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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001514
EISBN: 978-1-62708-218-1
... of the injuries sustained by the driver. The faulty welds in the unit body were apparently a consequence of improper settings of parameters on a multihead electrical resistance spot welding machine. Lack of appreciation of the hazard associated with failure of this weldment may have contributed to the low...
Abstract
A front-wheel drive hatchback automobile was involved in a severe front end impact. Failure analysis of the automobile revealed only a single sound spot weld in each of two 66 cm (26 in.) sections of both upper and lower floor sill flanges. Consequently, upon impact, the floor pan separated from the rocker panel, buckled and rotated upward and forward. This introduced slack in the seat belts since their retractors, being anchored to the floor pan, also rotated forward. Although not contributory to the accident itself, the faulty welds were responsible in part for the severity of the injuries sustained by the driver. The faulty welds in the unit body were apparently a consequence of improper settings of parameters on a multihead electrical resistance spot welding machine. Lack of appreciation of the hazard associated with failure of this weldment may have contributed to the low frequency of their physical inspection during production. A similar case involving faulty welds in a fuel delivery truck is also discussed.
Book Chapter
Aluminum/Refrigerant Reaction Resulting in the Failure of a Centrifugal Compressor
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001364
EISBN: 978-1-62708-215-0
... that a self-sustaining aluminum/refrigerant reaction (freon fire) had occurred in the failed compressor. The deposit samples consisted primarily of aluminum fluorides and carbon, known products of a high-temperature aluminum/refrigerant reaction. The highly exothermic reaction, which consumes aluminum, led...
Abstract
An investigation of the impeller and deposit samples from a centrifugal compressor revealed that an aluminum IR-12 refrigerant reaction had occurred, causing extensive damage to the second-stage impeller and contaminating the internal compressor components. The spherical surface morphology of the impeller fragments suggested that the aluminum had melted and resolidified. The deposits were similar in composition and were identified by XRD as consisting primarily of aluminum trifluoride. In addition, EDS analysis detected major amounts of chlorine and iron. Results of a combustion test indicated that the compressor deposit was comprised of a 9. 8 wt% carbon and that the condenser deposit contained 8.7 wt% carbon. It was concluded that the primary cause of failure was the rubbing of the impeller against the casting and that a self-sustaining Freon fire had occurred in the failed compressor
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001906
EISBN: 978-1-62708-217-4
... Abstract Suspension lugs fabricated from AISI 4340 steel used to facilitate loading of bombs onto the underside of military aircraft could not sustain required loads during routine proof load testing. Three failed lugs underwent visual examination, chemical analysis, metallography, hardness...
Abstract
Suspension lugs fabricated from AISI 4340 steel used to facilitate loading of bombs onto the underside of military aircraft could not sustain required loads during routine proof load testing. Three failed lugs underwent visual examination, chemical analysis, metallography, hardness testing, scanning electron microscopy, and energy-dispersive x-ray spectroscopy. It was determined that the failures were due to forging defects. Both forging laps and seams acted as stress concentrators when the lugs were loaded during proof testing.
Book Chapter
Introduction to Failure Analysis and Prevention
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003500
EISBN: 978-1-62708-180-1
... Abstract This article briefly introduces the concepts of failure analysis and root cause analysis (RCA), and the role of failure analysis as a general engineering tool for enhancing product quality and failure prevention. It reviews four fundamental categories of physical root causes, namely...
Abstract
This article briefly introduces the concepts of failure analysis and root cause analysis (RCA), and the role of failure analysis as a general engineering tool for enhancing product quality and failure prevention. It reviews four fundamental categories of physical root causes, namely, design deficiencies, material defects, manufacturing/installation defects, and service life anomalies, with examples. The article describes several common charting methods that may be useful in performing an RCA. It also discusses other failure analysis tools, including review of all sources of input and information, people interviews, laboratory investigations, stress analysis, and fracture mechanics analysis. The article concludes with information on the categories of failure and failure prevention.
Book Chapter
Introduction to Failure Analysis and Prevention
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006753
EISBN: 978-1-62708-295-2
... in a production environment. Six Sigma adopts these themes and extends the “reach” of the system to all levels of organizations, with a system to achieve, sustain, and maximize business success ( Ref 10 ). Six Sigma is founded on the use of measurements, facts, and statistics to move organizations in directions...
Abstract
This article briefly introduces the concepts of failure analysis, including root-cause analysis (RCA), and the role of failure analysis as a general engineering tool for enhancing product quality and failure prevention. It initially provides definitions of failure on several different levels, followed by a discussion on the role of failure analysis and the appreciation of quality assurance and user expectations. Systematic analysis of equipment failures reveals physical root causes that fall into one of four fundamental categories: design, manufacturing/installation, service, and material, which are discussed in the following sections along with examples. The tools available for failure analysis are then covered. Further, the article describes the categories of mode of failure: distortion or undesired deformation, fracture, corrosion, and wear. It provides information on the processes involved in RCA and the charting methods that may be useful in RCA and ends with a description of various factors associated with failure prevention.
Book Chapter
Hydrogen-Assisted Stress Cracking of Carburized and Zinc Plated SAE Grade 8 Wheel Studs
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001383
EISBN: 978-1-62708-215-0
... as sustained-load clamp tests, with and without a 5% salt solution. Visual Examination of General Physical Features The appearance of both front and rear stud failures were similar in that the fracture surfaces showed no sign of fatigue beach marks or deformation in the form of shear lips that would...
Abstract
Several case-hardened and zinc-plated carbon-manganese steel wheel studs fractured in a brittle manner after very limited service life. The fracture surfaces of both front and rear studs showed no sign of fatigue beach marks or deformation in the form of shear lips that would indicate either a fatigue mechanism or ductile overload failure. SEM analysis revealed that the mode of fracture was intergranular decohesion, which indicates an environmental influence in the fracture mechanism. The primary fracture initiated at a thread root and propagated by environmentally-assisted slow crack growth until final fracture. The natural stress concentration at the thread root, when tightened to the required clamp load concomitant with the presence of cracks in the carburized case, was sufficient to exceed the critical stress intensity for hydrogen-assisted stress cracking (HASC). The zinc plating exacerbated the situation by providing a strong local corrosion cell in the form of a sacrificial anode region adjacent to the cracked thread. The enhanced generation of hydrogen in a corrosive environment subsequently lead to HASC of the wheel studs.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001522
EISBN: 978-1-62708-235-8
... approach can reduce and help eliminate turbulent flow problems, saving potentially millions of manufacturing dollars through enhanced part production quality and fewer delivery schedule delays. The results may also have important long-term implications, positively impacting Air Force sustainability...
Abstract
In the EMD-2 Joint Directed Attack Munition (JDAM), the A357 aluminum alloy housing had been redesigned and cast via permanent mold casting, but did not meet the design strength requirements of the previous design. Mechanical tests on thick and thin sections of the forward housing assembly revealed tensile properties well below the allowable design values. Radiology and CT evaluations revealed no casting defects. Optical microscopy revealed porosity uniformly distributed throughout the casting on the order of 0.1 mm pore diam. Scanning electron microscopy revealed elongated pores, which indicated turbulent filling of the mold. Spherical pores would have indicated the melt had been improperly degassed. Based on these findings, it was recommended that the manufacturer analyze and redesign the gating system to eliminate the turbulent flow problem during the permanent mold casting process.
Book Chapter
Ruptured Stainless Steel Heater Tube
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.petrol.c9001247
EISBN: 978-1-62708-228-0
... material which could not then sustain the normal running conditions. Sulphidation could have occurred during the overheating period thereby weakening the tube just prior to rupture. Analysis has shown the corrosion products to be complex containing iron, nickel and sulphur. The form of the corrosion...
Abstract
Three samples from a ruptured 316 stainless steel tube were examined. The tube, 114 mm OD, wall thickness 8.00 mm, with 13 mm thick 321 stainless steel fins welded to the outer surface of the tube, was part of a heater through which sour gas, containing methane plus H2S and CO, passed at 1150 psig. The sour gas was heated to 600 deg F by burners playing on the outside of the tube burning “sweet” gas plus air. The inner and outer surfaces of all samples showed evidence of corrosive attack. Electron probe microanalysis showed the corrosion products contained sulfur with iron, together with nickel to a lesser extent. Local thinning, cavitation, and ductile deformation markings associated with the unmatched sample taken from the center of the fire showed the tube ruptured as a result of overheating. Overheating while the temperature recorder was off the chart caused severe loss of tube strength, resulting in ductile rupture. The minimum overheating temperature could be deduced at around 1200 deg F due to the presence of a eutectic observed metallographically within the surface corrosion products.
Book Chapter
Stress Corrosion Cracking of Ring Type Joint of Reactor Pipeline of a Hydrocracker Unit
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001774
EISBN: 978-1-62708-241-9
... [ 1 ]. SCC results from the combined action of three factors, namely, sustained tensile stresses in the material, a corrosive medium (a chloride-bearing or hydrogen-sulfide environment), and elevated temperature. There are also other factors which affect the SCC mechanism in austenitic grade...
Abstract
A ring-type joint in a reactor pipeline for a hydrocracker unit had failed. Cracks were observed on the flange and the associated ring gasket during an inspection following a periodic shutdown of the unit. The components were manufactured from stabilized grades of austenitic stainless steel; the flange from type 321, and the ring gasket from 347. Examination revealed that the failure occurred by transgranular stress-corrosion cracking, initiated by the presence of polythionic acid. Detailed metallurgical investigation was subsequently conducted to identify what may have caused the formation of polythionic acid in the process gas.
Book Chapter
Designing with Plastics
Available to PurchaseSeries: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006927
EISBN: 978-1-62708-395-9
... manner. The sustainable design perspective aims to address the user’s feeling of attachment toward the product, and to meet the user’s need to retain and reuse the product. Giving serious forethought to the user’s emotions while using the product; attempting to encourage the end-user’s behavior...
Abstract
This article provides background information needed by design engineers to create part designs optimized for plastics and plastic manufacturing processes. It describes the four essential elements of plastic part development, namely, material, process, tooling, and design, and provides general design rules for the plastic forming processes covered. It also discusses the steps involved in design validation and verification.
Book Chapter
Environmentally-Induced Fracture of Type 410 Martensitic Stainless Steel Self-Drilling Tapping Screws
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001094
EISBN: 978-1-62708-214-3
... sustained torque loading, and environmental exposure to distilled water, city water, rainwater, and brackish water under various torque loadings. The conditions of the field failures, that is, loss of torque and intergranular cracking, were reproducible for all the aqueous environmental exposures...
Abstract
Cadmium-coated type 410 martensitic stainless steel 1 4 -14 self-drilling tapping screws fractured during retorquing tests within a few weeks after installation. The screws were used to assemble structural steel frames for granite panels that formed the outer skin of a high-rise building. Fractographic and metallographic examination showed that the fractures occurred in a brittle manner from intergranular crack propagation. Laboratory and simulated environmental tests showed that an aqueous environment was necessary for the brittle fracture/cracking phenomenon. The cracks were singular and intergranular with little branching. Secondary subsurface cracks suggested possible hydrogen embrittlement. The 410 screws had been introduced to replace conventional case-hardened carbon steel screws that conform to SAE specification J78. Carbon steel screws had a proven record of acceptable performance for the intended application. It was recommended that use of the 410 screws be discontinued in preference to the case-hardened carbon steel screws.
Book Chapter
Hydrogen Damage and Embrittlement
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006784
EISBN: 978-1-62708-295-2
... environmental hydrogen. It is also commonly considered a subcritical crack growth mechanism that often produces time-delayed fractures in production parts (especially high-strength steels) even with no externally applied stress. The phenomenon is characterized by the simultaneous interactions of sustained...
Abstract
Hydrogen damage is a term used to designate a number of processes in metals by which the load-carrying capacity of the metal is reduced due to the presence of hydrogen. This article introduces the general forms of hydrogen damage and provides an overview of the different types of hydrogen damage in all the major commercial alloy systems. It covers the broader topic of hydrogen damage, which can be quite complex and technical in nature. The article focuses on failure analysis where hydrogen embrittlement of a steel component is suspected. It provides practical advice for the failure analysis practitioner or for someone who is contemplating procurement of a cost-effective failure analysis of commodity-grade components suspected of hydrogen embrittlement. Some prevention strategies for design and manufacturing problem-induced hydrogen embrittlement are also provided.
Book Chapter
Hydrogen Damage and Embrittlement
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003552
EISBN: 978-1-62708-180-1
... of a steel component is suspected. Many of the types of parts that were commonly diagnosed with hydrogen embrittlement in the 1980s and 1990s were low-cost commodity products, such as self-tapping screws and small spring clips. The financial resources available to perform a failure analysis in such cases...
Abstract
This article provides an overview of the classification of hydrogen damage. Some specific types of the damage are hydrogen embrittlement, hydrogen-induced blistering, cracking from precipitation of internal hydrogen, hydrogen attack, and cracking from hydride formation. The article focuses on the types of hydrogen embrittlement that occur in all the major commercial metal and alloy systems, including stainless steels, nickel-base alloys, aluminum and aluminum alloys, titanium and titanium alloys, copper and copper alloys, and transition and refractory metals. The specific types of hydrogen embrittlement discussed include internal reversible hydrogen embrittlement, hydrogen environment embrittlement, and hydrogen reaction embrittlement. The article describes preservice and early-service fractures of commodity-grade steel components suspected of hydrogen embrittlement. Some prevention strategies for design and manufacturing problem-induced hydrogen embrittlement are also reviewed.
Book Chapter
Corrosion and Cracking of the Internal Surfaces of a Black Liquor Digester
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001049
EISBN: 978-1-62708-214-3
.... Deep corrosion fissures then developed at hot crack sites as a result of crevice corrosion. Use of the appropriate overlay material was recommended. Claddings, corrosion Wood products 309 UNS S30900 Crevice corrosion Surface treatment related failures Background Routine inspections...
Abstract
Routine inspections of a carbon steel wood pulp digester revealed a sharply increasing number of cracks in the overlay metal on the internal surface of the digester after 1 and 2 years of service. The weld overlay was composed of type 309 stainless steel on the top fourth of the digester and of a proprietary high-nickel material on the bottom three-fourths. Examination revealed three distinct modes of deterioration. General corrosion was linked to the use of unspecified overlay metal. Cracking resulted during installation from the use of a material susceptible to hot cracking. Deep corrosion fissures then developed at hot crack sites as a result of crevice corrosion. Use of the appropriate overlay material was recommended.
Book Chapter
Design-Related Failures of Plastic Parts
Available to PurchaseSeries: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006938
EISBN: 978-1-62708-395-9
... expansion mismatch between materials and time-based failures such as creep and environmental stress cracking if a sustained load is present. Design envelope considerations regarding the assembly of parts in a product therefore include the identification and specification of the nature of intended...
Abstract
A design may be improvable without presenting an unacceptable risk related to safety or performance. However, design-related failures can result from an oversight in performing one of the major design activities or from a failure to balance the competing demands inherent to part design. This article focuses on design-related failures in products utilizing polymeric materials, and reviews important considerations of the design envelope of plastic parts. The article provides a non-exhaustive list and descriptions of design tools that can support the design process and the prevention of design-related failures. It also discusses the most common causes of design-related failures of plastic parts. The article can assist in both failure analysis and in the prevention of failures in which design may be a contributing factor or a root cause.
Book Chapter
Failure of a Boiler Feed Pump Second-Stage Impeller
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001084
EISBN: 978-1-62708-214-3
.... The latter had sustained substantial mechanical damage, rendering it useless for evaluation. Therefore, the entire failure analysis was performed on small sections cut from the impeller itself. Visual Examination of General Physical Features The surface of the casting was visually examined for casting...
Abstract
Failure analysis was performed on a fractured impeller from a boiler feed pump of a fossil fuel power plant. The impeller was a 12% Cr martensitic stainless steel casting. The failure occurred near the outside diameter of the shroud in the vicinity of a section change at the shroud/vane junction. Sections cut from the impeller were examined visually and by SEM fractography. Microstructural, chemical, and surface analyses and surface hardness tests were conducted on the impeller segments. The results indicated that the impeller failed in fatigue with casting defects increasing stress and initiating fracture. In addition, the composition and hardness of the impeller did not meet specifications. Revision of the casting process and institution of quality assurance methods were recommended.
Book Chapter
Failure of Nickel-Aluminum-Bronze Hydraulic Couplings, with Comments on General Procedures for Failure Analysis
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.marine.c9001617
EISBN: 978-1-62708-227-3
... cracks had been exposed to seawater, usually were uniformly corroded, but, in one case, bands of corrosion product with different colors were observed ( Fig. 7 ). For inboard couplings, on the other hand, there were generally little or no signs of corrosion on fracture surfaces, and x-ray photoelectron...
Abstract
Failures of various types of hydraulic couplings used to connect pipes in a naval vessel are described and used to illustrate some of the general procedures for failure analysis. Cracking of couplings, which were manufactured from nickel-aluminum- bronze extruded bar, occurred in both seawater and air environments. Cracks initiated at an unusually wide variety of sites and propagated in either longitudinal or circumferential directions with respect to the axis of the couplings. Fracture surfaces were intergranular and exhibited little or no sign of corrosion (for couplings cracked in air), and there was very limited plasticity. Macroscopic progression markings were observed on fracture surfaces of several couplings but were not generally evident. At very high magnifications, numerous slip lines, progression markings, and striations were observed. In a few cases, where complete separation had occurred in service, small areas of dimpled overload fracture were observed. It was concluded from these observations, and from comparisons of cracks produced in service with cracks produced by laboratory testing under various conditions, that cracking had occurred by fatigue. The primary cause of failure was probably the unanticipated presence of high-frequency stress cycles with very low amplitudes, possibly due to vibration, resonance, or acoustic waves transmitted through the hydraulic fluid. Secondary causes of failure included the presence of high tensile residual stresses in one type of coupling, undue stress concentrations at some of the crack-initiation sites, and overtorquing of some couplings during installation. Recommendations on ways to prevent further failures based on these causes are discussed.
Book Chapter
Fracture of Cast Steel Equalizer Beams
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c0089572
EISBN: 978-1-62708-218-1
... of dendritic segregation at lower left. 65x. (d) Micrograph showing nonhomogenized microstructure consisting of transformation products and ferrite. 65x The appearance of the fracture surface suggests that propagation of the crack occurred in a sequence of four large increments (regions B, C, D, and E...
Abstract
Two sand-cast low-alloy steel equalizer beams (ASTM A 148, grade 105-85) designed to distribute the load to the axles of a highway truck broke after an unreported length of service. Normal service life would have been about 805,000 km (500,000 mi) of truck operation. Investigation (visual inspection, chemical analysis, tensile testing, unetched 65x and 1% nital etched 65x magnification) supported the conclusions that the steel was too soft for the application – probably due to improper heat treatment. Fracture of the equalizer beams resulted from growth of mechanical cracks that were formed before the castings were heat treated. Recommendations included the following changes in processing: better gating and risering in the foundry to achieve sounder castings; better shakeout practice to avoid mechanical damage; better inspection to detect imperfections; and normalizing and tempering to achieve better mechanical properties.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001907
EISBN: 978-1-62708-217-4
... the plating process (in the case that the parts were electroplated rather than vacuum coated). The bolts were loaded to 80% of the UTS and sustained for 200 h. No failures occurred as a result of this testing. Also, ARL examined a number of bolts from different manufacturing lots for carburization and grain...
Abstract
Aircraft missile launcher attachment bolts fabricated from cadmium-coated Hy-tuf steel were found broken. Subsequent analysis of the broken bolts indicated three causes of failure. First, the bolts had been carburized, which was not in conformance with the heat treating requirements. Second, macroetching showed that the bolts has been machined from stock rather than forged, and the threads cut rather than rolled. It was also determined that hydrogen-assisted stress-corrosion cracking also played a part in the failure of the high-strength bolts.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003556
EISBN: 978-1-62708-180-1
... by the organisms disrupting the protective film. In addition to corrosion and hydrogen effects, the buildup of certain microbial metabolites in an environment may also foster crack growth by EAC. One example is the production of high levels of CO 2 needed to sustain near-neutral pH SCC ( Ref 42 ). This CO 2...
Abstract
This article focuses on the mechanisms of microbially induced or influenced corrosion (MIC) of metallic materials as an introduction to the recognition, management, and prevention of microbiological corrosion failures in piping, tanks, heat exchangers, and cooling towers. It discusses the degradation of various protective systems, such as corrosion inhibitors and lubricants. The article describes the failure analysis of steel, iron, copper, aluminum, and their alloys. It also discusses the probes available to monitor conditions relevant to MIC in industrial systems and the sampling and analysis of conditions usually achieved by the installation of removable coupons in the target system. The article also explains the prevention and control strategies of MIC in industrial systems.
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