Immediately after installation, leakage was observed at the mounting surface of several rebuilt hydraulic actuators that had been in storage for up to three years. At each joint, there was an aluminum alloy spacer and a vellum gasket. The mounting flanges of the steel actuators had been nickel plated. During assembly of the actuators a lubricant containing molybdenum disulfide had been applied to the gaskets as a sealant. The vellum gasket was found to be electrically conductive, and analysis (visual inspection, 500x unetched micrographs, galvanic action testing, and x-ray diffraction) supported the conclusions that leakage was the result of galvanic corrosion of the aluminum alloy spacers while in storage. The molybdenum disulfide was apparently suspended in a volatile water-containing vehicle that acted as an electrolyte between the aluminum alloy spacer and the nickel-plated steel actuator housing. Initially, the vellum gasket acted as an insulator, but the water-containing lubricant gradually impregnated the vellum gasket, establishing a galvanic couple. Recommendations included discontinuing use of molybdenum disulfide lubricant as a gasket sealer, and assembling the actuators using dry vellum gaskets.

Several cases of embrittlement failure are analyzed, including liquid-metal embrittlement (LME) of an aluminum alloy pipe in a natural gas plant, solid metal-induced embrittlement (SMIE) of a brass valve in an aircraft engine oil cooler, LME of a cadmium-plated steel screw from a crashed helicopter, and LME of a steel gear by a copper alloy from an overheated bearing. The case histories illustrate how LME and SMIE failures can be diagnosed and distinguished from other failure modes, and shed light on the underlying causes of failure and how they might be prevented. The application of LME as a failure analysis tool is also discussed.

Two clevis-head self-retaining bolts used in the throttle-control linkage of a naval aircraft failed on the aircraft assembly line. Specifications required the bolts to be heat treated to a hardness of 39 to 45 HRC, followed by cleaning, cadmium electroplating, and baking to minimize hydrogen embrittlement. The bolts broke at the junction of the head and shank. The nuts were, theoretically, installed fingertight. The failure was attributed to hydrogen embrittlement that had not been satisfactorily alleviated by subsequent baking. The presence of burrs on the threads prevented assembly to finger-tightness, and the consequent wrench torquing caused the actual fractures. The very small radius of the fillet between the bolt head and the shank undoubtedly accentuated the embrittling effect of the hydrogen. To prevent reoccurrence, the cleaning and cadmium-plating procedures were stipulated to be low-hydrogen in nature, and an adequate post plating baking treatment at 205 deg C (400 deg F), in conformity with ASTM B 242, was specified. A minimum radius for the head-to-shank fillet was specified at 0.25 mm (0.010 in.). All threads were required to be free of burrs. A 10-day sustained-load test was specified for a sample quantity of bolts from each lot.

A type 316L stainless steel angled plate failed. The fatigue fracture was found to have occurred at a plate hole. Symmetric cyclic bending forces were revealed by the fatigue damage at the fracture edge at the top surface of the plate. Fatigue striations and slip bands produced on the surface during cyclic loading were observed. The material was showed by the deformation structure to be in the cold-worked condition and was termed to not be the cause of the implant failure.

Stainless steel is frequently used for bone fracture fixation in spite of its sensitivity to pitting and cracking in chloride containing environments (such as organic fluids) and its susceptibility to fatigue and corrosion fatigue. A 316L stainless steel plate implant used for fixation of a femoral fracture failed after only 16 days of service and before bone callus formation had occurred. The steel used for the implant met the requirements of ASTM Standard F138 but did contain a silica-alumina inclusion that served as the initiation point for a fatigue/corrosion fatigue fracture. The fracture originated as a consequence of stress intensification at the edge of a screw hole located just above the bone fracture; several fatigue cracks were also observed on the opposite side of the screw hole edge. The crack propagated in a brittle-like fashion after a limited number of cycles under unilateral bending. The bending loads were presumably a consequence of leg oscillation during assisted perambulation.

A few Cr-Mo steel piston rods from different production batches were found identically cracked in the eye end near the radius after chrome plating and baking treatment. Two of them cracked in the plating stage itself instantly broke on slight tapping. Cracking initiated from the outer base surface of the forked eye end. The 40 mm diam forged piston rods were subjected to plating after heavy machining on the part without any stress-relieving treatment. Also, time lapses between plating and baking were varied from 3 to 11 h. The brittle cracking along forked eye-end radius portion was attributed to hydrogen embrittlement that occurred during chrome plating.

Fretting and fretting corrosion at the contact area between the screw hole of a type 316LR stainless steel bone plate and the corresponding screw head was studied. The attack on the 316LR stainless steel was only shallow. Mechanical grinding and polishing structures were exhibited by a large portion of the contact area. Fine corrosion pits in the periphery were observed and intense mechanical material transfer that can take place during fretting was revealed. Smearing of material layers over each other during wear was observed and attack by pitting corrosion was interpreted to be possible.

A large portion of the four-hole Lane plate disintegrated and consisted mainly of corrosion products after remaining in the body for 26 years. Transformation structures and carbides were exhibited by the plate which was made from chromium steel. Minimal corrosion was exhibited by the soft austenitic 304 stainless steel used to make the screws. The corrosion products of the plate were revealed by microprobe analysis to impregnate the surrounding tissues. Improper material selection was concluded to be the reason for the general corrosion behavior.

A broken aircraft crankshaft and a severely damaged main brass bearing were examined to determine whether engine failure was initiated in the bearing or in the crankshaft. The steel crankshaft failure was a classical fatigue fracture. The bearing had been subjected to extremely high temperatures, as indicated by melting in the brass components and the extreme distortion in the rollers. Microscopic examination on the crankshaft material showed it to be a good quality steel. On the other hand, the chromium plate was thick, porous, and cracked in many places, including the point of the main fatigue crack. It was concluded that the over-all failure was initiated in the crankshaft, and the failure of the bearing resulted from that failure.

A narrow bone plate made of type 316 stainless steel and used to stabilize an open midshaft femur fracture failed. A crack at a plate hole next to the fracture site had been revealed by a radiograph taken 13 weeks after the operation. The plate was revealed to be slightly bent in the horizontal plane, and the fracture gap was considerably open. The screws and plates supplied by different manufacturers were revealed to be different with respect to microcleanliness (primary inclusion content) of the materials and only one of them was found to be according to specifications. The local crack formation was influenced by the presence of larger inclusions. The screw failed was revealed to have failed through a fatigue mechanism by the presence of striations in the scanning electron micrograph. The crack in the plate was revealed to have originated at the upper, outer corner of the plate by the beach marks which indicated the action of asymmetric bending and rotational forces.

The locking collar on a machine failed suddenly when the shaft it restrained was inadvertently subjected to an axial load slightly higher than the allowable working load. The locking collar fractured abruptly, producing four large fragments. This allowed the shaft to be propelled forcefully in the direction of the load, causing substantial damage to other machinery components in the vicinity. The failed component, which was 43 cm (17 in.) in diameter, was machined from 4140 plate and heat treated to 34 to 36 HRC. Analysis (visual inspection, composite micrographs, scanning electron microscopy, and mechanical-property analysis) supported the conclusions that the alloy steel plate used in this application contained significant brittle microstructural fibering or banding. This condition produced considerable anisotropy in ductility and toughness as revealed by mechanical testing. Unfortunately, the potential effects of anisotropy were apparently neglected when this component was designed and manufactured from the plate stock, because the loading was applied in a direction that stressed the weakest planes in the material, that is, a direction normal to the fibering. No recommendations were made.

A number of rotating blades in a diffuser at a sugar beet processing plant fabricated from rectangular bars cut from rolled carbon-manganese steel plate fractured brittlely. However, apparently identical blades underwent significant plastic deformation without fracture. Inspection of both fractured and bent blades revealed similar preexisting cracks at the toes of bar attachment welds. Metallographic examination of the bent and the fractured bars revealed they had been cut parallel and transverse, respectively, to the rolling direction of the steel plate. Due to the combined effects of the low fracture toughness of the plate on planes parallel in the rolling direction, the presence of the preexisting cracks, and the relatively large section thickness of the bars, the bars whose lengths were transverse to the rolling direction fractured brittlely when subjected to impact loads. Had the poor transverse properties of thick-section plate been recognized, and all the bars properly cut with respect to the rolling direction, the premature fractures would not have occurred.

A portable propane container with a name-plate soldered onto it exploded in service. When the vessel was inspected afterwards, it was found to have developed a crack in the top end plate. A portion of the end plate cut out to include the midlength and one termination of the crack was examined microscopically. This revealed that the crack was associated with intergranular penetration by molten metal. The microstructure in general was indicative of a good-quality mild steel. It was evident from that solder that was responsible for the penetration and that fused brass from the hand wheel had not played any part. Tensile stress was present at the time of the failure sufficiently high to enable solder penetration to take place. The use of soft solder as a medium for attaching name-plates directly on to stressed steel parts is not recommended. It would be preferable to use a welded-on patch plate or to employ one of the high-strength, non-metallic adhesives.