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scanning electron fractography
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Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001052
EISBN: 978-1-62708-214-3
... followed a multidirectional/circular pattern, occasionally chipping off the convolutions, an indication of high-resonance fatigue-type cracking. Scanning electron fractography showed fatigue striations throughout the fracture surface. The microstructure consisted of relatively large grains and an abnormal...
Abstract
A failure analysis was conducted to determine the cause of recurring failure of flexible bellows in an exhaust hose assembly. The bellows were made of type 321 stainless steel. Visual examination showed that cracks followed a path along the seam weld in the bellows. Most of the cracks followed a multidirectional/circular pattern, occasionally chipping off the convolutions, an indication of high-resonance fatigue-type cracking. Scanning electron fractography showed fatigue striations throughout the fracture surface. The microstructure consisted of relatively large grains and an abnormal degree of titanium-base stringers. Wall thickness was about 0.15 mm (0.006 in.) underside. It was concluded that the high vane pass frequency excited the natural vibration of the bellows to a higher resonance and cracked the bellows after a relatively short service period. The assembly was redesigned, and no further cracking occurred.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001828
EISBN: 978-1-62708-241-9
... to establish the root cause of the failure included chemical and metallurgical analysis, scanning electron fractography, mechanical property testing, finite element analysis of the shrink fitted journal, and a design review of the assembly fits. The journal failure was attributed to corrosion fatigue...
Abstract
A heat transport pump in a heavy water reactor failed (exhibiting excessive vibration) during a restart following a brief interruption in coolant flow due to a faulty valve. The pump had developed a large crack across the entire length of a bearing journal. An investigation to establish the root cause of the failure included chemical and metallurgical analysis, scanning electron fractography, mechanical property testing, finite element analysis of the shrink fitted journal, and a design review of the assembly fits. The journal failure was attributed to corrosion fatigue. Corrective actions to make the journals less susceptible to future failures were implemented and the process by which they were developed is described.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003536
EISBN: 978-1-62708-180-1
... that are based on fracture profilometry. This is followed by a section describing the methods based on scanning electron microscope fractography. The article also addresses procedures for three-dimensional fracture surface reconstruction. In each case, sufficient methodological details, governing equations...
Abstract
The quantitative characterization of fracture surface geometry, that is, quantitative fractography, can provide useful information regarding the microstructural features and failure mechanisms that govern material fracture. This article is devoted to the fractographic techniques that are based on fracture profilometry. This is followed by a section describing the methods based on scanning electron microscope fractography. The article also addresses procedures for three-dimensional fracture surface reconstruction. In each case, sufficient methodological details, governing equations, and practical examples are provided.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003533
EISBN: 978-1-62708-180-1
... discussed. display equipment electron optical column fractography microstructure sample preparation scanning electron microscopy signal detection vacuum system THE SCANNING ELECTRON MICROSCOPE (SEM) is one of the most versatile instruments for investigating the microstructure of metallic...
Abstract
The scanning electron microscopy (SEM) is one of the most versatile instruments for investigating the microstructure of metallic materials. This article highlights the development of SEM technology and describes the operation of basic systems in an SEM, including the electron optical column, signal detection and display equipment, and vacuum system. It discusses the preparation of samples for observation using an SEM and describes the application of SEM in fractography. If the surface remains unaffected and undamaged by events subsequent to the actual failure, it is often a simple matter to determine the failure mode by the use of an SEM. In cases where the surface is altered after the initial failure, the case may not be so straightforward. The article presents typical examples that illustrate these points. Image dependence on the microscope type and operating parameters is also discussed.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006769
EISBN: 978-1-62708-295-2
... should be given the opportunity to examine the specimen before it is prepared for examination in the SEM or altered in any other way. Application of Scanning Electron Microscope in Fractography Fractography is one of the most common applications of SEM. The large depth of focus, the possibility...
Abstract
The scanning electron microscope (SEM) is one of the most versatile instruments for investigating the microscopic features of most solid materials. The SEM provides the user with an unparalleled ability to observe and quantify the surface of a sample. This article discusses the development of SEM technology and operating principles of basic systems of SEM. The basic systems covered include the electron optical column, signal detection and display equipment, and the vacuum system. The processes involved in the preparation of samples for observation using an SEM are described, and the application of SEM in fractography is discussed. The article covers the failure mechanisms of ductile failure, brittle failure, mixed-mode failure, and fatigue failure. Lastly, image dependence on microscope type and operating parameters is also discussed.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.matlhand.c0091092
EISBN: 978-1-62708-224-2
.... Investigation (visual inspection, inspection records review, optical and scanning electron microscopy, and fractography) supported the conclusion that the fracture mode for both shafts was low-cycle rotating-bending fatigue initiating and propagating by combined torsional and reverse bending stresses...
Abstract
A 60.3 mm (2.375 in.) diam drive shaft in the drive train of an overhead crane failed. The part submitted for examination was a principal drive shaft that fractured near a 90 deg fillet where the shaft had been machined down to 34.9 mm (1.375 in.) to serve as a wheel hub. A 9.5 mm (0.375 in.) wide x 3.2 mm (0.125 in.) deep keyway was machined into the entire length of the hub, ending approximately 1.6 mm (0.062 in.) away from the 90 deg fillet. A second shaft was also found to have cracked at a change in diameter, where it was machined down to serve as the motor drive hub. Investigation (visual inspection, inspection records review, optical and scanning electron microscopy, and fractography) supported the conclusion that the fracture mode for both shafts was low-cycle rotating-bending fatigue initiating and propagating by combined torsional and reverse bending stresses. Recommendations included replacing all drive shafts with new designs that eliminated the sharp 90 deg chamfers in favor of a more liberal chamfer, which would reduce the stress concentration in these areas.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001770
EISBN: 978-1-62708-241-9
... were subsequently welded over with 308 stainless steel filler wire and the base plate was replaced with new material. Soon after, the tank began leaking along the weld bead, triggering a full-scale investigation; spectroscopy, optical and scanning electron microscopy, fractography, SEM-EDS analysis...
Abstract
A storage tank had been in service at a petrochemical plant for 13 years when inspectors discovered cracks adjacent to weld joints and in the base plate near the foundation. The tank was made from AISI 304 stainless steel and held styrene monomer, a derivative of benzene. The cracks were subsequently welded over with 308 stainless steel filler wire and the base plate was replaced with new material. Soon after, the tank began leaking along the weld bead, triggering a full-scale investigation; spectroscopy, optical and scanning electron microscopy, fractography, SEM-EDS analysis, and microhardness, tensile, and impact testing. The results revealed transgranular cracks in the HAZ and base plate, likely initiated by stresses developed during welding and the presence of chloride from seawater used in the plant. It was also found that the repair weld was improperly done, nor did it include a postweld heat treatment to remove weld sensitization and minimize residual stresses.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001041
EISBN: 978-1-62708-214-3
... section and an internal fillet-welded diaphragm. Sections from each of the cross members were subjected to a complete analysis, including chemical analysis, magnetic particle testing, mechanical testing, scanning electron microscope/fractography, and metallography. The primary mode of failure was found...
Abstract
Four truck cross members intended for use in heavy-duty transport trucks were investigated. Two of the members had cracked on a prototype vehicle and two had been fatigue tested in the laboratory. The cross members were fabricated from SAE 950X plate and consisted of a formed channel section and an internal fillet-welded diaphragm. Sections from each of the cross members were subjected to a complete analysis, including chemical analysis, magnetic particle testing, mechanical testing, scanning electron microscope/fractography, and metallography. The primary mode of failure was found to be fatigue cracking that initiated at the toes of the fillet welds. Secondary fatigue cracking occurred at the torque rod mounting holes. Failure was attributed to cyclic stresses at the weld toes that exceeded the lowered fatigue strength at this location. A design change that eliminated the fillet welds alleviated the problem.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001075
EISBN: 978-1-62708-214-3
... Abstract Several type 316L stainless steel wires in an electrostatic precipitator at a paper plant fractured in an unexpectedly short time. Failed wires were examined using optical and scanning electron microscope, and hardness tests were conducted. Fractography clearly established...
Abstract
Several type 316L stainless steel wires in an electrostatic precipitator at a paper plant fractured in an unexpectedly short time. Failed wires were examined using optical and scanning electron microscope, and hardness tests were conducted. Fractography clearly established that fracture was caused by fatigue originating at corrosion pits on the surface of the wire. It was recommended that higher-molybdenum steel in the annealed condition be used to combat pitting corrosion.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.med.c9001606
EISBN: 978-1-62708-226-6
... Abstract Failures of four different 300-series austenitic stainless steel biomedical fixation implants were examined. The device fractures were observed optically, and their surfaces were examined by scanning electron microscopy. Fractography identified fatigue to be the failure mode for all...
Abstract
Failures of four different 300-series austenitic stainless steel biomedical fixation implants were examined. The device fractures were observed optically, and their surfaces were examined by scanning electron microscopy. Fractography identified fatigue to be the failure mode for all four of the implants. In every instance, the fatigue cracks initiated from the attachment screw holes at the reduced cross sections of the implants. Two fixation implant designs were analyzed using finite-element modeling. This analysis confirmed the presence of severe stress concentrations adjacent to the attachment screw holes, the fatigue crack initiation sites. Conclusions were reached regarding the design of these types of implant fixation devices, particularly the location of the attachment screw holes. The use of austenitic stainless steel for these biomedical implant devices is also addressed. Recommendations to improve the fixation implant design are suggested, and the potential benefits of the substitution of titanium or a titanium alloy for the stainless steel are discussed.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c9001733
EISBN: 978-1-62708-225-9
... obtained. 1 A wealth of information about the microscopic aspects of a failure exists on a fracture surface. 2 Electron fractography has become a valuable tool for use in analyzing a fracture surface. Ref 3 , 4 , 5 , 6 , 7 The scanning electron microscope (SEM) offers resolution better than...
Abstract
Drive cables from a rubber processing machine were failing in less than 8 h of operation, the expected service life being much greater than 100 h. Comparison cables were tested to failure under known stress conditions, including tensile overload, torsional loading, reversed bending alternating stress, and buckling (compressive) cyclic loading. The mode of failure was found to be reversed bending fatigue caused by drive cables moving over guide pulleys of small radii. Modifications of the machinery and drive cable system were suggested.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001042
EISBN: 978-1-62708-214-3
... to be sound. No lamination was found, only minor nonmetallic inclusions that are normal in a stainless steel. Testing Procedure and Results Surface Examination Scanning Electron Microscopy/Fractography Scanning electron microscopy/fractography ( Fig. 1 ) showed only striations and arrest patterns...
Abstract
Failure occurred in a type 304 stainless steel leaf spring attached to the undercarriage assembly of an airport shuttle train. Failure analysis showed that the fracture was caused by low-cycle, reversed bending fatigue. The stresses leading to failure were imposed by poor alignment. It was recommended that improved assembly procedures be used and that, if another failure occurred, a steel of higher fatigue strength be used.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001144
EISBN: 978-1-62708-217-4
.... Fractographic analysis of the fractures by scanning electron microscopy revealed striations typical of fatigue, as shown in Fig. 3 . Each striation usually corresponds to a single load cycle ( 1 , 2 , 3 ). The striation pattern indicated random loading with additional distinct spike load indications...
Abstract
A helicopter was hovering approximately 10 ft above a ship when one spar section failed explosively. Visual inspection revealed a crack had progressed through one member of a dual spar plate assembly at a fold pin lug hole. The remaining spar plate carried the blade load until the aircraft was landed. The helicopter main rotor blade spar fracture was analyzed by conventional and advanced computerized fractographic techniques. Digital fractographic Imaging Analysis of theoretical and actual fracture surfaces was applied for automatic detection of fatigue striation spacing. The approach offered a means of quantification of fracture features, providing for objective fractography.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001038
EISBN: 978-1-62708-214-3
... not be released for testing. Therefore, the investigation was limited to nondestructive means, including photographic examination (visually and at 10× magnification) of the wheel and replication of pertinent fracture surfaces for further study via scanning electron microscope (SEM) fractography. Visual...
Abstract
The rear outside wheel of an over-the-road 18-wheel tractor-trailer failed at its bolt holes, permitting the tire and wheel to separate from the hub. Failure analysis was conducted using photographic examination of actual fracture surfaces and SEM examination of fracture replicas. The examinations indicated that fatigue cracks had originated at the rim backside and propagated to the rim midsection. Catastrophic failure occurred at a final overland. Fatigue fracture of the wheel rim was attributed to cyclic loading created by improper wheel mounting of a spare tire.
Image
Published: 30 August 2021
Fig. 14 (a) Brittle fisheyes appear as bright spots in gray ductile matrix. Original magnification: 1.7×. (b) Mixed-mode fracture in as-welded three-point bend-test specimen at room temperature (scanning electron microscope). Optical fractography. Original magnification: 1500×
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Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001097
EISBN: 978-1-62708-214-3
... mode was fatigue. Scanning Electron Microscopy/Fractography Transverse cross sections of the broken screws were metallurgically polished. Figure 2 shows the plan view of the surface of a broken screw. Figure 3 is a magnified side view of the fracture surface, revealing the corrosion pits...
Abstract
Two type 316L stainless steel orthopedic screws broke approximately 6 weeks after surgical implant. The screws had been used to fasten a seven-hole narrow dynamic compression plate to a patient's spine. The broken screws and screws of the same vintage and source were examined using macrofractography, SEM fractography, and hardness testing. Fractography established that fracture was by fatigue and that the fatigue cracking originated at corrosion pits. Hardness while below specification, still indicated that the screws were in the cold-worked condition and notch sensitive during fatigue loading. Use of a steel with a higher molybdenum content (317L) in the annealed condition was recommended.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.med.c0048400
EISBN: 978-1-62708-226-6
... a tension band fixation containing a cerclage wire, two screws, and washers beneath the screw heads. See also Fig. 2 . Fig. 2 Intercrystalline corrosion of a type 304 stainless steel cerclage wire. (a) Broken cerclage wire. (b) Energy-dispersive x-ray analysis under the scanning electron...
Abstract
Cerclage wire, which was used with two screws and washers for a tension band in a corrective internal fixation, was found broken at several points and corroded after nine months in service. The material was examined using energy-dispersive x-ray analysis and determined not to be in compliance with standards (type 304 stainless steel without molybdenum). The screws and washers were found to be made of remelted implant-quality type 316L stainless steel and were intact. Signs of sensitization, characterized by chromium carbide precipitates at the grain boundaries, were revealed by the microstructure. Intercrystalline corrosion with pitted grains was indicated by SEM fractography. Improper heat treatment of the steel was interpreted to have led to intercrystalline corrosion and implant separation.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006776
EISBN: 978-1-62708-295-2
... of materials since the 1950s, and scanning electron microscopes (SEMs) have been commercially available since 1965 ( Ref 23 ). Today (2020), the SEM is standard equipment for any laboratory performing failure analysis and fractography. The SEM offers significantly superior resolution and depth of field...
Abstract
Fatigue failure of engineering components and structures results from progressive fracture caused by cyclic or fluctuating loads. Fatigue is an important potential cause of mechanical failure, because most engineering components or structures are or can be subjected to cyclic loads during their lifetime. This article focuses on fractography of fatigue. It provides an abbreviated summary of fatigue processes and mechanisms: fatigue crack initiation, fatigue crack propagation, and final fracture,. Characteristic fatigue fracture features that can be discerned visually or under low magnification are then described. Typical microscopic features observed on structural metals are presented subsequently, followed by a brief discussion on fatigue in polymers and polymer-matrix composites.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001290
EISBN: 978-1-62708-215-0
.... Macrofractography/Scanning Electron Fractography The fragments were examined in a stereomicroscope and in a scanning electron microscope (SEM). The features observed on the fracture edges and on the surfaces of the fragments are shown in Fig. 3 . These features were pronounced in the fragments obtained from...
Abstract
Damage to a passenger aircraft that resulted from a midair explosion and subsequent emergency landing was investigated to determine the cause and location of the explosion. Extensive damage had occurred in the front toilet and cockpit areas and to the undercarriage and underside of the aircraft. Fractographic and surface examination of metal fragments (stainless steel and aluminum alloy) from damaged areas indicated that the accident was caused by an explosion in the front toilet. A reconstruction exercise confirmed this conclusion. Damage to the undercarriage and underside resulted from the emergency landing.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001090
EISBN: 978-1-62708-214-3
... to fracture. Fig. 1 Failed stainless steel flexible connector. Fig. 2 Inside view of outer end of connector where the bellows fractured. Fig. 3 Portion of the bellows containing the fracture. Surface Examination Scanning Electron Microscopy/Fractography SEM examination...
Abstract
A stainless steel flexible connector failed after a short period of service. Visual examination of the failed part revealed that a fracture had occurred in the thin-walled stainless steel bellows brazed into the flanges at each end. Surface examination by SEM fractography showed that failure of the bellows occurred via fatigue. The crack in the bellows had widened considerably after the fracture, and the bellows had been severely compressed on the fracture side prior to failure. Based on these observations, it was concluded that bellows had been damaged prior to installation. The damage resulted in high mean tensile stresses upon which were superimposed cyclic stresses, with fatigue failure the final result.
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