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Book Chapter
Polymer Processing—An Introduction
Available to PurchaseSeries: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006864
EISBN: 978-1-62708-395-9
... Abstract This article discusses technologies focused on processing plastic materials or producing direct tools used in plastics processing. The article focuses on extrusion and injection molding, covering applications, materials and their properties, equipment, processing details, part design...
Abstract
This article discusses technologies focused on processing plastic materials or producing direct tools used in plastics processing. The article focuses on extrusion and injection molding, covering applications, materials and their properties, equipment, processing details, part design guidelines, and special processes. It also covers the functions of the extruder, webline handling, mixing and compounding operations, and process troubleshooting. Thermoforming and mold design are covered. Various other technologies for polymer processing covered in this article are blow molding, rotational molding, compression molding, transfer molding, hand lay-up process, casting, and additive manufacturing.
Book Chapter
An Investigation of the Development of Defects During Flow Forming of High Strength Thin Wall Steel Tubes
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001601
EISBN: 978-1-62708-235-8
... Abstract Flow forming technology has emerged as a promising, economical metal forming technology due to its ability to provide high strength, high precision, thin walled tubes with excellent surface finish. This paper presents experimental observations of defects developed during flow forming...
Abstract
Flow forming technology has emerged as a promising, economical metal forming technology due to its ability to provide high strength, high precision, thin walled tubes with excellent surface finish. This paper presents experimental observations of defects developed during flow forming of high strength SAE 4130 steel tubes. The major defects observed are fish scaling, premature burst, diametral growth, microcracks, and macrocracks. This paper analyzes the defects and arrives at the causative factors contributing to the various failure modes.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003533
EISBN: 978-1-62708-180-1
... Abstract The scanning electron microscopy (SEM) is one of the most versatile instruments for investigating the microstructure of metallic materials. This article highlights the development of SEM technology and describes the operation of basic systems in an SEM, including the electron optical...
Abstract
The scanning electron microscopy (SEM) is one of the most versatile instruments for investigating the microstructure of metallic materials. This article highlights the development of SEM technology and describes the operation of basic systems in an SEM, including the electron optical column, signal detection and display equipment, and vacuum system. It discusses the preparation of samples for observation using an SEM and describes the application of SEM in fractography. If the surface remains unaffected and undamaged by events subsequent to the actual failure, it is often a simple matter to determine the failure mode by the use of an SEM. In cases where the surface is altered after the initial failure, the case may not be so straightforward. The article presents typical examples that illustrate these points. Image dependence on the microscope type and operating parameters is also discussed.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006819
EISBN: 978-1-62708-329-4
... of high-cycle welded fatigue methods, cycle-counting techniques, and a discussion on ratcheting are also offered. A historical synopsis of fatigue technology advancements and commentary on component design and fabrication strategies to mitigate fatigue damage and improve damage tolerance are provided...
Abstract
This article offers an overview of fatigue fundamentals, common fatigue terminology, and examples of damage morphology. It presents a summary of relevant engineering mechanics, cyclic plasticity principles, and perspective on the modern design by analysis (DBA) techniques. The article reviews fatigue assessment methods incorporated in international design and post construction codes and standards, with special emphasis on evaluating welds. Specifically, the stress-life approach, the strain-life approach, and the fracture mechanics (crack growth) approach are described. An overview of high-cycle welded fatigue methods, cycle-counting techniques, and a discussion on ratcheting are also offered. A historical synopsis of fatigue technology advancements and commentary on component design and fabrication strategies to mitigate fatigue damage and improve damage tolerance are provided. Finally, the article presents practical fatigue assessment case studies of in-service equipment (pressure vessels) that employ DBA methods.
Book Chapter
X-Ray Spectroscopy in Failure Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006770
EISBN: 978-1-62708-295-2
... in failure analysis than the more exact instrumentation employed in SEMs, the technology is advancing and is worthy of note due to its capability for nondestructive analysis and application in the field. This article begins with information on the basis of the x-ray signal. This is followed by information...
Abstract
X-ray spectroscopy is generally accepted as the most useful ancillary technique that can be added to any scanning electron microscope (SEM), even to the point of being considered a necessity by most operators. While “stand-alone” x-ray detection systems are used less frequently in failure analysis than the more exact instrumentation employed in SEMs, the technology is advancing and is worthy of note due to its capability for nondestructive analysis and application in the field. This article begins with information on the basis of the x-ray signal. This is followed by information on the operating principles and applications of detectors for x-ray spectroscopy, namely energy-dispersive spectrometers, wavelength-dispersive spectrometers, and handheld x-ray fluorescence systems. The processes involved in x-ray analysis in the SEM and handheld x-ray fluorescence analysis are then covered. The article ends with a discussion on the applications of x-ray spectroscopy in failure analysis.
Book Chapter
Nondestructive Testing in Failure Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006764
EISBN: 978-1-62708-295-2
... with discussion about the concept of the probability of detection (POD), on which the statistical reliability of crack detection is based. The coverage includes the various methods of surface inspection, including visual-examination tools, scanning technology in dimensional metrology, and the common methods...
Abstract
Nondestructive testing (NDT), also known as nondestructive evaluation (NDE), includes various techniques to characterize materials without damage. This article focuses on the typical NDE techniques that may be considered when conducting a failure investigation. The article begins with discussion about the concept of the probability of detection (POD), on which the statistical reliability of crack detection is based. The coverage includes the various methods of surface inspection, including visual-examination tools, scanning technology in dimensional metrology, and the common methods of detecting surface discontinuities by magnetic-particle inspection, liquid penetrant inspection, and eddy-current testing. The major NDE methods for internal (volumetric) inspection in failure analysis also are described.
Book Chapter
Scanning Electron Microscopy for Failure Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006769
EISBN: 978-1-62708-295-2
... the development of SEM technology and operating principles of basic systems of SEM. The basic systems covered include the electron optical column, signal detection and display equipment, and the vacuum system. The processes involved in the preparation of samples for observation using an SEM are described...
Abstract
The scanning electron microscope (SEM) is one of the most versatile instruments for investigating the microscopic features of most solid materials. The SEM provides the user with an unparalleled ability to observe and quantify the surface of a sample. This article discusses the development of SEM technology and operating principles of basic systems of SEM. The basic systems covered include the electron optical column, signal detection and display equipment, and the vacuum system. The processes involved in the preparation of samples for observation using an SEM are described, and the application of SEM in fractography is discussed. The article covers the failure mechanisms of ductile failure, brittle failure, mixed-mode failure, and fatigue failure. Lastly, image dependence on microscope type and operating parameters is also discussed.
Book Chapter
Inspection and Analysis of Aluminium Racks in Spent Fuel Storage Basins
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001710
EISBN: 978-1-62708-229-7
... the removal of the racks from the basin, a failure occurred in one of the racks and the Savannah River Technology Center was asked to investigate. This paper presents the results of the failure analysis and provides a discussion of the effects of corrosion on the structural integrity of the storage racks...
Abstract
Aluminum-clad spent nuclear fuel is stored in water filled basins at the Savannah River Site awaiting processing or other disposition. After more than 35 years of service underwater, the aluminum storage racks that position the fuel bundles in the basin were replaced. During the removal of the racks from the basin, a failure occurred in one of the racks and the Savannah River Technology Center was asked to investigate. This paper presents the results of the failure analysis and provides a discussion of the effects of corrosion on the structural integrity of the storage racks.
Book Chapter
Cracking of Pipe Nipples in Welding
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001206
EISBN: 978-1-62708-235-8
... in shaping and welding technology, it should be possible to prevent crack formation with steel type 35.8 of normal composition. Cracking (fracturing) Pipe Welded joints St 35.8 Joining-related failures A number of seamless pipe nipples of 70 mm diameter and 3.5 mm wall thickness made of steel...
Abstract
A number of seamless pipe nipples of 70 mm diam and 3.5 mm wall thickness made of steel type 35.8 were oxyacetylene welded to collectors of greater wall thickness with a round bead. X-ray examination showed crack initiation in the interior of the nipples close to the root of the weld seam. The cracks only appeared where the originally deposited bead was remelted in the regions of overlap. Given the construction and welding technique used, it would have been preferable to make the nipples of a steel lower in sulfur content. However, by taking advantage of all the potential in shaping and welding technology, it should be possible to prevent crack formation with steel type 35.8 of normal composition.
Book Chapter
Failure of Rockbolts in Underground Mines in Australia
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.conag.c9001637
EISBN: 978-1-62708-221-1
... Abstract Over the last 15 years there has been an increasing incidence of failure in rockbolts used in underground mines in Australia. Failures have also been observed in the United Kingdom where Australian Technology rockbolting is also used. Most of the failures in the United Kingdom were...
Abstract
Over the last 15 years there has been an increasing incidence of failure in rockbolts used in underground mines in Australia. Failures have also been observed in the United Kingdom where Australian Technology rockbolting is also used. Most of the failures in the United Kingdom were found to be initiated by corrosion pits, but in Australia, the fractures were considered likely to be due to stress-corrosion cracking (SCC). This paper reports a metallurgical study of 44 failed rockbolts from four different underground mines in Australia. The study confirmed that failure was generally due to SCC and showed that this was usually initiated by bending of the bolts that occurred due to lateral movement of the rock strata. It also showed that many of the failed bolts had very low toughness with Charpy impact values of 4 to 7 Joules.
Book Chapter
Fracture of Steam Pipes Removed From Service
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001128
EISBN: 978-1-62708-214-3
Abstract
Creep crack growth and fracture toughness tests were performed using test material machined from a seam welded ASTM A-155-66 class 1 (2.25Cr-1Mo) steel steam pipe that had been in service for 15 years. The fracture morphology was examined using SEM fractography. Dimpled fracture was found to be characteristic of fracture toughness specimens. Creep crack growth generally followed the fusion line region and was characterized as dimpled fracture mixed with cavities. These fracture morphologies were similar to those of an actual steam pipe. It was concluded that creep crack growth behavior was the prime failure mechanism of seam-welded steam pipes.
Book Chapter
Catastrophic Failure of a Fan in a Diesel Engine Cooler
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001612
EISBN: 978-1-62708-218-1
... edge distance and improper cleaning of the mating surfaces before welding may have contributed to the propensity to failure. Acknowledgments The cooperation and help rendered by the staff of the Materials Science & Technology Division, TCIRD during the investigation is greatly acknowledged...
Abstract
The fan used to cool a diesel engine fractured catastrophically after approximately 100 h of operation. The fan failed at a spider, which was resistance spot welded to a shim placed between two circular spiders of 3 mm thickness. The detailed analysis of the fracture indicated that the premature failure of the fan was due to inadequate bonding between the sheets at the weld nugget. The fracture was initiated from the nugget-plate interface. The inadequate penetration and lack of fusion between the steel sheets during resistance spot welding led to poor weld strength and the fracture during operation. The propensity to crack initiation and failure was accentuated by improper cleaning of the surfaces prior to welding and to inadequate nugget-to-sheet edge distance.
Book Chapter
Reactor Cooling Water Expansion Joint Bellows: The Role of the Seam Weld in Fatigue Crack Development
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001682
EISBN: 978-1-62708-229-7
Abstract
The secondary cooling water system pressure boundary of Savannah River Site reactors includes expansion joints utilizing a thin-wall bellows. While successfully used for over thirty years, an occasional replacement has been required because of the development of small, circumferential fatigue cracks in a bellows convolute. One such crack was recently shown to have initiated from a weld heat-affected zone liquation microcrack. The crack, initially open to the outer surface of the rolled and seam welded cylindrical bellows section, was closed when cold forming of the convolutes placed the outer surface in residual compression. However, the bellows was placed in tension when installed, and the tensile stresses reopened the microcrack. This five to eight grain diameter microcrack was extended by ductile fatigue processes. Initial extension was by relatively rapid propagation through the large-grained weld metal, followed by slower extension through the fine-grained base metal. A significant through-wall crack was not developed until the crack extended into the base metal on both sides of the weld. Leakage of cooling water was subsequently detected and the bellows removed and a replacement installed.
Book Chapter
Pitting Corrosion of Steel Tubes in an Air Preheater
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001616
EISBN: 978-1-62708-229-7
... & Technology Division, TCIRD during the investigation is greatly acknowledged by the authors. The authors are also thankful to the director of TCIRD for permission to publish the work. Reference Reference 1. Incropera F.P. and Dewitt D.P. : Fundamentals of Heat and Mass Transfer , 3rd ed...
Abstract
Severe pitting corrosion of a carbon steel tube was observed in the air preheater of a power plant, which runs on rice straw firing. Approximately 1450 tubes were removed from Stage 3 of the preheater (air inlet and flue gas outlet) due to corrosion and local bursting. Samples from Stage 2 (where corrosion was low) and Stage 3 (severe corrosion) were taken and subjected to visual inspection, SEM, x-ray diffraction, microhardness measurement, and chemical and microstructural analysis. It was determined that extended non-operation of the plant resulted in the settlement of corrosive species on the tubes in Stage 3. The complete failure of the tube occurred due to diffusion of these elements into the base metal and precipitation of potassium and chlorine compounds along the grain boundaries, with subsequent dislodging of grains. The nonmetallic inclusions acted as nucleating sites for local pitting bursting. Nonuniform heat transfer in Stage 3 operation accelerated the selective corrosion of front-end tubes. The relatively high heat transfer in this stage resulted in condensation of some corrosive gases and consequent corrosion. Continuous operation of the plant with some precautions during assembly of the tubes reduced the corrosion problem.
Book Chapter
Analysis of Center Burst During Hot Forging
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001615
EISBN: 978-1-62708-235-8
... of the material during upset forging. Strict control over the inclusion content in the raw material by changing the vendor eliminated the problem. Acknowledgments The cooperation and help rendered by the staff of Materials Science & Technology Division, TCIRD during the investigation is greatly...
Abstract
Carbon steel axle forgings were rejected due to internal cracks observed during final machining. To determine the cause of the cracks, the preforms of the forging were analyzed in detail at each stage of the forging. The analysis revealed a large central burst in the intermediate stage of the forging preform, which subsequently increased in the final stage. A high upset strain during forging, especially in the final stage, accentuated the center burst by high lateral flow of the metal. It was concluded that the center burst of the axle forging resulted from a high concentration of nonmetallic inclusions in the central portion of the raw bar stock rather than the usual problem of improper forging temperature. Strict control over the inclusion content in the raw material by changing the vendor eliminated the problem.
Book Chapter
Hydrogen Induced Cracking of a Tappet Adjusting Screw
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001613
EISBN: 978-1-62708-235-8
... to reduce the hardness after carburizing, completely eliminated the problem. Acknowledgments The cooperation and help rendered by the staff of the Materials Science & Technology Division, TCIRD during the investigation is greatly acknowledged by the author. The author is also thankful...
Abstract
The electroplated tappet adjusting screws used in diesel engines failed during initial bend testing. The analysis of the failure showed that the fracture was nucleated from the subsurface of the screw. The fracture surface was intergranular at the ID and OD region and microvoid coalescence in the center. The improper baking after electroplating of the screw led to H2-induced blistering/cracking. The high strength of the threaded region of the adjusting screw increased the failure propensity.
Book Chapter
Failure Analysis of Cylinder Clamping Rods in Diesel Engines
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.design.c9001582
EISBN: 978-1-62708-233-4
Abstract
This article discusses the failure of cylinder clamping rods in single cylinder diesel engines. The AISI 4140 hardened and tempered steel clamping rods were failing after 200 to 250 h of operation. The fatigue failures initiated at the root of the last thread on the clamping rod that was engaged in a blind hole in the cylinder block. The failures were caused by loose tolerances on the threads that resulted in a non-uniform distribution of load. The load was concentrated on the last threads to engage, thus causing fatigue crack nucleation at the thread root and propagation until the rod broke by overload. Changing the tolerance on the threads virtually eliminated the fatigue problem.
Book Chapter
Thermomechanical Fatigue—Mechanisms and Practical Life Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006781
EISBN: 978-1-62708-295-2
Abstract
Thermomechanical fatigue (TMF) is the general term given to the material damage accumulation process that occurs with simultaneous changes in temperature and mechanical loading. TMF may couple cyclic inelastic deformation accumulation, temperature-assisted diffusion within the material, temperature-assisted grain-boundary evolution, and temperature-driven surface oxidation, among other things. This article discusses some of the major aspects and challenges of dealing with TMF life prediction. It describes the damage mechanisms of TMF and covers various experimental techniques to promote TMF damage mechanisms and elucidate mechanism coupling interactions. In addition, life modeling in TMF conditions and a practical application of TMF life prediction are presented.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001643
EISBN: 978-1-62708-234-1
... to have shear lips of its own, indicating that not only did this vertical crack occur after the horizontal crack, but that the vertical crack traveled from top to bottom as it appears in this image. The “prove it to yourself” thinking skill is becoming increasing important as new tools and technologies...
Abstract
A crumpled piece of sheet metal had two cracks in a T-junction shape. The relative locations of shear lips in the cracks allowed deduction of which crack happened first, and which direction the cracks propagated.
Book Chapter
Thermomechanical Fatigue: Mechanisms and Practical Life Analysis
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003546
EISBN: 978-1-62708-180-1
... propagating into the substrate material of a thin-walled blade. Courtesy of Ashok Koul, Life Prediction Technologies, Inc. With this knowledge it should be possible to: Define the conditions for which empirical, experimentally based, life-prediction equations may be used Develop an appropriate...
Abstract
Thermomechanical fatigue (TMF) refers to the process of fatigue damage under simultaneous changes in temperature and mechanical strain. This article reviews the process of TMF with a practical example of life assessment. It describes TMF damages caused due to two possible types of loading: in-phase and out-of-phase cycling. The article illustrates the ways in which damage can interact at high and low temperatures and the development of microstructurally based models in parametric form. It presents a case study of the prediction of residual life in a turbine casing of a ship through stress analysis and fracture mechanics analyses of the casing.
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