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Annealing tests with specimens from flange disk. 1 × (see additional design...
Available to Purchase
in Steel Casting with Insufficient Strength Properties
> ASM Failure Analysis Case Histories: Processing Errors and Defects
Published: 01 June 2019
Fig. 11 Annealing tests with specimens from flange disk. 1 × (see additional designation at fractures)
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Book Chapter
Failure Investigation of Longitudinal Seam Welded Elevated Temperature Header
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001669
EISBN: 978-1-62708-229-7
... overtemperature lead specimen approach was taken, whereby failure of a test specimen in the laboratory would precede failures in the plant. These tests revealed approximately a 2:1 difference in life for the base metal as compared to weld metal. Electric power generation Outlet header Superheaters Welded...
Abstract
As the result of a leak detected in a plate-formed header at PENELEC'S Shawville Unit No. 3, an extensive failure investigation was initiated to determine the origin of cracking visible along the longitudinal weld seam. Fabricated from SA387-D material and designed for a superheater outlet temperature of 566 deg C, the 11.4 cm thick header had operated for approximately 187,000 h at the time of the failure. Discussion focuses on the results of a metallographic examination of boat samples removed from the longitudinal seam weldment in the vicinity of the failure and at other areas of the header where peak temperatures were believed to have been reached. The long-term mechanical properties of the service-exposed base metal and creep-damaged weld metal were determined by creep testing. Based on the utility's decision to replace the header within one to three years, an isostress overtemperature lead specimen approach was taken, whereby failure of a test specimen in the laboratory would precede failures in the plant. These tests revealed approximately a 2:1 difference in life for the base metal as compared to weld metal.
Book Chapter
Intergranular Cracking in an Air Bottle Because of Torch Overheating Before Welding
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047632
EISBN: 978-1-62708-235-8
... boss on one side. After annealing, hot spinning, annealing a second time, and tack welding a port fitting, the assembly was torch preheated to 120 to 150 deg C (250 to 300 deg F). The port fitting was then welded in place. Final full heat treatment to the T62 temper was followed by machining, testing...
Abstract
An air bottle, machined from a solid block of aluminum alloy 2219-T852, displayed liquid-penetrant crack indications after assembly welding. The air bottle was machined to rough shape, a 3.8 mm (0.15 in.) wall thickness cylindrical cup with a 19 mm (3/4 in.) wall thickness integral boss on one side. After annealing, hot spinning, annealing a second time, and tack welding a port fitting, the assembly was torch preheated to 120 to 150 deg C (250 to 300 deg F). The port fitting was then welded in place. Final full heat treatment to the T62 temper was followed by machining, testing, and inspection. The crack indications were found only on one side of the boss and on the lower portion of the hot-spun dome region. The metallographic specimens revealed triangular voids and severe intergranular cracks. The cracks displayed the glossy surfaces typical of melted and resolidified material. The localized cracks in the air bottle were from grain-boundary eutectic melting caused by local torch overheating used in preparation for assembly welding of a port fitting. A change in design was scheduled to semiautomatic welding without the use of preheating for the joining of the port fitting for the dome opening.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.design.c0046155
EISBN: 978-1-62708-233-4
... Abstract A structure had been undergoing fatigue testing for several months when a post-like member heat treated to a tensile strength of 1517 to 1655 MPa (220 to 240 ksi) ruptured. The fracture occurred in the fillet of the post that contacted the edge of a carry-through box bolted...
Abstract
A structure had been undergoing fatigue testing for several months when a post-like member heat treated to a tensile strength of 1517 to 1655 MPa (220 to 240 ksi) ruptured. The fracture occurred in the fillet of the post that contacted the edge of a carry-through box bolted to the member. At failure, the part was receiving a second set of loads up to 103.6% of design load. Visual investigations showed rubbing and galling of the fillet. Microscopic and metallographic examination revealed beach marks on the fracture surface and evidence of cold work and secondary cracking in the rubbed and galled area. Electron fractography confirmed that cracking had initiated at a region of tearing and that the cracks had propagated by fatigue. Mechanical properties of all specimens exceeded the minimum values specified for the post. This evidence supports the conclusion that fatigue was the primary cause of failure. Rubbing of the faying surfaces worked the interference area on the post until small tears developed. These small tears became stress-concentration points that nucleated fatigue cracks. Recommendations included rounding the edge of the box in the area of contact with the post to ensure a tangency fit.
Book
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.9781627082952
EISBN: 978-1-62708-295-2
Book Chapter
Accelerated Life Testing and Aging
Available to PurchaseSeries: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006909
EISBN: 978-1-62708-395-9
...), estimating the long-term performance or life expectancy of components designed to operate without failure or loss of functionality for 10 to 20 years (or longer) is difficult. Few, if any, products or components can be expected to fail or degrade substantially when tested at normal (unaccelerated) conditions...
Abstract
Accelerated life testing and aging methodologies are increasingly being used to generate engineering data for determining material property degradation and service life (or fitness for purpose) of plastic materials for hostile service conditions. This article presents an overview of accelerated life testing and aging of unreinforced and fiber-reinforced plastic materials for assessing long-term material properties and life expectancy in hostile service environments. It considers various environmental factors, such as temperature, humidity, pressure, weathering, liquid chemicals (i.e., alkalis and acids), ionizing radiation, and biological degradation, along with the combined effects of mechanical stress, temperature, and moisture (including environmental stress corrosion). The article also includes information on the use of accelerated testing for predicting material property degradation and long-term performance.
Book Chapter
Mechanical Testing and Properties of Plastics—An Introduction
Available to PurchaseSeries: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006928
EISBN: 978-1-62708-395-9
..., the test specimen is either a standard type I or II bar, in accordance with ASTM D638, that is preconditioned to ASTM D618 specifications. The test apparatus is designed to ensure that the applied force does not vary with time and is coaxial with the specimen. As with other tests, the test specimen must...
Abstract
This article briefly introduces some commonly used methods for mechanical testing. It describes the test methods and provides comparative data for the mechanical property tests. In addition, creep testing and dynamic mechanical analyses of viscoelastic plastics are also briefly described. The article discusses the processes involved in the short-term and long-term tensile testing of plastics. Information on the strength/modulus and deflection tests, impact toughness, hardness testing, and fatigue testing of plastics is also provided. The article describes tension testing of elastomers and fibers. It covers two basic methods to test the mechanical properties of fibers, namely the single-filament tension test and the tensile test of a yarn or a group of fibers.
Book Chapter
Impact Loading and Testing
Available to PurchaseSeries: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006919
EISBN: 978-1-62708-395-9
... design requirements. Perhaps three of the most commonly used tests for impact performance are the Izod and Charpy notched-beam tests and the dart penetration test. Each is briefly discussed as follows. The Izod and Charpy tests are very similar in that they are both notched-beam specimens subjected...
Abstract
This article reviews the impact response of plastic components and the various methods used to evaluate it.. It describes the effects of loading rate on polymer deformation and the influence of temperature and strain rate on failure mode. It discusses the advantages and limitations of standard impact tests, the use of puncture tests for assessing material behavior under extreme strain, and the application of fracture mechanics for analyzing impact failures. It also develops and demonstrates the theory involved in the design and analysis of thin-walled, injection-molded plastic components.
Book Chapter
Mechanical Testing in Failure Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006761
EISBN: 978-1-62708-295-2
... are designed to give a quantitative result and have an objective endpoint. In contrast, bending ductility tests give a pass/fail result with a subjective endpoint; the test operator judges whether a surface has undergone cracking. Test procedures and specimen-preparation methods have evolved without close...
Abstract
Mechanical testing is an evaluative tool used by the failure analyst to collect data regarding the macro- and micromechanical properties of the materials being examined. This article provides information on a few important considerations regarding mechanical testing that the failure analyst must keep in mind. These considerations include the test location and orientation, the use of raw material certifications, the certifications potentially not representing the hardware, and the determination of valid test results. The article introduces the concepts of various mechanical testing techniques and discusses the advantages and limitations of each technique when used in failure analysis. The focus is on various types of static load testing, hardness testing, and impact testing. The testing types covered include uniaxial tension testing, uniaxial compression testing, bend testing, hardness testing, macroindentation hardness, microindentation hardness, and the impact toughness test.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001852
EISBN: 978-1-62708-241-9
... and elevated temperature have not received much attention even though such properties should be known for the design and application of electroformed nickel parts. Monotonic and cyclic testing, metallographic testing, and finite element analysis of an electroformed pure nickel mould under cyclic thermal...
Abstract
A 2–3 mm thick electroformed nickel mold showed early cracking under thermal load cycles. To determine the root cause, investigators obtained monotonic and cyclic properties of electroformed nickel at various temperatures and identified possible fatigue mechanisms. With the help of finite element modeling, they analyzed the material as well as the design and in-service application of the mold. They discovered that overconstraining the mold, while it was in service, caused excessive thermal stresses which accelerated crack initiation and propagation. Investigators also proposed remedies to prevent additional failures.
Book Chapter
Analysis of Bearing Cup Assembly Failure in Drive Shaft Assembly
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001759
EISBN: 978-1-62708-241-9
... For push-out force checking, load testing rig was used. Fig. 5 shows load testing rig. Fig. 5 Load testing rig It consists of rotating handle screw connected to shaft, which in turn exerts the applied load on specimen, and analog pointer shows the magnitude of the load applied on specimen...
Abstract
A bearing cup in a drive shaft assembly on an automobile was found to have failed. A detailed analysis was conducted using the QC story approach, which begins by proposing several possible failure scenarios then following them to determine the main root cause. A number of alternative solutions were identified and then validated based on chemical analysis, endurance and hardness tests, and microstructural examination. The investigation revealed that carbonitriding can effectively eliminate the type of failure encountered because it prevents through hardening of the bearing cup assembly.
Book Chapter
Failure Analysis of a Space Shuttle Solid Rocket Booster Auxiliary Power Unit (APU) Fuel Isolation Valve
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001294
EISBN: 978-1-62708-215-0
... assembly passes a preflight helium pressure test. However a future design should use the same material for the poppet and bellows so that the final heat treatment will produce an assembly not susceptible to IGA. Booster rockets Heating effects Sensitizing Tempering UNS S35500 UNS S35080 AM355...
Abstract
A precipitation-hardened stainless steel poppet valve assembly used to shut off the flow of hydrazine fuel to an auxiliary power unit was found to leak. SEM and optical micrographs revealed that the final heat treatment designed for the AM-350 bellows material rendered the AM-355 poppet susceptible to intergranular corrosive attack (IGA) from a decontaminant containing hydroxy-acetic acid. This attack provided pathways for which fluid could leak across the sealing surface in the closed condition. It was concluded that the current design is flight worthy if the poppet valve assembly passes a preflight helium pressure test. However a future design should use the same material for the poppet and bellows so that the final heat treatment will produce an assembly not susceptible to IGA.
Book Chapter
Failure of a Seat on a School Playground Swing Set
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001130
EISBN: 978-1-62708-214-3
... fracture surface section to a position two hole-rows away. The remainder was left as received for future tests by the manufacturer. One specimen was prepared for scanning electron microscope (SEM) fractographic examination, four specimens were cut for tensile and ductility testing, and one tab...
Abstract
The failure during use of a seat on a heavy-duty swing set at an elementary school was investigated. The seat contained a perforated reinforcing sheet metal (galvanized type 430 stainless steel) insert covered by an elastomeric material. Specimens of the reinforcing sheet from the failed seat were examined using SEM fractography, tensile and ductility tests, and spectrographic chemical analysis. The test results showed that the steel used did not meet the manufacturer's specifications for ductility (elongation). In addition, the small-diameter punched holes caused a stress concentration factor that aggravated the brittleness of the steel.
Book Chapter
High-Temperature Failure by Perforation of Incoloy 800H Pigtails in Reformer Furnaces
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001108
EISBN: 978-1-62708-214-3
.... Fig. 2 Metallographic sample (a) and tensile test specimen (b) from the pigtail tubing. Visual Examination of General Physical Features Visual and low-magnification optical examination of the samples revealed evidence of perforation only in the curved parts. No major distortion...
Abstract
The curved parts of exit pigtails made of wrought Incoloy 800H tubing used in steam reforming furnaces failed by performance after a period of service shorter than that predicted by the designers. Examination of a set of tubes consisting of both curved (perforated) and straight parts revealed that the cracks initiated at the outer surface by a combined mechanism of creep and intergranular embrittlement. A smaller grain size resulting from cold bending fabrication procedures for the curved parts was responsible for accelerating the embrittlement. It was recommended that hot bending be used for fabrication of the curved parts. A change of alloy to a low-alloy chromium-molybdenum allay to protect against heat was also suggested.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c9001151
EISBN: 978-1-62708-219-8
... test results on the spliced angle iron sections. A specimen being tensile tested is shown in Fig. 8 . This particular specimen included the pair of angle iron sections containing a splice and the splice bar. Of the thirty specimen tested, twenty-five were single specimens and only five were pairs...
Abstract
A portion of the roof of a single story building collapsed during a thunder storm. A failure analysis was conducted to determine whether this structural failure was due to improper design, substandard construction materials, faulty erection, or extreme weather conditions. The failure analysis consisted of an onsite inspection, macrofractographic examination of the fractures where the girders were welded to the columns, macrofractographic examination of the fractured trusses, metallographic examination of the girder and truss materials, chemical analysis of the low-carbon steel girder and truss materials, and mechanical testing of the truss material. It was concluded that substandard structural components in combination with faulty construction was responsible for this service failure.
Book Chapter
Failure of a Copper Condenser Dashpot
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001312
EISBN: 978-1-62708-215-0
... . Fig. 9 Typical microhardness variations in the lower tubular portion Tensile Properties To study the effect of brazing on the mechanical properties of copper tube in the HAZ, miniaturized tensile test specimens were taken from the annealed region (near the upper cup portion) as well...
Abstract
A copper condenser dashpot in a refrigeration plant failed prematurely. The dashpot was a long tubular component with a cup brazed at each end. Stereomicroscopic examination of the fracture surface at low magnification revealed a typical ductile mode of failure. The failure was attributed to insufficient component thickness, which made the dashpot unable to withstand internal operating pressure, and to extensive annealing in the heat-affected zones of the brazed joints. It was recommended that the condenser dashpot design take into account the annealing effects of brazing. Hydrostatic testing at a pressure times greater than the maximum operating pressure prior to placing the component in service was also suggested.
Book Chapter
Cracking at the Threads of Stud Bolts Used for Lifting Plastic Mold Dies
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001378
EISBN: 978-1-62708-215-0
... face of the boss in contact with the die. Use roll forming rather than machine cutting for the threads. Devise a design that allows a wrench to engage the boss to allow insertion or removal of the stud bolt (for example, a hexagonal or square-headed boss). Conduct nondestructive testing...
Abstract
Two 38 mm (1.5 in.) diam threaded stud bolts that were part of a steel mold die assembly from a plastics molding operation were examined to determine their serviceability. Chemical analysis showed the material to be a plain carbon steel that approximated 1045. Visual examination revealed evidence of severe hammer blows to the clevis and boss areas and a gap between the die and the underside of the boss. Magnetic particle inspection showed cracks at the thread roots that, when examined metallographically, were found to contain MnS stringers. The cracking of the threads was attributed to a poor stud bolt design, which allowed a high stress concentration to occur at the base of the threads upon application of a lateral load. It was recommended that bolts of a new design that incorporated a stress-relieving groove be used. Threading of the bolt to eliminate the gap between the lower face of the boss and the die and an improved method of inserting or removing the bolt to avoid hammering (use of a wrench on a square or hexagonal boss) were also recommended.
Book Chapter
Fatigue and Corrosion Fatigue Failure Surfaces of Concrete Reinforcement
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c9001656
EISBN: 978-1-62708-219-8
... tested in sea water. It can be seen from Figure 8 that, unlike the former specimen, neither initiation site A1 nor A2 are located at the intersection of a longitudinal and a transverse lug. This, and the fact that there are more than one initiation site, shows that the corrosive environment...
Abstract
Some corrosion processes in the presence of chlorides, for steel embedded in concrete, are described and illustrated with the aid of scanning electron microscope EDXA data. Observations made of failure surfaces of reinforcements removed from the concrete beams after being subjected to sinusoidal load fluctuations at 6.7 Hz in air, 3% NaCl solution, and natural sea water are described. Reinforcement types studied included: hot-rolled mild steel bar, hot-rolled alloyed high strength bar, cold-worked high strength bar, galvanized bar of all these three types, nickel-clad bar and epoxy-coated bar.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001329
EISBN: 978-1-62708-215-0
... factors, the information presented should be viewed from a qualitative, rather than quantitative, perspective. Results of EDS scans (semiquantitative analysis) Table 1 Results of EDS scans (semiquantitative analysis) Specimen Composition, % EDS scan Mill test report Cu Al...
Abstract
Various aluminum bronze valves and fittings on the essential cooling water system at a nuclear plant were found to be leaking. The leakage was limited to small-bore socket-welded components. Four specimens were examined: three castings (an ASME SB-148 CA 952 elbow from a small-bore fitting and two ASME SB-148 CA 954 valve bodies) and an entire valve assembly. The leaks were found to be in the socket-weld crevice area and had resulted from dealloying. It was recommended that the weld joint geometry be modified.
Book Chapter
Reactor Cooling Water Expansion Joint Bellows: The Role of the Seam Weld in Fatigue Crack Development
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001682
EISBN: 978-1-62708-229-7
... the ultimate strength perpendicular to the seam weld was approximately 586 MPa (85,000 psi). The seam weld was stronger than the base material and when tests were conducted on samples which had the seam weld perpendicular to the specimen axis, most of the deformation was remote from the weld and fracture took...
Abstract
The secondary cooling water system pressure boundary of Savannah River Site reactors includes expansion joints utilizing a thin-wall bellows. While successfully used for over thirty years, an occasional replacement has been required because of the development of small, circumferential fatigue cracks in a bellows convolute. One such crack was recently shown to have initiated from a weld heat-affected zone liquation microcrack. The crack, initially open to the outer surface of the rolled and seam welded cylindrical bellows section, was closed when cold forming of the convolutes placed the outer surface in residual compression. However, the bellows was placed in tension when installed, and the tensile stresses reopened the microcrack. This five to eight grain diameter microcrack was extended by ductile fatigue processes. Initial extension was by relatively rapid propagation through the large-grained weld metal, followed by slower extension through the fine-grained base metal. A significant through-wall crack was not developed until the crack extended into the base metal on both sides of the weld. Leakage of cooling water was subsequently detected and the bellows removed and a replacement installed.
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