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Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001839
EISBN: 978-1-62708-241-9
... Abstract Several stainless steel coils cracked during a routine unwinding procedure, prompting an investigation to determine the cause. The analysis included optical and scanning electron microscopy, energy-dispersive x-ray spectrometry, and tensile testing. An examination of the fracture...
Abstract
Several stainless steel coils cracked during a routine unwinding procedure, prompting an investigation to determine the cause. The analysis included optical and scanning electron microscopy, energy-dispersive x-ray spectrometry, and tensile testing. An examination of the fracture surfaces revealed a brittle intercrystalline mode of fracture with typical manifestations of clear grain facets. Branched and discrete stepwise microcracks were also found along with unusually high levels of residual hydrogen. Mechanical tests revealed a marked loss of tensile ductility in the defective steel with elongations barely approaching 8%, compared to 50% at the time of delivery weeks earlier. Based on the timing interval and the fact that failure occurred at operating stresses well below the yield point of the material, the failure is being attributed to hydrogen-induced damage. Potential sources of hydrogen are considered as are remedial measures for controlling hydrogen content in steels.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001177
EISBN: 978-1-62708-234-1
... Abstract A solution containing 50 to 70% calcium chloride (pH 7.5 to 8.5) was concentrated by evaporation in a brick-lined vessel by passing steam at a pressure of 15 atmospheres through a system of heating coils made of austenitic stainless steel X 10 Cr-Ni-Mo-Ti 18 12 (Material No. 1.4573...
Abstract
A solution containing 50 to 70% calcium chloride (pH 7.5 to 8.5) was concentrated by evaporation in a brick-lined vessel by passing steam at a pressure of 15 atmospheres through a system of heating coils made of austenitic stainless steel X 10 Cr-Ni-Mo-Ti 18 12 (Material No. 1.4573). After five months one of the coils, which consisted of tubes having a wall thickness of 3.4 mm, developed a leak. Tightly closed cracks were seen on the outer surface of the tube. Further tests with color penetration process revealed multiple branched cracks. Longitudinal section showed that the cracks had started from the outside surface of the tube. Electrolytic etching further showed that they had propagated mainly across the grains. It was concluded that this was a typical case of transcrystalline stress corrosion.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.matlhand.c0048064
EISBN: 978-1-62708-224-2
... Abstract A 10,890-kg coil hook torch cut from 1040 steel plate failed while lifting a load of 13,600 kg after eight years of service. The normal ironing (wear) marks were exhibited by the inner surface of the hook. It was revealed by visual examination that cracking had originated at the inside...
Abstract
A 10,890-kg coil hook torch cut from 1040 steel plate failed while lifting a load of 13,600 kg after eight years of service. The normal ironing (wear) marks were exhibited by the inner surface of the hook. It was revealed by visual examination that cracking had originated at the inside radius of the hook. Beach marks (typical of fatigue fracture) were found extending over approximately 20% of the fracture surface. Numerous cracks were revealed by macroscopic examination of the torch-cut surfaces. It was revealed by macrograph of an etched specimen that the cracks had initiated in a hardened martensitic zone at the torch-cut surface and had extended up to the coarse pearlite structure beneath the martensitic zone. The fatigue fracture was concluded to have initiated in the brittle martensitic surface while failure was contributed by the 25% overload. As a corrective measure, the coil hooks were flame cut from ASTM A242 fine-grain steel plate, ground to remove the material damaged by flame cutting and stress relieved at 620 deg C.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001686
EISBN: 978-1-62708-220-4
... Abstract A root cause failure analysis was performed on a vaporizer coil removed from a horizontal forced circulation vaporizer. The carbon steel coil was wound in a right-hand helix with a coil centerline diameter of about 2 m. The vaporizer was gas fired and used Dowtherm A as the heat...
Abstract
A root cause failure analysis was performed on a vaporizer coil removed from a horizontal forced circulation vaporizer. The carbon steel coil was wound in a right-hand helix with a coil centerline diameter of about 2 m. The vaporizer was gas fired and used Dowtherm A as the heat transfer fluid. Design conditions are based on annular fluid flow to cool the coil wall. NDE, metallographic and fractographic examinations were performed. Numerous, circumferentially oriented, OD initiating cracks were found near the crown for two coils near the non-fired end of the vaporizer. The cracking was confined to the inner diameter of the vaporizer coil at positions from 4:00 to 7:00. The cracking was characterized as transgranular and the fracture surface had beach marks. The failure mechanism was thermal fatigue. The heat transfer calculation predicted that dryout of the coil would occur for coils at the non-fired end of the vaporizer during low flow transients. Dryout results in rapid increase in the tube wall temperature. Thermal cycling of the coil is completed by liquid quenching resulting from resumption of normal flow rates and the return to annular flow. The probable root cause of failure was low flow transient operation.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001012
EISBN: 978-1-62708-234-1
..., the rapid failure, and presence of mercury led to the conclusion of stress-corrosion cracking. It was impossible to remove mercury from the system so carbon steel coils were substituted for the brass ones. The carbon steel coils gave failure-free service for over nine years. Corrosion environments...
Abstract
An interstage radiator gas coil began leaking after only 45 days of service. The original brass coil with several aluminum fins was replaced three times but each replacement lasted less than a day. After removing the fins, leaks were found at circumferential cracks. A section of a tube was removed and split, revealing a series of cracks, evenly spaced. Crack spacing coincided with fin spacing, indicating that stresses incurred during installation of the fins promoted failure. Metallographic examination showed intergranular, branched cracking, characteristic of stress corrosion failures, with the cracks starting on the inside surfaces of the tubes. There was no known corrosive agent in the system, and no other corrosion damage could be found. Qualitative tests and spectrographic analysis gave a positive indication for mercury. The spacing of the cracks, the branched intergranular cracking, the rapid failure, and presence of mercury led to the conclusion of stress-corrosion cracking. It was impossible to remove mercury from the system so carbon steel coils were substituted for the brass ones. The carbon steel coils gave failure-free service for over nine years.
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Published: 01 January 2002
Fig. 14 Torch-cut 1040 steel coil hook that failed by fatigue. (a) Fracture region of the 10,890-kg (12-ton) hook. (b) Macrograph of a nital-etched section showing cracks propagating from the surface (top), which was hardened and embrittled during torch cutting. 7 1 2 ×. (c
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in X-Ray Diffraction Residual Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 01 January 2002
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in Metallurgical Investigation into the Incidence of Delayed Catastrophic Cracking in Low Nickel Austenitic Stainless Steel Coils
> Handbook of Case Histories in Failure Analysis
Published: 01 December 2019
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in Failures of Cranes and Lifting Equipment
> Analysis and Prevention of Component and Equipment Failures
Published: 30 August 2021
Fig. 34 Torch-cut grade 1040 steel coil hook that failed by fatigue. (a) Fracture region of the 10,890 kg (12 ton) hook. (b) Macrograph of a nital-etched section showing cracks propagating from the surface (top), which was hardened and embrittled during torch cutting. Original magnification: 7
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in X-Ray Diffraction Residual-Stress Measurement in Failure Analysis
> Failure Analysis and Prevention
Published: 15 January 2021
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in Use of XRD to Assess Residual Stresses in Steel Springs
> ASM Failure Analysis Case Histories: Automobiles and Trucks
Published: 01 June 2019
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in Fatigue Fracture of a 1040 Steel Coil Hook
> ASM Failure Analysis Case Histories: Material Handling Equipment
Published: 01 June 2019
Fig. 1 Torch-cut 1040 steel coil hook that failed by fatigue. (a) Fracture region of the 10,890-kg (12-ton) hook. (b) Macrograph of a nital-etched section showing cracks propagating from the surface (top), which was hardened and embrittled during torch cutting. 7 1 2 ×. (c
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in Analysis of Hot Rolled Steel Transit Damage
> ASM Failure Analysis Case Histories: Improper Maintenance, Repair, and Operating Conditions
Published: 01 June 2019
Fig. 18 Poor Strapping: (a) Coils of hot rolled steel from Russia, said to have suffered damage during handling during the voyage. Examination revealed that the damage had occurred during transport, but the coils had been rendered vulnerable to damage because of poor strapping at manufacture
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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001169
EISBN: 978-1-62708-220-4
... Abstract Austenitic stainless steel (X 10 Cr-Ni-Mo-Ti 18 10, Material No. 1.4571) cooling coils were found leaking in 15 spots after eight weeks of service in an apparatus in which ammonium sulfide solution was converted into ammonium sulfate. The external temperature of the coil...
Abstract
Austenitic stainless steel (X 10 Cr-Ni-Mo-Ti 18 10, Material No. 1.4571) cooling coils were found leaking in 15 spots after eight weeks of service in an apparatus in which ammonium sulfide solution was converted into ammonium sulfate. The external temperature of the coil was approximately 175 deg C and it was cooled by water at 3 atm. Examination of two sections of the coil showed pinhead size pitting cavities at the exterior surface and partially parallel and partially angled array of fine cracks on external as well as the internal surfaces of the bend. Metallographic examination conducted on longitudinal and transverse sections showed predominantly transcrystalline cracks, originated from the pits at the external surfaces of the pipe. Their appearance suggested they were stress corrosion cracks that occur in austenitic steels under the combined effect of stresses and certain corrosion agents, especially chlorides. If chlorides were absent, hydrogen sulfide which causes similar pitting and is capable of causing cracks could be suspected. Favorable state of stresses, which could be residual or due to heat treating, bending or straightening operations, would be recommended for better behavior of the container.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001403
EISBN: 978-1-62708-220-4
... distributing units Heating coils Vessels 18Cr-8Ni-3Mo Stress-corrosion cracking Transgranular fracture This case study concerns a process vessel heating coil, which was fabricated from 3 in. O.D. × 12 s.w.g. austenitic stainless steel. The coil consisted of several 3 ft. diameter turns...
Abstract
A process vessel heating coil, consisting of several 3 ft diam turns, was supplied with steam at 400 psi and a temperature of 343 deg C (650 deg F). At bi-weekly intervals well water was introduced to effect rapid cooling of the contents. After about eight months, leakage developed from a circumferential crack on the underside of the uppermost turn. Shorter cracks were found at a similar location on the bottom turn, and further leakage occurred at pinhole perforations adjacent to the crack in the top turn and near to a butt-weld in the coil. Microscopic examination revealed that the cracks were predominantly of the intergranular variety. In addition, transgranular cracks were present. Material was an austenitic stainless steel of the type specified but the absence of columbium and titanium in significant amounts showed that it was not stabilized against intergranular carbide precipitation. The transgranular cracks indicated that failure was due partly to stress-corrosion. It was concluded that the chlorides provided the main corrodent for both the stress and intercrystalline-corrosion cracking.
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in Analysis of Hot Rolled Steel Transit Damage
> ASM Failure Analysis Case Histories: Improper Maintenance, Repair, and Operating Conditions
Published: 01 June 2019
, caused by rubbing during coiling. Such damage is not possible during transport; (b and c) serrated edges on hot rolled steel coil. This condition is a natural result of hot rolling, but it should be trimmed away at the steel mill prior to shipping.
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in Metallurgical Investigation into the Incidence of Delayed Catastrophic Cracking in Low Nickel Austenitic Stainless Steel Coils
> Handbook of Case Histories in Failure Analysis
Published: 01 December 2019
Fig. 12 Cause and effect analysis into the incidence of delayed catastrophic cracking in low nickel austenitic stainless steel coils
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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.usage.c9001608
EISBN: 978-1-62708-236-5
... test sheet is shown in Fig. 3c . Fig. 3 (a) Hot rolled coils after exposure for 2–4 weeks and 10 weeks in Malaysia; (b) Hot rolled coils after exposure for 34 weeks in Malaysia; (c) Corrosion in 10 days on clean, descaled steel exposed outdoors in Malaysia Insurance of Hot Rolled Steel...
Abstract
Investigation of alleged corrosion damage to hot-rolled steel during transit requires metallurgical, chemical, and corrosion knowledge. Familiarity with non-destructive techniques and sampling procedures is necessary. A complete record of shipment history is also required, including the purchasing specifications and observations and photographs taken during surveys enroute. A frequent conclusion of such investigations is that the alleged corrosion is of no significance or did not occur during the voyage.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c9001646
EISBN: 978-1-62708-219-8
... if broken. The interlock also inhibits the ingress of moisture into the rope and the egress of lubricant from the rope, thus reducing the chances of internal corrosion. By virtue of their design, locked coil wire ropes have a greater area of steel in proportion to the diameter than other types of ropes...
Abstract
Locked coil wire ropes, by virtue of their unique design and construction, have specialized applications in aerial ropeways, mine hoist installations, suspension bridge cables, and so forth. In such specialty ropes, the outer layer is constructed of Z-profile wires that provide not only effective interlocking but also a continuous working surface for withstanding in-service wear. The compact construction and fill-factor of locked coil wire ropes make them relatively impervious to the ingress of moisture and render them less vulnerable to corrosion. However, such ropes are comparatively more rigid than conventional wire ropes with fiber cores and therefore are more susceptible to the adverse effects of bending stresses. The reasons for premature in-service wire rope failures are rather complex but frequently may be attributed to inappropriate wire quality and/or abusive operating environment. In either case, a systematic investigation to diagnose precisely the genesis of failure is desirable. This article provides a microstructural insight into the causes of wire breakages on the outer layer of a 40 mm diam locked coil wire rope during service. The study reveals that the breakages of Z-profile wires on the outer rope layer were abrasion induced and accentuated by arrays of fine transverse cracks that developed on a surface martensite layer.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.matlhand.c0048026
EISBN: 978-1-62708-224-2
... Abstract The 11 mm diam 8 x 19 fiber-core rope, constructed from improved plow steel wire, on the cleaning-line crane failed while lifting a normal load of coils after five weeks of service. Several broken wires and fraying of the fiber core were revealed by visual examination of a section...
Abstract
The 11 mm diam 8 x 19 fiber-core rope, constructed from improved plow steel wire, on the cleaning-line crane failed while lifting a normal load of coils after five weeks of service. Several broken wires and fraying of the fiber core were revealed by visual examination of a section of the wire rope adjacent to the fracture. Fatigue cracks originating from both sides of the wire were revealed by microscopic examination of a longitudinal section of a wire. The diam of the sheave on the bale (27 cm) was found to be slightly below that specified for the 11 mm diam rope. It was observed that the sudden shock received by the hook in rolling the coils over the edge of the rinse tank after pickling caused vibration which was most severe at the clamped end of the rope. It was concluded that this caused the fatigue failure of the rope. As a corrective measure, the diam of the sheave was increased to 33 cm and pitched roll plates were installed between the tanks where rolling of coils was required.
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