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thermomechanical analysis
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Published: 15 May 2022
Fig. 24 Thermomechanical analysis (TMA) evaluation of degree of cure by penetration. Source: Ref 25
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Published: 15 May 2022
Fig. 25 Thermomechanical analysis (TMA), Vicat softening temperatures, under 10.3 MPa (1.5 ksi). Source: Ref 26
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Published: 15 May 2022
Fig. 26 Thermomechanical analysis (TMA) deflection temperature under load (DTUL) at 1.82 MPa (0.264 ksi). Source: Ref 26
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Published: 15 May 2022
Fig. 28 Thermomechanical analysis (TMA) properties of commercial polymers. PSU, polysulfone; PPO, polyphenylene oxide; PVC, polyvinyl chloride; PTFE, polytetrafluoroethylene; PS-BD, polystyrene-butadiene; PMMA, polymethyl methacrylate; PS, polystyrene; PC, polycarbonate; ABS, acrylonitrile
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Published: 15 May 2022
Fig. 19 Properties of commercial polymers according to thermomechanical analysis. PS, polystyrene; PPO, polyphenylene oxide; PSU, polysulfone; ABS, acrylonitrile-butadiene-styrene; PC, polycarbonate; PVC, polyvinyl chloride; PMMA, polymethyl methacrylate; PE, polyethylene; PS-BD, polystyrene
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in Characterization of Thermosetting Resins and Polymers
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
Fig. 19 Idealized thermomechanical analysis curve in the expansion mode. α, coefficient of thermal expansion; T g , glass transition temperature. Source: Ref 7
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in Characterization of Thermosetting Resins and Polymers
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
Fig. 40 Thermomechanical analysis penetration as a function of temperature for a molded polyester gel coat. Source: Ref 45
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in Characterization of Thermosetting Resins and Polymers
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
Fig. 42 Schematic of thermomechanical analysis sample-support fixture used to measure heat-distortion temperature. Source: Ref 88
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in Characterization of Thermosetting Resins and Polymers
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
Fig. 43 Thermomechanical analysis (TMA) probe-displacement curves and extrapolated heat-distortion temperature values for two-ply unidirectional graphite composite. Source: Ref 88
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in Characterization of Plastics in Failure Analysis
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
Fig. 10 Thermomechanical analysis thermogram representing a typical semicrystalline plastic resin
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in Characterization of Plastics in Failure Analysis
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
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in Characterization of Plastics in Failure Analysis
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
Fig. 12 Thermomechanical analysis thermogram showing a high level of residual stress in an amorphous plastic resin
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Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003546
EISBN: 978-1-62708-180-1
... stress analysis and fracture mechanics analyses of the casing. fracture mechanics residual life prediction stress analysis thermomechanical fatigue turbine casing THERMOMECHANICAL FATIGUE (TMF) refers to the process of fatigue damage under simultaneous changes in temperature and mechanical...
Abstract
Thermomechanical fatigue (TMF) refers to the process of fatigue damage under simultaneous changes in temperature and mechanical strain. This article reviews the process of TMF with a practical example of life assessment. It describes TMF damages caused due to two possible types of loading: in-phase and out-of-phase cycling. The article illustrates the ways in which damage can interact at high and low temperatures and the development of microstructurally based models in parametric form. It presents a case study of the prediction of residual life in a turbine casing of a ship through stress analysis and fracture mechanics analyses of the casing.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006781
EISBN: 978-1-62708-295-2
... Abstract Thermomechanical fatigue (TMF) is the general term given to the material damage accumulation process that occurs with simultaneous changes in temperature and mechanical loading. TMF may couple cyclic inelastic deformation accumulation, temperature-assisted diffusion within the material...
Abstract
Thermomechanical fatigue (TMF) is the general term given to the material damage accumulation process that occurs with simultaneous changes in temperature and mechanical loading. TMF may couple cyclic inelastic deformation accumulation, temperature-assisted diffusion within the material, temperature-assisted grain-boundary evolution, and temperature-driven surface oxidation, among other things. This article discusses some of the major aspects and challenges of dealing with TMF life prediction. It describes the damage mechanisms of TMF and covers various experimental techniques to promote TMF damage mechanisms and elucidate mechanism coupling interactions. In addition, life modeling in TMF conditions and a practical application of TMF life prediction are presented.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006924
EISBN: 978-1-62708-395-9
... Abstract This article discusses the most common thermal analysis methods for thermosetting resins. These include differential scanning calorimetry, thermomechanical analysis, thermogravimetric analysis, and dynamic mechanical analysis. The article also discusses the characterization of uncured...
Abstract
This article discusses the most common thermal analysis methods for thermosetting resins. These include differential scanning calorimetry, thermomechanical analysis, thermogravimetric analysis, and dynamic mechanical analysis. The article also discusses the characterization of uncured thermosetting resins as well as the curing process. Then, the techniques to characterize the physical properties of cured thermosets and composites are presented. Several examples of stress-strain curves are shown for thermosets and thermoplastic polymers.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001593
EISBN: 978-1-62708-234-1
... utilized included scanning electron microscopy, Fourier transform infrared spectroscopy, differential scanning calorimetry, thermomechanical analysis, and melt flow rate determination. It was the conclusion of the investigation that the part failed via brittle fracture, with evidence also indicating low...
Abstract
A failure analysis was conducted on a flow-sensing device that had cracked while in service. The polysulfone sensor body cracked radially, adjacent to a molded-in steel insert. This article describes the investigative methods used to conduct the failure analysis. The techniques utilized included scanning electron microscopy, Fourier transform infrared spectroscopy, differential scanning calorimetry, thermomechanical analysis, and melt flow rate determination. It was the conclusion of the investigation that the part failed via brittle fracture, with evidence also indicating low cycle fatigue associated with cyclic temperature changes from normal service. The design of the part and the material selection were significant contributing factors because of stresses induced during molding, physical aging of the amorphous polysulfone resin, and the substantial differential in coefficients of thermal expansion between the polysulfone and the mating steel insert.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003525
EISBN: 978-1-62708-180-1
... Abstract This article reviews the analytical techniques most commonly used in plastic component failure analysis. These include the Fourier transform infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis...
Abstract
This article reviews the analytical techniques most commonly used in plastic component failure analysis. These include the Fourier transform infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis. The descriptions of the analytical techniques are supplemented by a series of case studies that include pertinent visual examination results and the corresponding images that aid in the characterization of the failures. The article describes the methods used for determining the molecular weight of a plastic resin. It explains the use of mechanical testing in failure analysis and also describes the considerations in the selection and use of test methods.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006931
EISBN: 978-1-62708-395-9
... the characterization of plastics by infrared and nuclear magnetic resonance spectroscopy, differential scanning calorimetry, differential thermal analysis, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis. The article also discusses the use of X-ray diffraction for analyzing...
Abstract
This article presents tools, techniques, and procedures that engineers and material scientists can use to investigate plastic part failures. It also provides a brief survey of polymer systems and the key properties that need to be measured during failure analysis. It describes the characterization of plastics by infrared and nuclear magnetic resonance spectroscopy, differential scanning calorimetry, differential thermal analysis, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis. The article also discusses the use of X-ray diffraction for analyzing crystal phases and structures in solid materials.
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in Characterization of Thermosetting Resins and Polymers
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
Fig. 39 Schematic of measurement of softening temperature by thermomechanical analysis in the penetration mode. Source: Ref 7
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Image
Published: 15 May 2022
Fig. 17 Heat-deflection temperature in accordance with ASTM D648 at 1.8 MPa (0.264 ksi) of thermoplastics according to thermomechanical analysis; 5 °C/min (9 °F/min) in flexure. PVC, polyvinyl chloride; LDPE, low-density polyethylene; HDPE, high-density polyethylene; PC, polycarbonate
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