Failure analysis of a fishhook that broke during retrieval is described. Although the broken hook was discarded, several companion hooks were analyzed (chemistry, microhardness, metallographic cross section, and tensile properties) as were comparable products made by other hook manufacturers. Tensile test data indicated that the companion hooks were significantly different from hooks made by other manufacturers. The hooks broke into several pieces and failed with little or no plastic deformation, while hooks made by other manufacturers plastically deformed and did not break during testing.

A longeron assembly constructed of Alclad 2024, some parts being in the T3 condition, others in the T42 condition, failed at a rivet hole. Plastic deformation at the crack site was found, but no plastic deformation was found in similar failed components. It was concluded that the numerous hairline cracks in the Alclad layer adjacent to the main fracture were fatigue cracks. In another case, bonded samples of 2024-T3 sheet were fatigue tested at various stress levels. Failures could be separated into three groups: those that failed in the adhesive bond, those that failed in the base material, and those that exhibited a dual failure. The last category failed in the adhesive bond and also showed a type of pitting on one face of the base material. In a third case, a 2024-T4 extrusion section was found to exhibit blistering after chemical milling. The presence of interconnecting microcracks between adjacent discontinuities supported a hydrogen blistering diagnosis.

A missile detached from a Navy fighter jet during a routine landing on an aircraft carrier deck because of a faulty missile launcher detent spring. Visual inspection of Inconel 718 detent spring assembly revealed that four of the nine spring leafs comprising the assembly were plastically deformed while two of the deformed leafs did not meet minimal hardness or tensile requirements. Liquid penetrant testing revealed no cracks or other surface discontinuities on the leaf springs. Material sectioned from the soft spring leafs was heat-treated according to specifications in the laboratory. The resultant increase in mechanical properties of the re-heat-treated material indicated that the original heat treatment was not performed correctly. The failure was attributed to improper heat treatment. Recommendations focused on more stringent quality control of the heat-treat operations.

A forging die in a 250-ton press producing brass valves began to show signs of fatigue after a few thousand hits. By the time it reached 30,000 hits, the die was badly damaged and was submitted for analysis along with one of the last forgings produced. The investigation included visual and macroscopic inspection, metallographic and chemical analysis, SEM imaging, optical profilometry, mechanical property testing, and EDX analysis. The die was made of chromium hot-work tool steel and the forgings were made of CuZn39Pb3 heated to an initial working temperature 700 deg C. The entire surface of the die was covered with fatigue cracks and many fillets had been plastically deformed. Several other types of damage were also observed, including areas of oxidation, corrosion pits, voids, abrasive wear, die adhesion, and thermal fatigue. Fatigue cracking was the primary cause of failure with significant contributions from the other damage mechanisms.

One of three valves in a dry automatic sprinkler system tripped accidentally, thus activating the sprinklers. Maintenance records showed that the three valves had been in service less than two years. The valve consisted of a cast copper alloy clapper plate that was held closed by a pivoted malleable iron latch. The latch and top surface of the clapper plate were usually in a sanitary-water environment (stabilized, chlorinated well water with a pH of 7.3) under stagnant conditions. Process make-up water that had been clarified, filtered, softened, and chlorinated and had a pH of 9.8 was occasionally used in the system. Analysis (visual inspection and 250x micrograph) supported the conclusions that failure of the latch was caused by plastic deformation from extensive loss of metal by galvanic corrosion and the sudden loading related to the tripping of the valve. Failure in some regions of the contact area was by ductile (transgranular) fracture. Recommendations included changing the latch material from malleable iron to silicon bronze (C87300). The use of silicon bronze prevents corrosion or galvanic attack and proper adjustment of the latch maintains an adequate contact area.

A compression hip screw is a device designed to hold fractures in the area of the femur in alignment and under compression. A side plate, which is an integral part of the device, is attached by screws to the femur, and it holds the compression screw in position. The device analyzed had broken across the eighth hole (of nine holes) from the end of the plate. The detailed metallurgical failure analysis of the device, including metallography and fractography, is reported here. It was found that the device had adequate metallurgical integrity for the application for which it was intended. It is believed that failure was caused by the lack of a screw in the ninth hole. Evidence is also presented which indicates that the device was bent prior to insertion, and the local plastic deformation may have caused structural changes leading to premature crack initiation.

Microstructural examinations on transverse cross sections of a steam reformer tube, showed the presence of large macrovoids elongated in the radial direction and emanating from the internal surface of the tube. The macrovoids were located at the interdendritic regions, and were partially filled by a Mn-Fe bearing chromium oxide film. The areas adjacent to the oxide film were chemically depleted in C, Cr and Mn and rich in Fe and Ni. Associated with this depletion were a large concentration of microvoids. It was suggested that the dissolution of carbides in areas surrounding the macrovoids and the concentration of stresses at their tips, caused extensive localized plastic deformation which led to the formation of microvoids and subsequently to the spalling of the oxide film. The non-protective character of the film induced a progressive deterioration of the grain boundaries properties. Grain boundary sliding and dislocation motion were enhanced, causing a local increase in the steady state strain rate and the premature failure of the tube.

After some 87,000 h of operation, failure took place in the bend of a steam pipe connecting a coil of the third superheater of a steam generator to the outlet steam collector. The unit operated at 538 deg C and 135 kPa, producing 400 t/h of steam. The 2.25Cr-1Mo steel pipe in which failure took place was 50.8 mm in diam with a nominal wall thickness of 8 mm. It connected to the AISI 321 superheater tube by means of a butt weld and was one of 46 such parallel connecting tubes. The Cr-Mo tubing was situated outside the heat transfer zone of the superheater. The overall sequence of failure involved overheating of the Cr-Mo outlet tubes, heavy oxidation, oxide cracking on thermal cycling, thermal fatigue cracking plus oxidation, creep-controlled crack growth, and rapid plastic deformation and rupture. This failure was indicative of excess temperature of the steam coming from the heat transfer zone of the coil. It showed that many damage mechanisms may combine in the transition from fracture initiation to final failure. The presence of grain boundary sliding as an indication of creep damage was useful in the characterization of the stress level as high and showed that the process of creep was not operative throughout the life of the equipment.

Several ruptures took place in the front wall tubes of a water tube boiler. Some rupture samples showed ductile failure while others showed brittle failure. Specimens taken from the rupture where a thick edge had been produced, i.e., with little evidence of prior plastic deformation, showed a coarse microstructure indicative of gross overheating. The examination indicated that failure in the main resulted from gross overheating arising from water starvation as could have been due to a number of causes. The ruptures in some tubes were of the type commonly found in overheated tubes, the material being drawn out to a feather edge at the time of rupture. Other ruptures in the same and other tubes were of a more brittle type, this being associated with penetration of material by molten copper derived from scale.

A number of rotating blades in a diffuser at a sugar beet processing plant fabricated from rectangular bars cut from rolled carbon-manganese steel plate fractured brittlely. However, apparently identical blades underwent significant plastic deformation without fracture. Inspection of both fractured and bent blades revealed similar preexisting cracks at the toes of bar attachment welds. Metallographic examination of the bent and the fractured bars revealed they had been cut parallel and transverse, respectively, to the rolling direction of the steel plate. Due to the combined effects of the low fracture toughness of the plate on planes parallel in the rolling direction, the presence of the preexisting cracks, and the relatively large section thickness of the bars, the bars whose lengths were transverse to the rolling direction fractured brittlely when subjected to impact loads. Had the poor transverse properties of thick-section plate been recognized, and all the bars properly cut with respect to the rolling direction, the premature fractures would not have occurred.

An 1100 aluminum alloy connector of a high-tension aluminum conductor steel-reinforced (ACSR) transmission cable failed after more than 20 years in service, in a region of consider able industrial pollution. The steel core was spliced with a galvanized 1020 carbon steel sheath. Visual examination showed that the connector had undergone considerable plastic deformation and necking before fracture. The steel sheath was severely corroded, and the steel splice was pressed off-center in the axial direction inside the connector. Examination of the fracture surface and micro-structural analysis indicated that the failure was caused by mechanical overload, which occurred because of weakening of the steel support cable by corrosion inside the fitting. The corrosion was ascribed to defective assembly of the connector which allowed moisture penetration.

Superelastic nitinol wires that fractured under various conditions were examined under a scanning electron microscope in order to characterize the fracture surfaces, produce reference data, and compare the findings with prior published work. The study revealed that nitinol fracture modes and morphologies are generally consistent with those of ductile metals, such as austenitic stainless steel, with one exception: Nitinol exhibits a unique damage mechanism under high bending strain, where damage occurs at the compression side of tight bends or kinks while the tensile side is unaffected. The damage begins as slip line formation due to plastic deformation, which progresses to cracking at high strain levels. The cracks appear to initiate from slip lines and extend in shear (mode II) manner.

A carbon steel ball-peen hammer ejected a chip that struck the user's eye. Failure occurred when two hammers were struck together during an attempt to free a universal joint from an automotive drive shaft. Two samples were cut from the face of the hammer one through the chipped area on the chamfer and the other from the undamaged area on the chamfer. The shape and texture of the fracture surfaces were typical of spalling. The fracture was conchoidal and exhibited a complete lack of plastic deformation. White etching bands that intersected the face and chamfer were revealed during metallographic examination. Fracture occurred through a white band. Failure was attributed to formation of envelopes of untempered martensite under the chamfer that ruptured explosively during service.

Wear, a form of surface deterioration, is a factor in a majority of component failures. This article is primarily concerned with abrasive wear mechanisms such as plastic deformation, cutting, and fragmentation which, at their core, stem from a difference in hardness between contacting surfaces. Adhesive wear, the type of wear that occurs between two mutually soluble materials, is also discussed, as is erosive wear, liquid impingement, and cavitation wear. The article also presents a procedure for failure analysis and provides a number of detailed examples, including jaw-type rock crusher wear, electronic circuit board drill wear, grinding plate wear failure analysis, impact wear of disk cutters, and identification of abrasive wear modes in martensitic steels.

This article describes concepts and tools that can be used by the failure analyst to understand and address deformation, cracking, or fracture after a stress-related failure has occurred. Issues related to the determination and use of stress are detailed. Stress is defined, and a procedure to deal with stress by determining maximum values through stress transformation is described. The article provides the stress analysis equations of typical component geometries and discusses some of the implications of the stress analysis relative to failure in components. It focuses on linear elastic fracture mechanics analysis, with some mention of elastic-plastic fracture mechanics analysis. The article describes the probabilistic aspects of fatigue and fracture. Information on crack-growth simulation of the material is also provided.

Optimized modeling of fracture-critical structural components and connections requires the application of elastic-plastic fracture mechanics. Such applications, however, can require sophisticated analytical techniques such as crack tip opening displacement (CTOD), failure assessment diagram (FAD), and deformation plasticity failure assessment diagram (DPFAD). This article presents the origin and description of FAD and addresses R6 FAD using J-integral. It details the fracture criteria of BS 7910. The factors to be considered during the use of FAD and the applications of FAD are also reviewed.

A high-chromium white cast iron shell liner installed in an ore crusher sustained impact damage in the course of operation. Visual-optical examination revealed horizontal cracks on the surface of the liner along with particles that had fractured off. Metallographic examination indicated a heavily deformed surface layer with chip formation at the wear surface. The chemical composition of the liner was found to be Fe-2.74C-0.75Mn-0.55Si-0.51Ni-19.4Cr-1.15M. This alloy is highly resistant to abrasive wear, yet at the same time, prone to chipping because little plastic displacement will occur at the surface. The liner failed as a result of severe abrasion caused by the impact of taconite rock. This was a material-selection problem in that the wrong alloy was used for a condition not anticipated in the original choice.

This article reviews the mechanical behavior and fracture characteristics that discriminate structural polymers from metals. It provides information on deformation, fracture, and crack propagation as well as the fractography involving the examination and interpretation of fracture surfaces, to determine the cause of failure. The fracture modes such as ductile fractures and brittle fractures are reviewed. The article also presents a detailed account of various fracture surface features. It concludes with several cases of field failure in various polymers that illustrate the applicability of available analytical tools in conjunction with an understanding of failure mechanisms.

A copper condenser dashpot in a refrigeration plant failed prematurely. The dashpot was a long tubular component with a cup brazed at each end. Stereomicroscopic examination of the fracture surface at low magnification revealed a typical ductile mode of failure. The failure was attributed to insufficient component thickness, which made the dashpot unable to withstand internal operating pressure, and to extensive annealing in the heat-affected zones of the brazed joints. It was recommended that the condenser dashpot design take into account the annealing effects of brazing. Hydrostatic testing at a pressure times greater than the maximum operating pressure prior to placing the component in service was also suggested.

Explosive cladding is a viable method for cladding different materials together, but the complicated behavior of materials under ballistic impacts raises the probability of interfacial shear failure. To better understand the relationship between impact energy and interfacial shear, investigators conducted an extensive study on the shear strength of explosively cladded Inconel 625 and plain carbon steel samples. They found that by increasing impact energy, the adhesion strength of the resulting cladding can be improved. Beyond a certain point, however, additional impact energy reduces shear strength significantly, causing the cladding process to fail. The findings reveal the decisive role of plastic strain localization and the associated development of microcracks in cladding failures. An attempt is thus made to determine the optimum cladding parameters for the materials of interest.