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surface structure
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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0089459
EISBN: 978-1-62708-235-8
... marks to be the rough ground surface. An incipient crack 9.5 mm along with several other cracks on one of the fractured rods was revealed by liquid penetration examination. Metallographic examination of the fractured rods indicated a banded structure consisting of zones of ferrite and pearlite...
Abstract
The connecting end of two forged medium-carbon steel rods used in an application in which they were subjected to severe low-frequency loading failed in service. The fractures extended completely through the connecting end. The surface hardness of the rods was found to be lower than specifications. The fractures were revealed to be in areas of the transition regions that had been rough ground to remove flash along the parting line. The presence of beach marks, indicating fatigue failure, was revealed by examination. The fracture origin was confirmed by the location and curvature of beach marks to be the rough ground surface. An incipient crack 9.5 mm along with several other cracks on one of the fractured rods was revealed by liquid penetration examination. Metallographic examination of the fractured rods indicated a banded structure consisting of zones of ferrite and pearlite. It was established that the incipient cracks found in liquid-penetrant inspection had originated at the surface in the banded region, in areas of ferrite where this constituent had been visibly deformed by grinding. Closer control on the microstructure, hardness of the forgings and smooth finish in critical area was recommended.
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in Poorly Drawable Steel Wire for Ball Bearings
> ASM Failure Analysis Case Histories: Processing Errors and Defects
Published: 01 June 2019
Fig. 3 a). Surface structure of the wire, longitudinal section, etch: picral. 500× Crack region. b). Surface structure of the wire, longitudinal section, etch: picral. 500× At 300 mm distance from fracture.
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Published: 01 December 1992
Fig. 4 Surface structure along a longitudinal axis of specimen 2. The dark matrix is tempered martensite; the light-colored grainboundary network is cementite. Nital etch. 200×.
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in Failure of a Pump Shaft Ascribed to Accidental Local Heating
> ASM Failure Analysis Case Histories: Chemical Processing Equipment
Published: 01 June 2019
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in Leaking Coil Made of Stainless Steel
> ASM Failure Analysis Case Histories: Chemical Processing Equipment
Published: 01 June 2019
Fig. 4 Structure of carburized zone at the internal surface. Longitudinal section, etch: V2A-pickle. 500 ×
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in Brittle Failure of Reformer Tube During Pressure Test
> ASM Failure Analysis Case Histories: Failure Modes and Mechanisms
Published: 01 June 2019
Fig. 5 Further portion of fracture surface showing columnar crystal structure adjacent to outer wall.
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Published: 01 June 2019
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Published: 01 June 2019
Fig. 4 Structure of slide, etch: Picral. 200×. In center of gliding surface, transverse sections D—D and E—E.
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Published: 01 June 2019
Fig. 5 Structure of slide, etch: Picral. 200×. At edges of gliding surface, transverse sections D—D and E—E.
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Published: 01 June 2019
Fig. 8 Transverse section, etch: Picric acid. Structure near surface with deformation caused by shot peening.
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in Poorly Drawable Steel Wire for Ball Bearings
> ASM Failure Analysis Case Histories: Processing Errors and Defects
Published: 01 June 2019
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in Failure Analysis of NiTi Wires Used in Medical Applications
> Handbook of Case Histories in Failure Analysis
Published: 01 December 2019
Fig. 2 SEM image that shows candy cane structure on outside surface and flat fracture surface on torsional fracture
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in Problems Associated with Heat Treated Parts
> Analysis and Prevention of Component and Equipment Failures
Published: 30 August 2021
Fig. 13 Structure at the surface of a steel that was carburized and then subjected to decarburization. (a) Below Ac 1 . (b) Between Ac 1 and Ac 3 . (c) Above Ac 3
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Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003555
EISBN: 978-1-62708-180-1
... approximately 0.572 mm (0.0225 in.) Fig. 5 Sulfidation penetration into IN-690 liner approximately 50 to 250 μm deep. The sulfidized weakened structure of the alloy has led to cracking. Fig. 6 Formation of chromium sulfides (gray areas, such as marked by arrow) along the surface, caused...
Abstract
High temperature corrosion may occur in numerous environments and is affected by factors such as temperature, alloy or protective coating composition, time, and gas composition. This article explains a number of potential degradation processes, namely, oxidation, carburization and metal dusting, sulfidation, hot corrosion, chloridation, hydrogen interactions, molten metals, molten salts, and aging reactions including sensitization, stress-corrosion cracking, and corrosion fatigue. It concludes with a discussion on various protective coatings, such as aluminide coatings, overlay coatings, thermal barrier coatings, and ceramic coatings.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001258
EISBN: 978-1-62708-235-8
... sides of the fracture of 300 mm each. Missing in the lamellar surface structure, with the exception of the remnants of a coarse network, were the pre-eutectically precipitated carbides to be expected in this steel. Surrounding the ferritic region in the surface structure, a ring of lamellar pearlite...
Abstract
A drawing plant which processed steel wire of designation 105 Cr 2 for ball bearings had losses due to crack formation and wire breakage during drawing. To establish the reason for the breakage, seven fractures were submitted for investigation with contiguous wire segments on both sides of the fracture of 300 mm each. Missing in the lamellar surface structure, with the exception of the remnants of a coarse network, were the pre-eutectically precipitated carbides to be expected in this steel. Surrounding the ferritic region in the surface structure, a ring of lamellar pearlite is seen, which turns into the granular annealed structure towards the core. The described structural phenomena were noted in all of the seven fracture regions. Their intensity always decreased with increasing distance from the fracture. Surface decarburization caused the formation of lamellar pearlite during annealing. This investigation further revealed that the localized decarburization and pearlite formation was present already in the rolled wire in uneven distribution over the entire coil length.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001366
EISBN: 978-1-62708-215-0
... in the vicinity of the vane trailing edge. Some remaining vanes exhibited radial and transverse cracks in similar locations. Binocular and scanning electron microscope examinations showed that the cracks had been caused by high-cycle fatigue and had progressed from multiple origins on the vane surface. Structural...
Abstract
An AMS 4126 (7075-T6) aluminum alloy impeller from a radial inflow turbine fractured during commissioning. Initial examination showed that two adjacent vanes had fractured through airfoils in the vicinity of the vane leading edges, and one vane fractured through an airfoil near the hub in the vicinity of the vane trailing edge. Some remaining vanes exhibited radial and transverse cracks in similar locations. Binocular and scanning electron microscope examinations showed that the cracks had been caused by high-cycle fatigue and had progressed from multiple origins on the vane surface. Structural analysis indicated that the fatigue loading probably had been caused by forced excitation, resulting in the impeller vibrating at its resonant frequency. It was recommended that the impeller design, control systems, and material of construction be changed.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006774
EISBN: 978-1-62708-295-2
... (ductile, brittle, fatigue, and creep) are described briefly, principally in terms of fracture appearances. A description of the surface, structure, and behavior of each fracture process is also included. The article provides a framework from which a prospective analyst can begin to study the fracture...
Abstract
Engineering component and structure failures manifest through many mechanisms but are most often associated with fracture in one or more forms. This article introduces the subject of fractography and aspects of how it is used in failure analysis. The basic types of fracture processes (ductile, brittle, fatigue, and creep) are described briefly, principally in terms of fracture appearances. A description of the surface, structure, and behavior of each fracture process is also included. The article provides a framework from which a prospective analyst can begin to study the fracture of a component of interest in a failure investigation. Details on the mechanisms of deformation, brittle transgranular fracture, intergranular fracture, fatigue fracture, and environmentally affected fracture are also provided.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001498
EISBN: 978-1-62708-218-1
... no positive identification of material, a chemical analysis should be performed. Case Hardness Traverse Surface hardness (by Tukon, 500g): 58 HRC Effective case depth: 0.060 in. Core hardness: 35 HRC at midpoint, and at root, 33 HRC Microstructure Core structure: Low-carbon...
Abstract
One end of an axle shaft containing the integral spur pinion was submitted for examination, along with the report of a tooth pitting failure. The spur pinion, integral to the axle shaft, operated in a medium-size, off-highway truck at an open-pit mine, for “a relatively short time.” Only the pinion head had been returned. The shaft portion had been torch-cut away. Chemical analysis along with the microstructure confirmed the specified material was SAE 43BV12 Ni-Cr-Mo alloy steel. The mode of failure was surface contact fatigue through the shear plane subsurface at the lowest point of single-tooth contact. The cause of failure was tooth-tip interference from the mating gear teeth. Because the mating parts within the assembly had not been returned or examined, unanswered questions remained.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001503
EISBN: 978-1-62708-234-1
...-carbon martensite and pearlite. The case structure displayed very fine tempered martensite throughout, and no retained austenite. And the surface structure showed no evidence of frictional distress; it had been cleanly cut by abrasion. Final Analysis The mode of failure was severe abrasive wear...
Abstract
A hypoid pinion made from 4820 Ni-Mo alloy steel was the driving member of a power unit operating a rapid transit car. The pinion had been removed from service at the end of the initial test period because it showed undue wear. The mode of failure was severe abrasive wear. The cause of failure was insufficient surface hardness, resulting from improper heat treatment. A service recall for the remaining pinions was immediately initiated.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001037
EISBN: 978-1-62708-214-3
... grain-boundary network of cementite. Fig. 3 Central longitudinal zone of sample 2, showing banded structure of white ferrite and dark unresolved pearlite with MnS inclusions (light gray). 2% nital etch. 200×. Fig. 4 Surface structure along a longitudinal axis of specimen 2. The dark...
Abstract
Six wrist pins in a high-performance six-cylinder automotive engine failed after 4800 km (3000 mi) of normal operation. The pins were made of low-carbon steel that had been carburized both inside and outside. Two failed pins were examined. One had fractured into three pieces. The other had not fractured, but exhibited circumferential cracks on the surface of the central zone. Visual surface examination and metallographic and chemical analyses were performed on the specimens. Cracking was attributed primarily to poor heat treatment, resulting in a brittle grain-boundary network of cementite, and to a design that had a raised central section of the inner diameter whose fillets were locations of high stress concentration. Rough machining of the inner diameter and an excessively deep case also contributed to failure. A double type of heat treatment after carburizing and change of the design to eliminate the raised central section were recommended.