A crankshaft was overloaded on a test stand and suffered an incipient crack in the crank pin. The crack run generally parallel to the longitudinal axis and branched off at the entrance into the two fillets at the transition to the crank arm. It consisted of many small cracks, all of which propagated at an angle of approximately 45 deg to the longitudinal axis, and therefore were caused by torsion stresses. Neither macroscopic nor microscopic examination determined any material or processing faults. Experience has shown that torsion vibration fractures of this kind usually appear in comparatively short journal pins at high stresses. This crankshaft fracture was an example of the damage that is caused or promoted neither by material nor heat treatment mistakes nor by defects of design or machining, but solely by overstressing.

Valve seats fractured during testing and during service. The seats were machined from grade 11L17 steel and were surface hardened by carburization. Investigation (visual inspection, hardness testing, 59x SEM images, and 2% nital etched 15x cross sections) supported the conclusion that the fracture occurred via brittle overload, which was predominantly intergranular. The amount of bending evidence and the directionality of the core overload fracture features suggest that the applied stresses were not purely axial, as would be anticipated in this application. The level of retained austenite in the hardened case layer likely contributed to the failure.

A cast countershaft pinion on a car puller for a blast furnace broke after one month of service; expected life was 12 months. The pinion was specified to be made of 1045 steel heat treated to a hardness of 245 HRB. The pinion steel was analyzed and was a satisfactory alternative to 1045 steel. The pinion was annealed before flame or induction hardening of the teeth to a surface hardness of 363 HRB and a core hardness of 197 HRB. The broken pinion had a tooth which had failed by fatigue fracture through the tooth root because of the low strength from incomplete surface hardening of the tooth surfaces. Contributing factors included uneven loading because of misalignment and stress concentrations in the tooth roots caused by tool marks. Greater strength was provided by oil quenching and tempering the replacement pinions to a hardness of 255 to 302 HRB. Machining of the tooth roots was revised to eliminate all tool marks. Surface hardening was applied to all tooth surfaces, including the root. Proper alignment of the pinion was ensured by carefully checking the meshing of the teeth at startup.

A lever (machined from a casting made of AISI type 410 stainless steel, then surface hardened by nitriding) that was a component of the main fuel-control linkage of an aircraft engine fractured in flight after a service life of less than 50 h. Investigation (radiographic inspection) supported the conclusions that the lever broke at a cold shut extending through approximately 95% of the cross section. The normally applied load constituted an overload of the remainder of the lever. Recommendations included adding magnetic-particle inspection to the inspection procedures for this cast lever.

A recurring piston shaft failure problem on the billet-loading tray of an extrusion press was investigated. Two shafts fractured within a period of 10 days. The shaft was machined from normalized EN3 (AISI C1022) steel stock without further treatment. Visual, microstructural, chemical, and mechanical (hardness and tensile properties) analyses of failed shaft specimens were conducted. The examinations showed that the shafts had failed by fatigue. It was recommended that a low-alloy steel (e.g., 3% Ni-Cr) in the hardened and tempered condition and subjected to shot-peening surface-hardening treatment be used. The provision of a stop to reduce bending stresses was also recommended.

Replacement sprockets installed on chain drive shafts for winding fibers exhibited excessive wear. Metallographic and chemical analyses conducted on the original and replacement sprockets showed that the material of the replacement sprocket was 1020 low-carbon steel, whereas the original (and specified) material was medium-carbon 1045 steel. The low-carbon steel also had lower hardness because of a lower pearlite fraction in the microstructure. It was recommended that replacement sprockets be made of normalized 1045 steel. It was further suggested that wear resistance could be improved by through hardening or induction surface hardening of the teeth.

Deformation, surface cracking, and spalling on the raceway of the outer ring (made of 4140 steel) of a large bearing caused it to be replaced from a radar antenna. The raceway surfaces were to be flame hardened to 55 HRC minimum and 50 HRC 3.2 mm below the surface, according to specifications. Samples from both the inner and outer rings were examined. A much lower hardness (25.2 to 18.9 HRC) was indicated during a vertical traverse 4.1 cm from the outer surface of the outer ring while slightly lower hardness values (46.8 to 54.8 HRC) were seen on the hardness traverse on the inner ring raceway. The lower hardness values were attributed to improper flame hardening. It was confirmed by metallographic examination of a 3% nital etched sample that the inner ring (tempered martensite and ferrite) and the outer ring (ferrite, scattered patches of pearlite, and martensite) were not properly austenitized. Displacement of metal on the outer raceway was revealed by elongation of grain structure. It was concluded that the failure of the raceway surface was due to incomplete austenitization caused by the improper heat treatment during flame hardening process.

A portion of two large spur tooth bull gears made from 4147H Cr-Mo alloy steel that had spalling teeth was submitted for evaluation. The gears were taken from a final drive wheel reduction unit of a very large open-pit mining truck. The parts had met the material and initial heat treat hardening specifications. The mode of failure was tooth profile spalling. By definition, spalling originates at a case/core interface or at the juncture of a hardened/nonhardened area. The cause of this failure was either insufficient or no induction-hardened case along the active profile. The cause was activated by a nonfunctioning induction hardening coil that did not or was not allowed to harden the midprofile of several teeth.

A case-hardened sleeve made of C 15 (Material No. 1.0401) was flattened at two opposing sides and had cracked open at these places, the crack initiating at a face plane. The wall of the sleeve was 9 mm thick, but the flat ends were machined down to 5.5 mm from the outside. The customer had specified a 2 mm case depth and a hardness of at least HRC 55 at a depth of 1.5 mm. An etched cross section of the cracked end showed that the case layer had a depth of 2.3 mm, so that the sleeve was almost through-hardened at the flat ends. While the core material with the full wall thickness had the quench structure of low-carbon steel, the structure of the flattened area consisted of coarse acicular martensite with a small amount of pearlite (quench troostite) and ferrite. Therefore the sleeve was overheated and probably quenched directly from case. To prevent damage, it would have been necessary to have a lower case depth, carburize less deeply, and prevent overheating that causes brittleness and leads also to increased case depth, or else use a fine-grained steel of lower hardenability.

Splined rotor shafts (constructed from 1151 steel) used on small electric motors were found to miss one spline each from several shafts before the motors were put into service. Apparent peeling of splines on the induction-hardened end of each rotor shaft was revealed by visual and stereo-microscopic examination. One tooth on each shaft was found to be broken off. It was revealed by metallographic examination of an unetched section through the fractured tooth that the fracture surface was concave and had an appearance characteristic of a seam. Partial decarburization of the surface was revealed after etching with 1% nital. The presence of a crack, with typical oxides found in seams at its root, was disclosed by an unetched section through the shaft in an area unaffected by induction heating. The etched samples revealed similar decarburization as was noted on the fracture surface of the tooth. It was concluded that the seam had been present before the shaft was heat treated and these seams acted as stress raisers during induction hardening to cause the shaft failure. It was recommended that the specifications should specify that the shaft material should be free of seams and other surface imperfections.

A pilot-valve bushing fractured after only a few hours of service. In operation, the bushing was subjected to torsional stresses with possible slight bending stresses. A slight misalignment occurred in the assembly before fracture. The bushing was made of 8617 steel and was case hardened to a depth of 0.13 to 0.4 mm (0.005 to 0.015 in.) by carbonitriding. Specifications required that the part be carbonitrided, cooled, rehardened by quenching from 790 deg C (1450 deg F), then tempered at about 175 deg C (350 deg F). Visual examination, hardness testing, and metallographic and microstructural investigation supported the conclusion that the bushing fractured in fatigue because of a highly stressed case-hardened surface of unsatisfactory microstructure and subsurface nonmetallic inclusions. Cracks initiated at the highly stressed surface and propagated across the section as a result of cyclic loading. The precise cause of the unsatisfactory microstructure of the carbonitrided case could not be determined, but it was apparent that heat-treating specifications had not been closely followed. Recommendations included that inspection procedures be modified to avoid the use of steel containing nonmetallic stringer inclusions and that specifications for carbonitriding, hardening, and tempering be rigorously observed.

The 8620 steel latch tip, carburized and then induction hardened to a minimum surface hardness of 62 HRC, on the main-clutch stop arm on a business machine fractured during normal operation when the latch tip was subjected to intermittent impact loading. Fractographic examination 9x showed a brittle appearance at the fractures. Micrograph examination of an etched section disclosed several small cracks. Fracture of the parts may have occurred through similar cracks. Also observed was a burned layer approximately 0.075 mm (0.003 in.) deep on the latch surface, and hardness at a depth of 0.025 mm (0.001 in.) in this layer was 52 HRC (a minimum of 55 HRC was specified). Thus, the failure was caused by brittle fracture in the hardness-transition zone as the result of excessive impact loading. The burned layer indicated that the cracks had been caused by improper grinding after hardening. Redesign was recommended to include reinforcing the backing web of the tip, increasing the radius at the relief step to 1.5 x 0.5 mm (0.06 x 0.02 in.), the use of proper grinding techniques, and a requirement that the hardened zone extend a minimum of 1.5 mm (0.06 in.) beyond the step.

Failure of a case hardened steel shaft incorporated fuel pump in a turbine-powered aircraft resulted in damage to the aircraft. The disassembled pump was found to be dry and free of any contamination. Damage was exhibited on the pressure side of each spline tooth in the impeller and the relatively smooth cavities and undercutting of the flank on this side indicated that the damage was caused by an erosion or abrasion mechanism. A relatively smooth worn area was formed at the center of each tooth due to an abrasive action and an undulating outline with undercutting was observed on the damaged side. Particles of sand, paint, or plastic, fibers from the cartridge, brass, and steel were viewed in the brown residue on the filter cartridge under a low power microscope and later confirmed by chemical analysis. Large amount of iron was identified by application of a magnet. It was concluded that the combined effect of vibration and abrasive wear by sand and metal particles removed from the splines damaged the shaft. Case hardened spline teeth surface was recommended to increase resistance to wear and abrasion.

A gear manufacturer experienced service problems with various gears and pinions that had worn prematurely or had fractured. All gears and pinions were forged from 1.60Mn-5Cr steel and were case hardened by pack carburizing. Gear Failure: One of the gears showed severe wear on the side of the teeth that came into contact with the opposing gear during engagement. The microstructure at the periphery of a worn tooth at its unworn side consisted of coarse acicular martensite with a large percentage of retained austenite. Pinion Failure: The teeth of the pinion exhibited severe spalling; the microstructure at the surface consisted of coarse acicular martensite with retained austenite. Also, a coarse network of precipitated carbide particles showed that the carburization of the case had appreciably exceeded the most favorable carbon content. This evidence supported the following conclusions: 1) High wear rate on the gears was caused by spalling of the coarse-grain surface layer. The underlying cause of the wear was overheating during the carburization. 2) Pinion failure resulted from overheating combined with excessive case carbon content. Thus, no recommendations were made.

Two intermediate impeller drive gears (made of AMS 6263 steel, gas carburized, hardened, and tempered) exhibited evidence of pitting and abnormal wear after production tests in test-stand engines. The gears were examined for hardness, case depth, and microstructure of case and core. It was found that gear 1 had a lower hardness than specified while the case hardness of gear 2 was found to be within limits. Both the pitting and the wear pattern were revealed to be more severe on gear 1 than on gear 2. Surface-contact fatigue (pitting) of gear 1 (cause of lower carbon content of the carburized case and hence lower hardness) was found to be the reason for failure. It was recommended that the depth of the carburized case on impeller drive gears be increased from 0.4 to 0.6 mm to 0.6 to 0.9 mm to improve load-carrying potential and wear resistance. A minimum case-hardness requirement was set at 81 HRA.

Several teeth of a bevel pinion which was part of a drive unit in an edging mill failed after three months in service. Specifications required that the pinion be made from a 2317 steel forging and that the teeth be carburized and hardened to a case hardness of 56 HRC and a core hardness of 250 HRB. Two teeth were revealed by visual examination to have broken at the root and fatigue marks extending across almost the entire tooth were exhibited by the surface of the fracture. Cracking in all the tooth was showed by magnetic-particle inspection. The pinion was concluded to have failed by tooth-bending fatigue. Spalling was also noted on the pressure (drive) side of each tooth at the toe end which indicated some mechanical misalignment of the pinion with the mating gear that caused the cyclic shock load to be applied to the toe ends of the teeth.

A bolt breaks along a change in cross section well below its rated capacity. An anchoring screw spins freely in place, having snapped at its first supporting thread. A motor unexpectedly disengages its load, its driveshaft having fractured near a keyway. Such failures – involving axles, leaf springs, engine rods, wing struts, bearings, gears, and more – can occur, seemingly without cause, due to vibrational fracture. Vibrational fractures begin as cracks that form under cyclic loading at nominal stresses which may be considerably lower than the yield point of the material. The fracture is proceeded by local gliding and the development of cracks along lattice planes favorably orientated with respect to the principal stress. This non-reversible process is often misleadingly called “fatigue” and presents significant challenges to engineering teams that ill-advisedly take to searching for material faults. Several examples of notch-induced vibrational fractures are presented along with guidelines for investigating their cause.

A service water pump in a nuclear reactor failed when its shaft gave way. The fracture originated in the threaded portion of the sleeve nut on the drive-end side of the shaft. Results of the failure analysis showed that the cracking initiated at the thread root as a result of corrosion fatigue. Crack propagation occurred either by corrosion or mechanical fatigue. Evidence was found indicating high rotary bending stresses on the shaft during operation. The nonstandard composition of the En 8 steel used in the shaft and irregular maintenance reduced the life of the shaft. Recommendations included use of a case-hardened En 8 steel with the correct composition and regular maintenance of the pump.

Hardenability evaluation is typically applied to heat treatment process control, but can also augment standard metallurgical failure analysis techniques for steel components. A comprehensive understanding of steel hardenability is an essential complement to the skills of the metallurgical failure analyst. The empirical information supplied by hardenability analysis can provide additional processing and service insight to the investigator. The intent of this paper is to describe some applications of steel thermal response concepts in failure analysis, and several case studies are included to illustrate these applications.

One percent Cr-Mo low alloy constructional steel is widely used for high tensile applications, e.g., for manufacture of high tensile fasteners, heat treated shafts and axles, for automobile applications such as track pins for high duty tracked vehicles etc. The steel is fairly through hardening and heat treatment does not present any serious difficulty. Care is still required in processing to avoid decarburization. In an application of track pins for tracked vehicles, bars about 22 mm diam were required in heat treated and centerless-ground condition prior to induction hardening of the surface. Indifferent results were obtained in induction hardening; cracks were noticed, and patchy hardness figures were obtained on the final product in several batches. Metallographic examination of transverse sections through the defective areas showed decarburization to varying degrees, i.e., from partial to total decarburization. Observations suggested the defects originated at the stages of ingot making and rolling. This was apparently the reason for complete decarburization of the area with original surface defect which opened up further in the oxidizing atmosphere of the furnace with low melting clinkers from scale and furnace lining filling up the crevice of the original defect.