A fractograph of the failed spring was found to indicate light streaks are parallel to the wire axis. A darker depressed area was visible between the streaks and below the center of the fractograph in which distinct outlines that represent sharp corners in the depressions were revealed by careful examination. A hard material (mill scale) was assumed to have been impressed during drawing of the wire and was broken out during peening, leaving the depressions with sharp-bottomed corners. Spring was concluded to have failed due to a surface defect.

An AISI 4320 H transfer gear shaft that was part of a transmission sustained severe surface damage after 12 h of dynamometer testing at various gearing and torque loads. The damage was characterized by generalized wear and spalling. Examination of a cross section of the shaft that intersected undamaged, burnished, and surface-spalled zones revealed no anomalies in the chemistry, microstructure, or hardness that could have caused the damage. The physical evidence suggested that the operable mechanism was contact fatigue caused by misalignment of the shaft in the assembly.

Several surface-mount chip resistor assemblies failed during monthly thermal shock testing and in the field. The resistor exhibited a failure mode characterized by a rise in resistance out of tolerance for the system. Representative samples from each step in the manufacturing process were selected for analysis, along with additional samples representing the various resistor failures. Visual examination revealed two different types of termination failures: total delamination and partial delamination. Electron probe microanalysis confirmed that the fracture occurred at the end of the termination. Transverse sections from each of the groups were examined metallographically. Consistent interfacial separation was noted. Fourier transform infrared and EDS analyses were also performed. It was concluded that low wraparound termination strength of the resistors had caused unacceptable increases in the resistance values, resulting in circuit nonperformance at inappropriate times. The low termination strength was attributed to deficient chip design for the intended materials and manufacturing process and exacerbated by the presence of polymeric contamination at the termination interface.

Two AISI type 316 stainless steel components intended for use in a reducer section for sodium piping in a fast breeder test reactor were found to be severely corroded—the first soon after pickling, and the second after passivation treatments. Metallographic examination revealed that one of the components was in a highly sensitized condition and that the pickling and passivation had resulted in severe intergranular corrosion. The other component was fabricated from thick plate and, after machining, the outer surface represented the transverse section of the original plate. Pickling and passivation resulted in severe pitting because of end-grain effect. Strict control of heat treatment parameters to prevent sensitization and modification of pickling and passivating conditions for machined components were recommended.

Routine magnetic-particle inspection revealed crack indications in a number of shafts produced from hot-rolled 4130 steel bar. A pronounced indication of this size is cause for rejection if the defect is not eliminated during subsequent machining. A microstructural analysis of the shaft cross section revealed that the crack was approximately 0.5 mm (0.020 in.) deep and oriented in a radial direction. Furthermore, no stringer-type nonmetallic inclusions were observed in the vicinity of the flaw, which did not display the intergranular characteristics of a quench crack. The defect did, however, contain substantial amounts of oxide, which evidently resulted from the hot-working operation. This evidence supports the conclusion that the appearance of this discontinuity, with the long axis parallel to the working direction and radial orientation with regard to depth, strongly suggests a seam produced during rolling. Use of components with surface-defect indications as small as 0.5 mm (0.02 in.) can be risky in certain circumstances. Depending on the orientation of the flaw with respect to applied loads, the nature of the applied forces (for example, cyclic), and the operating environment, such a surface flaw can become the initiating site for a fatigue crack or a corrosion-related failure.

The paper discusses the analysis of a coating defect on a high phosphorus electroless nickel (Ni-11 wt. % P) deposit plated on an aluminum alloy substrate. Preliminary investigations had indicated that the elongated defects were possibly caused by the entrapment of long fibers or particles during the plating. The possible sources of fibers were identified. The SEM/EDS analysis of fibers collected from the air duct filters correlated very well with the defect shape and the EDS profile collected from under the defect site. It appears that the fibers from air duct filters directly above the plating line were blown into the plating tank and getting co-deposited. The paper describes the step-by-step analysis of the defect that led to successful identification of the root cause of the defect.

The connecting end of two forged medium-carbon steel rods used in an application in which they were subjected to severe low-frequency loading failed in service. The fractures extended completely through the connecting end. The surface hardness of the rods was found to be lower than specifications. The fractures were revealed to be in areas of the transition regions that had been rough ground to remove flash along the parting line. The presence of beach marks, indicating fatigue failure, was revealed by examination. The fracture origin was confirmed by the location and curvature of beach marks to be the rough ground surface. An incipient crack 9.5 mm along with several other cracks on one of the fractured rods was revealed by liquid penetration examination. Metallographic examination of the fractured rods indicated a banded structure consisting of zones of ferrite and pearlite. It was established that the incipient cracks found in liquid-penetrant inspection had originated at the surface in the banded region, in areas of ferrite where this constituent had been visibly deformed by grinding. Closer control on the microstructure, hardness of the forgings and smooth finish in critical area was recommended.

Nodular cast iron crankshafts and their main-bearing inserts were causing premature failures in engines within the first 1600 km (1000 mi) of operation. The failures were indicated by internal noise, operation at low pressure, and total seizing. Concurrent with the incidence of engine field failures was a manufacturing problem: the inability to maintain a similar microfinish on the cope and drag sides of a cast main-bearing journal. Investigation supported the conclusion that the root cause of the failure was carbon flotation due to the crankshafts involved in the failures showing a higher-than-normal carbon content and/or carbon equivalent. Larger and more numerous cope side graphite nodules broke open, causing ferrite caps or burrs. They then became the mechanism of failure by breaking down the oil film and eroding the beating material. A byproduct was heat, which assisted the failure. Recommendations included establishing closer control of chemical composition and foundry casting practices to alleviate the carbon-flotation form of segregation. Additionally, some nonmetallurgical practices in journal-finishing techniques were suggested to ensure optimal surface finish.

Several crankshaft failures occurred in equipment that was being used in logging operations in subzero temperatures. Failure usually initiated at a cracked pin oil hole, and the failure origin was approximately 7.6 mm (0.3 in.) from the shaft surface. The holes were produced by gun drilling, giving rise to surface defects. The fracture surface was characteristic of fatigue in that it was flat, relatively shiny, and exhibited beach marks. The crack surface was at a 45 deg angle to the axis of the shaft, indicating dominant tensile stresses. The material was the French designation AFNOR 38CD4 (similar to AISI type 4140H) and was in the quenched-and-tempered condition, with a yield strength of about 760 MPa (110 ksi). It was treated to have compressive surface stresses, and the prior-austenite grain size was ASTM 8. Analysis (visual inspection, stress analyses, and macrographs) supported the conclusion that failure was caused by fatigue stress caused by surface defects in the oil holes. Recommendation includes drilling the oil holes by a technique that essentially eliminates surface defects.

A pushrod made by inertia welding two rough bored pieces of bar stock installed in a mud pump fractured after two weeks in service. The flange portion was made of 94B17 steel, and the shaft was made of 8620 steel. It was disclosed by visual examination that the fracture occurred in the shaft portion at the intersection of a 1.3 cm thick wall and a tapered surface at the bottom of the hole. The fatigue crack was influenced by one-way bending stresses initiated at the inner surface and progressed around the entire inner circumference. A heavily decarburized layer was detected on the inner surface of the flange portion and sharp corner was found at the intersection of the sidewall and bottom of the hole. It was concluded that the stress raiser due to the abrupt section change was accentuated by decarburized layer. As a corrective measure, the design of the pushrod was changed to a one-piece forging and circulation of atmosphere during heat treatment was permitted through a hole drilled in the flange end of the rod to avoid decarburization.

Laser surface mapping of a canister closure weld provided data that was used to generate three-dimensional images of the weld failure. These images were invaluable in that they allowed people who did not have access to the canister to see the anomaly in great detail. This aided in the scientific examination while reducing exposure to the radiologically contaminated canister. Precise measurements from the surface maps provided useful information about the location of weld features that were used in the examination of the weld failure. Laser surface mapping proved to be a powerful addition to the nondestructive examination tools available for surface phenomena.

After a quick-release fitting of an ejection seat broke, an investigation was performed to determine the manner and cause of crack propagation. Most fractography-based investigations aim to characterize only qualitative characteristics, such as the fracture orientation and origin position, topology, and details of interactions with microstructural features. The aim of this investigation was to use quantitative fractography as a tool to extract information, including striation spacing and size of the stretched zone, in order to make a direct correlation with fracture mechanic concepts. As the crack propagated, striations were created on the fracture surface as a result of service-induced load changes. The size of the striations were measured to estimate crack propagation rate. Remaining lifetime estimates were also made. The dimensions of plastically stretched zones found at the tips of the cracks were evaluated using electron micrograph stereo image pairs to characterize local fracture toughness. To complete the failure analysis, nondestructive evaluation, metallographic examination, and chemical investigations were carried out. No secondary cracks could be found. Most of the broken parts showed that the microstructure, the hardness, and the chemical composition of the Al-alloy were within the specification, but some of the cracked parts were manufactured using a different material than that specified.

A crankshaft was overloaded on a test stand and suffered an incipient crack in the crank pin. The crack run generally parallel to the longitudinal axis and branched off at the entrance into the two fillets at the transition to the crank arm. It consisted of many small cracks, all of which propagated at an angle of approximately 45 deg to the longitudinal axis, and therefore were caused by torsion stresses. Neither macroscopic nor microscopic examination determined any material or processing faults. Experience has shown that torsion vibration fractures of this kind usually appear in comparatively short journal pins at high stresses. This crankshaft fracture was an example of the damage that is caused or promoted neither by material nor heat treatment mistakes nor by defects of design or machining, but solely by overstressing.

This article discusses the operating principles, advantages, and limitations of scanning electron microscopy, atomic force microscopy, x-ray photoelectron spectroscopy, and secondary ion mass spectroscopy that are used to analyze the surface chemistry of plastics.

This article provides information on the chemical characterization of surfaces by Auger electron spectroscopy (AES), X-ray photoelectron spectroscopy (XPS), and time-of-flight secondary ion mass spectrometry (TOF-SIMS). It describes the basic theory behind each of these techniques, the types of data produced from each, and some typical applications. The article explains the strengths of AES, XPS, and TOF-SIMS based on data obtained from the surface of a slightly corroded stainless steel sheet.

This article covers the three most popular techniques used to characterize the very outermost layers of solid surfaces: Auger electron spectroscopy (AES), X-ray photoelectron spectroscopy (XPS), and time-of-flight secondary ion mass spectrometry (TOF-SIMS). Some of the more important attributes are listed for preliminary insight into the strengths and limitations of these techniques for chemical characterization of surfaces. The article describes the basic theory behind each of the different techniques, the types of data produced from each, and some typical applications. Also discussed are the different types of samples that can be analyzed and the special sample-handling procedures that must be implemented when preparing to do failure analysis using these surface-sensitive techniques. Data obtained fro