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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0089646
EISBN: 978-1-62708-235-8
... the failure. Recommendations included establishing closer control of chemical composition and foundry casting practices to alleviate the carbon-flotation form of segregation. Additionally, some nonmetallurgical practices in journal-finishing techniques were suggested to ensure optimal surface finish...
Abstract
Nodular cast iron crankshafts and their main-bearing inserts were causing premature failures in engines within the first 1600 km (1000 mi) of operation. The failures were indicated by internal noise, operation at low pressure, and total seizing. Concurrent with the incidence of engine field failures was a manufacturing problem: the inability to maintain a similar microfinish on the cope and drag sides of a cast main-bearing journal. Investigation supported the conclusion that the root cause of the failure was carbon flotation due to the crankshafts involved in the failures showing a higher-than-normal carbon content and/or carbon equivalent. Larger and more numerous cope side graphite nodules broke open, causing ferrite caps or burrs. They then became the mechanism of failure by breaking down the oil film and eroding the beating material. A byproduct was heat, which assisted the failure. Recommendations included establishing closer control of chemical composition and foundry casting practices to alleviate the carbon-flotation form of segregation. Additionally, some nonmetallurgical practices in journal-finishing techniques were suggested to ensure optimal surface finish.
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in Characterization of Metallic Piercings That Caused Adverse Reactions During Use
> ASM Failure Analysis Case Histories: Household Products and Consumer Goods
Published: 01 June 2019
Fig. 5 Comparison of the surface finish of Jewelry 2. (a) Initial as-received condition. (b) After electropolishing in perchloric acid (ethanol) solution, 35 V for 10 s. Scanning electron microscope, 100×
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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.homegoods.c9001610
EISBN: 978-1-62708-222-8
.... The lack of resistance to pitting corrosion associated with the poor surface finishing of the stainless steel jewelry may induce localized corrosion, promoting the release of cytotoxic metallic ions (such as Cr, Ni, and Mo) in the local tissue, which can promote several types of adverse effects...
Abstract
This investigation characterizes five surgical stainless steel piercings and one niobium piercing that caused adverse reactions during use, culminating with the removal of the jewelry. Chemical composition shows that none of the materials are in accordance with ISO standards for surgical implant materials. Additionally, none of the stainless steel piercings passed the pitting-resistance criterion of ISO 5832-1, which implies that [%Cr + 3.3(%Mo)] > 26. Under microscopic examination, most of the jewelry revealed the intense presence of linear irregularities on the surface. The lack of resistance to pitting corrosion associated with the poor surface finishing of the stainless steel jewelry may induce localized corrosion, promoting the release of cytotoxic metallic ions (such as Cr, Ni, and Mo) in the local tissue, which can promote several types of adverse effects in the human body, including allergic reactions. The adverse reaction to the niobium jewelry could not be directly associated with the liberation of niobium ions or the residual presence of cytotoxic elements such as Co, Ni, Mo, and Cr. The poor surface finish of the niobium jewelry seems to be the only variable of the material that may promote adverse reactions.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001640
EISBN: 978-1-62708-235-8
... of surface imperfections. Improving the surface finish or choosing a stronger alloy, were more likely to improve part durability than reducing the porosity. Complex failures Data interpretation Deviations from ideality Thinking errors Aluminum casting Casting-related failures A new supplier...
Abstract
A new supplier for aluminum die castings was being evaluated, and the castings failed to meet the durability test requirements. Specifically, the fatigue life of the castings was low. Initial inspection of the fatigue fracture surfaces revealed large-scale porosity visible to the naked eye. New castings with reduced porosity also failed the durability tests. The fatigue fracture surfaces of additional casting fragments were very rough and contained multiple ratchet marks along the inner fillet. These observations indicated the fatigue process was heavily influenced by the presence of surface imperfections. Improving the surface finish or choosing a stronger alloy, were more likely to improve part durability than reducing the porosity.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c0046205
EISBN: 978-1-62708-225-9
... include redesign of the fillet radius to a minimum of 1.6 mm (0.06 in.) and a maximum surface finish in the spline area of 0.8 microns. Material for the shafts should be modified to a nickel alloy steel, heat treated to a hardness of 28 to 32 HRC before machining. Ductile brittle transition Shafts...
Abstract
The splined shaft (1040 steel, heat treated to a hardness of 44 to 46 HRC and a tensile strength of approximately 1448 MPa, or 210 ksi) from a front-end loader used in a salt-handling area broke after being in service approximately two weeks while operating at temperatures near -18 deg C (0 deg F). During the summer, similar shafts had a service life of 5 to eight months. Examination of the fracture surface showed brittle fatigue cracks, and visual examination of the splines disclosed heavy chatter marks at the root of the spline, with burrs and tears at the fillet area. Evidence found supports the conclusion that the shaft failed as the result of stress in the sharp fillets and rough surfaces at the root of the splines. Cold weather failure occurred sooner than in hot weather because ductile-to-brittle transition temperature of the 1040 steel shaft was too high. Recommendations include redesign of the fillet radius to a minimum of 1.6 mm (0.06 in.) and a maximum surface finish in the spline area of 0.8 microns. Material for the shafts should be modified to a nickel alloy steel, heat treated to a hardness of 28 to 32 HRC before machining.
Book Chapter
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003562
EISBN: 978-1-62708-180-1
..., type of contact and vibration, impact fretting, surface finish, and residual stresses. The form, composition, and role of the debris are briefly discussed. The article also describes the measurement, mechanism, and prevention of fretting wear. It concludes with several examples of failures related...
Abstract
This article reviews the general characteristics of fretting wear in mechanical components with an emphasis on steel. It focuses on the effects of physical variables and the environment on fretting wear. The variables include the amplitude of slip, normal load, frequency of vibration, type of contact and vibration, impact fretting, surface finish, and residual stresses. The form, composition, and role of the debris are briefly discussed. The article also describes the measurement, mechanism, and prevention of fretting wear. It concludes with several examples of failures related to fretting wear.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001601
EISBN: 978-1-62708-235-8
... Abstract Flow forming technology has emerged as a promising, economical metal forming technology due to its ability to provide high strength, high precision, thin walled tubes with excellent surface finish. This paper presents experimental observations of defects developed during flow forming...
Abstract
Flow forming technology has emerged as a promising, economical metal forming technology due to its ability to provide high strength, high precision, thin walled tubes with excellent surface finish. This paper presents experimental observations of defects developed during flow forming of high strength SAE 4130 steel tubes. The major defects observed are fish scaling, premature burst, diametral growth, microcracks, and macrocracks. This paper analyzes the defects and arrives at the causative factors contributing to the various failure modes.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001380
EISBN: 978-1-62708-215-0
... Testing Procedure and Results Surface Examination Surface Finish Metallography Microstructural Analysis Fractography Plating Thickness and Uniformity Visual Mechanical Properties Hardness Macrohardness measurements were taken on a transverse section of the bolt. The results...
Abstract
One of the two AISI 4340 steel pitch horn bolts from the main rotor hub assembly failed while in service. Optical microscope revealed evidence of corrosion pitting in regions adjacent to the fracture. Fractographic examination utilizing a scanning electron microscope revealed multiple crack origins which assumed a “thumbnail” shape and displayed surface morphologies which resulted from intergranular decohesion. Many of the crack sites initiated from corrosion pits. Energy dispersive spectroscope performed on areas within the crack initiation site showed the presence of chlorides. The failure was attributed to stress-corrosion cracking. Short- and long-term recommendations to prevent future failures are given.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001910
EISBN: 978-1-62708-217-4
... analyses were conducted on the individual components: visual examination, surface finish, dimensional verification, magnetic particle inspection, metallography, chemical analysis, microhardness testing, macrohardness testing, coating thickness (where applicable), decarburization measurement (where...
Abstract
Breech bolt assemblies from the Gatling guns used on fighter aircraft failed during firing tests. Metallography of the failed components revealed considerable decarburization which resulted in a loss of surface hardness. It was also determined that the maraging steel components were not in the nitrided condition as was required. This resulted in lower wear and fatigue resistance. These components also had a silicon content nearly double of that specified. The high silicon content lowered the notch tensile strength and toughness of the components.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001030
EISBN: 978-1-62708-214-3
... (0.218 in.) in diameter that contained cracks exhibited grooves and surface finishes rougher than required (125 µm) ( Fig. 3 ). For the associated cracks, the fracture surface was observed to be normal to the short transverse grain direction. Fastener holes without cracks had surface finishes of both...
Abstract
Cracks were discovered between interference-fit fasteners (MoS2-coated Ti-6Al-4V) that had been incorporated into a fighter aircraft primary structural frame (D6ac steel) to enhance structural fatigue life. Examination of sections cut from the cracked frame established that the cracks propagated by stress-corrosion cracking. The cause of cracking was twofold: use of interference-fit fasteners exposed to moisture intrusion from a marine environment and poor hole quality. Failure was intensified by dissimilar-metal contact in the presence of weak acidic electrolyte (dissociated MoS2). Control of machining parameters to prevent formation of brittle martensite, use of galvanically compatible fasteners, and use of an alternate lubricant were recommended.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001287
EISBN: 978-1-62708-215-0
... not been subsequently heat treated or surface hardened. In addition to the tensile and compressive stresses applied to the shaft, bending forces were present. Surface finish and sharp changes in surface geometry can be more important than the nominal cross- sectional area with regard to fatigue...
Abstract
A recurring piston shaft failure problem on the billet-loading tray of an extrusion press was investigated. Two shafts fractured within a period of 10 days. The shaft was machined from normalized EN3 (AISI C1022) steel stock without further treatment. Visual, microstructural, chemical, and mechanical (hardness and tensile properties) analyses of failed shaft specimens were conducted. The examinations showed that the shafts had failed by fatigue. It was recommended that a low-alloy steel (e.g., 3% Ni-Cr) in the hardened and tempered condition and subjected to shot-peening surface-hardening treatment be used. The provision of a stop to reduce bending stresses was also recommended.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001377
EISBN: 978-1-62708-215-0
... into the normally sealed bearing cap chamber surrounding the bolt shank. A complete absence of fractures in bolts from one of the two vendors was attributed primarily to surface residual compressive stresses produced on the bolt shank by a finish machining operation after heat treatment. Shot cleaning, with fine...
Abstract
Sudden and unexplained bearing cap bolt fractures were experienced with reduced-shank design bolts fabricated from 42 CrMo 4 steel, quenched and tempered to a nominal hardness of 38 to 40 HRC. Fractographic analysis provided evidence favoring stress-corrosion cracking as the operating transgranular fracture failure mechanism. Water containing H7S was subsequently identified as the aggressive environment that precipitated the fractures in the presence of high tensile stress. This environment was generated by the chemical breakdown of the engine oil additive and moisture ingress into the normally sealed bearing cap chamber surrounding the bolt shank. A complete absence of fractures in bolts from one of the two vendors was attributed primarily to surface residual compressive stresses produced on the bolt shank by a finish machining operation after heat treatment. Shot cleaning, with fine cast shot, produced a surface residual compressive stress, which eliminated stress-corrosion fractures under severe laboratory conditions.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001583
EISBN: 978-1-62708-217-4
... (205,000) 1,482 (215,000) 55.0 13.0 Typical H1050 [ 2 ] (Long.) 1,241 (180,000) 1,310 (190,000) 55.0 15.0 Surface Roughness Each of the six failed retaining rods were examined with respect to surface roughness. Both the thread roots and the outside surface finishes were examined. ARL...
Abstract
The purpose of this investigation was to determine the root cause of the differences noted in the fatigue test data of main rotor spindle assembly retaining rods fabricated from three different vendors, as part of a Second Source evaluation process. ARL performed dimensional verification, accessed overall workmanship, and measured the respective surface roughness of the rods in an effort to identify any discrepancies. Next, mechanical testing was performed, followed by optical and electron microscopy, and chemical analysis. Finally, ARL performed laboratory heat treatments at the required aging temperature and follow-up mechanical testing.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006935
EISBN: 978-1-62708-395-9
...Process reinforcement capabilities and selected properties Table 1 Process reinforcement capabilities and selected properties Process Reinforcement Limitations to reinforcement Properties Surface finish (++ to −−) Flexural modulus Temperature resistance (trend) Tendency to warp...
Abstract
Manufacturing process selection is a critical step in plastic product design. The article provides an overview of the functional requirements that a part must fulfil before process selection is attempted. A brief discussion on the effects of individual thermoplastic and thermosetting processes on plastic parts and the material properties is presented. The article presents process effects on molecular orientation. It also illustrates the thinking that goes into the selection of processes for size, shape, and design factors. Finally, the article describes how various processes handle reinforcement.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c0047840
EISBN: 978-1-62708-223-5
... (the poor surface finish of the hole is visible). Examination at approximately 10× revealed that the rough surface was the result of the metal having been melted. Metallographic examination (at 250×) of specimens taken through the fracture origin revealed that melting had occurred around the hole...
Abstract
The A2 tool steel mandrel, part of a rolling tool used for mechanically joining two tubes was fractured after making five rolled joints. A 6.4 mm diam hole was drilled by EDM through the square end of the hardened mandrel due to difficulty was experienced in withdrawing the tool. The fracture progressed into the threaded section and formed a pyramid-shape fragment after it was initiated at approximately 45 deg through the hole in the square end. An irregular zone of untempered martensite with cracks radiating from the surface of the hole (result of melting around hole) was revealed by metallographic examination. A microstructure of fine tempered martensite containing some carbide particles was exhibited by the core material away from the hole. Brittle fracture characteristics with beach marks were exhibited by the fracture surfaces which is characteristic of a torsional fatigue fracture. As a corrective measure, the hole through the square end of the mandrel was incorporated into the design of the tool and was drilled and reamed before heat treatment and specified hardness of the threaded portion and square end of the mandrel was reduced.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0045926
EISBN: 978-1-62708-235-8
... is the peel test, in which a layer of material is pulled from its base material and the force required to peel it away is measured. A variation of this test is the tape test, which is used to test surface finish layer adhesion. This microanalytical techniques commonly used to characterize adhesion problems...
Abstract
A batch of bimetal foil/epoxy laminates was rejected because of poor peel strength. The laminates were manufactured by sintering a nickel/phosphorus powder layer to a copper foil, cleaning, then chromate conversion coating the nickel-phosphorus surface, and laminating the nickel-phosphorus side of the clad bimetal onto an epoxy film, so that the end product contained nickel-phosphorus sandwiched between copper and epoxy, with a chromate conversion layer on the epoxy side of the nickel-phosphorus. Peel testing showed abnormally low adhesion strength for the bad batch of peel test samples. Comparison with normal-strength samples using XPS indicated an 8.8% Na concentration on the surface of the bad sample; the good example contained less than 1% Na on the surface. After 15 min of argon ion etching, depth profiling showed high concentrations of sodium were still evident, indicating that the sodium was present before the chromate conversion treatment was performed. A review of the manufacturing procedures showed that sodium hydroxide was used as a cleaning agent before the chromate conversion coating. Failure cause was that apparently the sodium hydroxide had not been properly removed during water rinsing. Thus, recommendation was to modify that stage in the processing.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001747
EISBN: 978-1-62708-217-4
.... Propellers Straightening Surface finish 2219-T6 UNS A92219 2025-T6 UNS A92025 Fatigue fracture Blade damage (such as stone nicks or bruises, dents, pits, insufficiently removed nicks or gouges, and deeply dressed-out zones) can be present before an accident or incident. In a typical instance...
Abstract
This report covers case histories of failures in fixed-wing light airplane and helicopter components. In a 2025-T6 or 2219 aluminum alloy propeller blade that failed near the tip, cracks started on the leading edge at surface damage in the critical area-the zone between 4 and 10 in. from the tip of the blade. Incorrect dressing and inadequate pre-flight inspection were the two main causes. Two other types of propeller blade fatigue failures resulted mainly from propeller straightening operations, usually performed after previous blade bending damage. To eliminate blade tip failures, all surface-damaged material should be removed and polished smooth before further flight. The blade should be correctly dressed. Also, the tachometer should be calibrated to ensure the engine/propeller combination is not operated in the critical speed range at normal cruising speeds.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001801
EISBN: 978-1-62708-241-9
... surface areas. Circumferential notches were most critical in shortening fatigued life [ 5 ]. These notches could emanate from rod processing and/or poor surface finishing or from indentations from the clamping mechanism [ 6–8 ]. One researcher has stated that fatigue occurs at the clamp. Additionally...
Abstract
Both rods in a Harrington rod cervical stent failed after a short time in service. Metallurgical analysis revealed a significant number of notches as well as enlarged grain size in one of the two rods, rough shallow-cracked surfaces along the bend profiles, possible signs of corrosion, and fractures (on both rods) near indentations imparted by retaining clamps. The observations suggest that surface roughness and bending defects initiated cracking that led to the fatigue failure of the compromised rod, followed some time later by the overload fracture of the second rod.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0046222
EISBN: 978-1-62708-217-4
... the finished diameter, ground to finished size, and cadmium plated. The spindle that failed had been overhauled six times and reworked twice. More information on shot peening and methods for measuring the intensity of peening is available in the article "Shot Peening" in Surface Engineering , Volume 5...
Abstract
The spindle of a helicopter-rotor blade fractured after 7383 h of flight service. At every overhaul (the spindle that failed was overhauled six times and reworked twice), any spindle that showed wear was reworked by grinding the shank to 0.1 mm (0.004 in.) under the finished diam. The spindle was then shot peened with S170 shot to an Almen intensity of 0.010 to 0.012 A. Following shot peening, the shank was nickel sulfamate plated to 0.05 mm (0.002 in.) over the finished diam, ground to finished size, and cadmium plated. Visual and stereomicroscopic exam showed faint grinding marks and circumferential grooves on the surface near the fillet at the junction of the shank and fork, which should have been peened over and covered with peening dimples. Evidence found supports the conclusions that the spindle failed in fatigue that originated near the junction of the shank and fork. The nonuniformity of the shot-peened effect on the shank and fillet portions of the spindle resulted from incomplete peeing. The fracture was of the low-stress high-cycle type, initiated by stresses well below the gross yield strength and propagated by thousands of load cycles. No recommendations were made.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001372
EISBN: 978-1-62708-215-0
... material for fluctuating shear stresses is approximately 500 MPa (72 ksi). Considering factors such as surface finish, shape, and dimensions, the factor of safety for infinite fatigue life is estimated as 4. Chemical composition of the material was in accordance with the specified composition, even...
Abstract
A coupling in a line-shaft vertical turbine pump installed in a dam foundation fractured after a very short time. The coupling material was ASTM A582 416 martensitic stainless steel. Visual, macrofractographic, and scanning electron microscopic examination of the coupling showed that the fracture was brittle and was initiated by an intergranular cracking mechanism. The mode of fracture outside the crack initiation zone was transgranular cleavage. No indication of fatigue was found. The failure was attributed to improper heat treatment during manufacture, which resulted in a brittle microstructure susceptible to corrosion. The crack initiated either by stress-corrosion or hydrogen cracking. It was recommended that the couplings in the system be examined for surface cracking and, if present, corrective measures be taken.
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