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Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006838
EISBN: 978-1-62708-329-4
... and fabrication sources of failure, addresses the key factors in production and quality control, and explains failure analysis of AM parts. binder jet sintering directed energy deposition failure analysis metal products metallurgical characteristics powder bed fusion quality assurance ADDITIVE...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001674
EISBN: 978-1-62708-234-1
... that the preferential attack of the gold was due to HCN formed by decomposition of the explosive powder at high temperatures. Other associated reactions were also observed including the subsequent attack of the solder by the gold corrosion product and degradation of the plastic header. Bridgewires Detonators...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001387
EISBN: 978-1-62708-215-0
... of black powder was also present on the bottom or the cell. SEM/EDX studies of the outer and inner surfaces of the gouged anode showed the presence of iron globules at the interface between the gouged and the unattacked anode. The chemical composition of the black powder was determined to be primarily iron...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c9001548
EISBN: 978-1-62708-219-8
... of wood samples, including a sample wherein the fire retardant paint was removed. Analysis of the corrosion product, which was a fine white powder between the aluminum and plywood. This had not been done before. Contact the manufacturer of the fire retardant paint for more information regarding...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001712
EISBN: 978-1-62708-234-1
...Abstract Abstract A failure analysis was conducted in late 1996 on two rolls that had been used in the production of iron and steel powder. The rolls had elongated over their length such that the roll trunnions had impacted with the furnace wall refractory. The result was distortion and bowing...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0045926
EISBN: 978-1-62708-235-8
...Abstract Abstract A batch of bimetal foil/epoxy laminates was rejected because of poor peel strength. The laminates were manufactured by sintering a nickel/phosphorus powder layer to a copper foil, cleaning, then chromate conversion coating the nickel-phosphorus surface, and laminating...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001560
EISBN: 978-1-62708-217-4
... of testing in the residue paste was (1) linear polarization, (2) cathodic polarization, and (3) anodic polarization. X-Ray Diffraction and Elemental Analysis To identify the compounds and aggressive agent or agents present in the residue product both powder x-ray diffraction and microprobe analysis...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c0091853
EISBN: 978-1-62708-223-5
...Abstract Abstract A 230 mm (9 in.) diameter disk attrition mill was scheduled to grind 6.35 mm (0.25 in.) diameter quartz particles to a 0.075 mm (0.003 in.) diameter powder. Due to severe wear on the grinding plates, however, the unit was unable to complete the task of grinding the rock...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001390
EISBN: 978-1-62708-215-0
... into pieces. Some of the packings were also damaged. Pertinent Specifications The heaters use nichrome wire as the heating element, magnesia powder as insulating material, and type 304L stainless steel as sheathing material. The heaters were in coils of various lengths (5 to 30 m, or 15 to 100 ft...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c9001702
EISBN: 978-1-62708-219-8
... as a result of the expansive forces of the corrosion product. Once this happens, bridges must be either repaired or replaced. A 1993 report to congress stated that of the 575,413 bridges in the United States 44% are either structurally deficient or should be posted for weight restrictions ( 1 ). Bridges...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001843
EISBN: 978-1-62708-241-9
... powder and the plating material had separated from the substrate in many areas. Several connectors, including some that had been in service, were examined to determine what caused the change. The order stated that the connectors were to be coated with a layer of tin-bismuth (2% Bi) to guard against tin...
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001127
EISBN: 978-1-62708-214-3
... noninvasive energy-dispersive x-ray spectrum techniques in a scanning electron microscope. The coating was identified as zinc ( Fig. 6 ). Fig. 6 Energy-dispersive x-ray spectrum of white residue found in float ball cavities and on extension. Zinc oxide, a white water-insoluble powder, is used...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001342
EISBN: 978-1-62708-215-0
... and a white powdery by-product ( Fig. 5 ). Removal of the inner liner revealed a cracked portion ( Fig. 6 .) Fig. 5 Corrosion particles on surface of bellows (white powder) Fig. 6 Inner surface of bellows, showing circumferential crack Testing Procedure and Results Nondestructive...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001364
EISBN: 978-1-62708-215-0
... using wavelength dispersive spectroscopy (WDS) to verify the presence of fluorine. WDS can be used to detect elements of atomic number 5 (boron) and greater and has a detection limit on the order of 100 ppm. Crystalline compounds in the deposit samples were identified using powder x-ray diffraction...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001348
EISBN: 978-1-62708-215-0
..., residual stress measurements; 6, Chemical analysis Visual Examination of General Physical Features Visual examination of the first tank revealed red corrosion products on the surface where the dished ends were joined to the main body. These products, in the form of lines, propagated toward...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003507
EISBN: 978-1-62708-180-1
... powder metallurgy (P/M). A good review of powder metallurgy with coverage relevant to failure analysis of P/M forms is in Ref 2 . Imperfections in Wrought Forms Various terms are used to describe surface and subsurface imperfections in wrought product. The meaning of terms can vary by location...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001666
EISBN: 978-1-62708-229-7
... possibly related to chloride or sulphate ion steam contaminants. Subsequent sectioning and conventional metallography confirmed both the validity of the conclusions and the replication techniques. Corrosion products Field metallography Intergranular corrosion Turbine discs 2.5Ni-Cr-Mo-V Stress...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001713
EISBN: 978-1-62708-220-4
...Abstract Abstract On 21 April 1995, the contents of a large blender (6 cu m) reacted and caused an explosion that killed and injured a number of workers at a plant in Lodi, NJ. A mixture of sodium hydrosulfite and aluminum powder was being mixed at the time of the accident. This report focuses...
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006826
EISBN: 978-1-62708-329-4
..., and/or machining parameters cause workpiece rejection, catastrophic cutting tool failure, and/or workpiece failure during machining. Metallurgical factors contributing to (in-process) workpiece failures: Physical metallurgy effects on workpiece failures during production machining Machined part (in-service...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001784
EISBN: 978-1-62708-241-9
... near the socket surfaces showing brittle fracture are possibly due to carburized layer. Figure 5 shows fractured core of the socket indicating loose spherical particles showing poor sintering step in powder metallurgy (PM) production process or inclusion particles. Figures 6 and 7 show dimples...