It had been in service for about four years and had been subjected to mildly fluctuating stresses. Analysis (visual inspection, 0.3x photographs, 0.7x light fractographs, and metallographic examination) supported the conclusions that the spring failed by corrosion fatigue that resulted from application of a fluctuating load in the presence of a moisture-laden atmosphere. Recommendations included replacing all safety valves in the system with new open-top valves that had shot-peened and galvanized steel springs. Alternatively, the valve springs could be made from a corrosion-resistant metal-for example, a 300 series austenitic stainless steel or a nickel-base alloy, such as Hastelloy B or C.

A copper alloy C51000 (phosphor bronze, 5%A) failed prematurely during life testing of several such springs. The wire used for the springs was 0.46 mm (0.018 in.) in diam and was in the spring-temper condition. The springs were revealed to be subjected to cyclic loading, in the horizontal and vertical planes during the testing. The fracture was revealed to have occurred in bend 2. An indentation, presumably caused by the bending tool during forming, at the inner surface of the bend where fracture occurred was revealed by microscopic examination. Spiral marks produced on springs during rotary straightening were observed. A crack that had originated at the surface at the inside bend and had propagated toward the outside of the bend was revealed by microscopy of a longitudinal section taken through bend 2. The small bend radius was interpreted to contribute to spring fatigue as a result of result in straining at the bend zone. The spring was concluded to have failed in fatigue. It was recommended that the springs should be made of wire free from straightener marks and the bending tool should be redesigned so as not to indent the wire.

The conical helical spring sealed, within each switch enclosure, fractured to lead to the failure of several electrical toggle switches. The spring was fabricated from 0.43 mm diam AISI type 302 stainless steel wires. Appreciable amount of scale was observed on the fracture surface and tool marks were revealed on the inner surface of the broken spring. A typical fatigue fracture that originated at a tool mark on the wire surface was revealed by inspection of a fracture surface of the broken springs. Regions which displayed beach marks around the fracture origin and parallel striations within the beach-mark regions were revealed by scanning electron microscopy. As a corrective measure, the spring-winding operation was altered to eliminate the tool marks.