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Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001032
EISBN: 978-1-62708-214-3
... Abstract A Stirling engine heat pipe failed after only 2h of operation in a test situation. Cracking at the leading edge of an evaporator fin allowed air to enter the system and react with the sodium coolant. The fin was fabricated from 0.8 mm (0.03 in.) thick Inconel 600 sheet. The wick...
Abstract
A Stirling engine heat pipe failed after only 2h of operation in a test situation. Cracking at the leading edge of an evaporator fin allowed air to enter the system and react with the sodium coolant. The fin was fabricated from 0.8 mm (0.03 in.) thick Inconel 600 sheet. The wick material was type 316 stainless steel. Macro- and microexaminations of specimens from the failed heat pipe were conducted. The fin cracking was caused by overheating that produced intergranular corrosion in both the fin and the wick. Recommendations for alleviating the corrosion problem included reducing the heat flux, redesigning the wick, and reducing the oxygen content of the sodium.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001043
EISBN: 978-1-62708-214-3
... by the manufacturer in other hydrogen plants for years without any noted failures of the support tubes in the quench pots. Specimen Selection A section of pipe approximately 90 by 200 mm (3.5 by 8 in.) in length was received for examination. One lip of the section was eroded from service failure, whereas...
Abstract
A 76 mm (3 in.) type 304 stainless steel tube that was used as a heat shield and water nozzle support in a hydrogen gas plant quench pot failed in a brittle manner. Visual examination of a sample from the failed tube showed that one lip of the section was eroded from service failure, whereas the opposite side exhibited a planar-type fracture. Sections were removed from the eroded area and from the opposite lip for microscopic studies and chemical analysis. The eroded edges exhibited river bed ditching, indicative of thermal fatigue. Microstructural analysis showed massive carbide formations in a martensite matrix and outlining of prior-austenite grains by a network of fine, white lines. These features indicated that the material had been transformed by carburization by the impinging gas. The outer surface exhibited a heavy scale deposit and numerous cracks that originated at the surface of the tube. The cracks were covered with scale, indicating that thermal fatigue (heat cracking) had occurred. Chemical analysis confirmed that the original material was type 304 stainless steel that had been through-carburized by the formation of an endothermic gas mixture. It was recommended that plant startup and shutdown procedures be modified to reduce or eliminate the presence of the carburizing gas mixture.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001056
EISBN: 978-1-62708-214-3
... Abstract Type 347 stainless steel moderator circuit branch piping in a pressurized hot water reactor was experiencing frequent leakage. Investigation of the problem involved failure analysis of leaking pipe specimens, analytical stress analysis, and determination of “leak-before-break...
Abstract
Type 347 stainless steel moderator circuit branch piping in a pressurized hot water reactor was experiencing frequent leakage. Investigation of the problem involved failure analysis of leaking pipe specimens, analytical stress analysis, and determination of “leak-before-break” conditions using fracture mechanics and thermal fatigue simulation tests. Failure analysis indicated that cracking had been initiated by thermal fatigue. Data from the analysis were used in making the leak-before-break predictions. It was determined that the cracks could grow to two-thirds of the circumferential length of the pipe without catastrophic failure. A thin stainless steel sleeve was inserted in the branch pipe to resolve the problem.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001057
EISBN: 978-1-62708-214-3
... Abstract A brass (CDA alloy 230) pipe nipple that was part of a domestic cold water bath system failed two weeks after installation. Macrofractography, SEM examination, metallography, and chemical analyses were performed on specimens cut through the main fracture surface. The physical...
Abstract
A brass (CDA alloy 230) pipe nipple that was part of a domestic cold water bath system failed two weeks after installation. Macrofractography, SEM examination, metallography, and chemical analyses were performed on specimens cut through the main fracture surface. The physical and background evidence obtained indicated failure due to cracking initiated by stamped markings on the pipe wall and extended by high circumferential residual stresses. It was recommended that annealed pipe be used.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001060
EISBN: 978-1-62708-214-3
... Abstract A type 316 stainless steel pipe reducer section failed in service of bleached pulp stock transfer within 2 years in a pulp and paper mill. The reducer section fractured in the heat-affected zone of the flange-to-pipe weld on the flange side. The pipe reducer section consisted of 250...
Abstract
A type 316 stainless steel pipe reducer section failed in service of bleached pulp stock transfer within 2 years in a pulp and paper mill. The reducer section fractured in the heat-affected zone of the flange-to-pipe weld on the flange side. The pipe reducer section consisted of 250 and 200 mm (10 and 8 in.) diam flanges welded to a tapered pipe section. The tapered pipe section was 3.3 mm (0.13 in.) thick type 316 stainless steel sheet, and the flanges were 5 mm (0.2 in.) thick CF8M (type 316) stainless steel castings. Visual and metallographic analysis indicated that the fracture was caused by intergranular corrosion/stress-corrosion cracks that initiated from the external surface of the pipe reducer section. Contributory factors were the sensitized condition of the flange and the concentration of corrosive elements from the bleach stock plant environment on the external surface. In the absence of the sensitized condition of the flange, the service of the pipe reducer section was acceptable. A type 316L stainless steel reducer section was recommended to replace the 316 component because of its superior resistance to sensitization.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001061
EISBN: 978-1-62708-214-3
... Abstract Schedule 80 low-carbon steel pipes used to transfer kraft liquor in a Kamyr continuous pulp digester failed within 18 months after installation. Visual and metallographic examinations established that the cracking initiated on the internal surfaces of the equalizer pipes in the welds...
Abstract
Schedule 80 low-carbon steel pipes used to transfer kraft liquor in a Kamyr continuous pulp digester failed within 18 months after installation. Visual and metallographic examinations established that the cracking initiated on the internal surfaces of the equalizer pipes in the welds and heat-affected zones (HAZs). Fracture/crack morphology was brittle and primarily intergranular and deposits at crack tips were primarily iron oxides with significant amounts of sodium compounds. On these bases, the cracking was characterized as intergranular stress-corrosion cracking (IGSCC). Corrosion-related deterioration was not found, indicating that the material was generally suitable for the intended service. High residual tensile stresses in the welds and HAZS, resulting from field welding under highly constrained conditions using inadequate weld procedures, were the most probable cause of the failures. Minimizing residual stresses through use of welding procedures that include appropriate preweld and interpass temperatures and postweld stress relief heat treatment at 650 deg C (1200 deg F) was recommended to prevent further failures.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001066
EISBN: 978-1-62708-214-3
... present in the process stream. Circumstances Leading to Failure The pipe was removed from the system after cracks were observed in the painted coating. Sample Selection The entire 460 mm (18 in.) length of spool piece was sent for analysis. Testing Procedure and Results Surface...
Abstract
A flanged 100 mm (4 in.) diam low-carbon steel spool piece lined with Teflon was removed from a sulfuric acid denitrification system after cracks were observed in the painted coating. Visual and microstructural examination along with SEM fractography revealed scaled iron oxides on all opened crack surfaces. The surfaces had a faceted morphology, indicating intergranular fracture. Cracks originated at the interface between the tube and the Teflon liner Corrosion products were found caked into the intergranular region between the liner and the spool. The portion of the liner that had been exposed to the process stream was discolored. Failure of the spool was attributed to stress-corrosion cracking promoted by the presence of nitrates. Nitric acid contaminant in the sulfuric acid stream had diffused through the liner and accumulated in the annular space. Use of a liner that is more impermeable to the diffusion of ionic species was recommended.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001327
EISBN: 978-1-62708-215-0
... Abstract Three ASME SA106 grade B carbon steel feed water piping reducers from a pressurized water reactor showed indications of flaws near welds during ultrasonic testing. Further examination and testing indicated that the cracks resulted from a low-cycle corrosion fatigue phenomenon...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001331
EISBN: 978-1-62708-215-0
... Abstract A high-pressure steam pipe specified to be P22 low-alloy steel failed after 25 years of service. Located at the end of the steam line, the pipe reportedly received no steam flow during normal service. Visual examination of the failed pipe section revealed a window fracture...
Abstract
A high-pressure steam pipe specified to be P22 low-alloy steel failed after 25 years of service. Located at the end of the steam line, the pipe reportedly received no steam flow during normal service. Visual examination of the failed pipe section revealed a window fracture that appeared brittle in nature. Specimens from the fracture area and from an area well away from the fracture were examined metallographically and chemically analyzed. Results indicated that the pipe had failed by hydrogen damage that resulted in brittle fracture. Chemical analysis indicated that the pipe material was 1020 carbon steel, not P22. The misapplication of pipe material was considered to be a contributing factor. Position of the pipe within the system caused the localized damage.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001332
EISBN: 978-1-62708-215-0
... fracturing Pipe flanges Welded joints ASTM A105 UNS K03504 (Other, general, or unspecified) fracture Background A 356 mm (14 in.) diam slip-on flange cracked. Pertinent Specifications The specification called for an integral forging or a casting. Instead, the slip-on flange had been...
Abstract
A cracked 356 mm (14 in.) diam slip-on flange (Ni-Cr-Mo-V steel) was submitted for failure analysis. Reported results and observations indicated that the flange was not an integral forging or a casting, as specified. It had been fabricated by welding and machining a ring insert within a flange with a larger internal diameter. The flange cracked because the welds between the flange and the insert were inadequate to withstand the bolting pressures. A warning was issued to end users of the flanges, which are being inspected nondestructively for conformance to specifications.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001336
EISBN: 978-1-62708-215-0
... Abstract Catastrophic pitting corrosion occurred in type 304L stainless steel pipe flange assemblies in an industrial food processor. During regular service the pumped medium was pureed vegetables. In situ maintenance procedures included cleaning of the assemblies with a sodium hypochlorite...
Abstract
Catastrophic pitting corrosion occurred in type 304L stainless steel pipe flange assemblies in an industrial food processor. During regular service the pumped medium was pureed vegetables. In situ maintenance procedures included cleaning of the assemblies with a sodium hypochlorite solution. It was determined that the assemblies failed due to an austenite-martensite galvanic couple activated by a chlorine bearing electrolyte. The martensitic areas resulted from a transformation during cold-forming operations. Solution annealing after forming, revision of the design of the pipe flange assemblies to eliminate the forming operation, and removal of the source of chlorine were recommended.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001343
EISBN: 978-1-62708-215-0
... Abstract A section of type 304 stainless steel pipe from a stand by system used for emergency injection of cooling water to a nuclear reactor failed during precommissioning. Leaking occurred in only one spot. Liquid penetrant testing revealed a narrow circumferential crack. Metallographic...
Abstract
A section of type 304 stainless steel pipe from a stand by system used for emergency injection of cooling water to a nuclear reactor failed during precommissioning. Leaking occurred in only one spot. Liquid penetrant testing revealed a narrow circumferential crack. Metallographic examination of the cracked area indicated stress-corrosion cracking, which had originated at rusted areas that had formed on longitudinal scratch marks on the outer surface of the pipe. The material was free from sensitization, and there was no significant amount of cold work. It was recommended that the stainless steel be kept rust free.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c0048747
EISBN: 978-1-62708-229-7
... the conclusion that the pipe failed by fatigue. Cracks originated at crevices and pits in the weld area that acted as stress raisers, producing high localized stresses because of the sharp-radius corner design. Abnormally high structural stresses and alternating stresses resulting from the pump vibrations...
Abstract
A 455 mm diam x 8 mm thick wall carbon steel (ASTM A 53) discharge line for a circulating-water system at a cooling tower fractured in service; a manifold section cracked where a Y-shaped connection had been welded. Investigation (visual inspection and photographs) supported the conclusion that the pipe failed by fatigue. Cracks originated at crevices and pits in the weld area that acted as stress raisers, producing high localized stresses because of the sharp-radius corner design. Abnormally high structural stresses and alternating stresses resulting from the pump vibrations contributed to the failure. Recommendations included changing the joint design to incorporate a large-radius corner and improving fitting of the components to permit full weld penetration. Backing strips were suggested to increase weld quality, and the pipe wall thickness was increased from 8 to 9.5 mm.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c0091528
EISBN: 978-1-62708-229-7
... Abstract A 150 mm (6 in.) schedule 80S type 304 stainless steel pipe (11 mm, or 0.432 in., wall thickness), which had served as an equalizer line in the primary loop of a pressurized-water reactor, was found to contain several circumferential cracks 50 to 100 mm (2 to 4 in.) long. Two...
Abstract
A 150 mm (6 in.) schedule 80S type 304 stainless steel pipe (11 mm, or 0.432 in., wall thickness), which had served as an equalizer line in the primary loop of a pressurized-water reactor, was found to contain several circumferential cracks 50 to 100 mm (2 to 4 in.) long. Two of these cracks, which had penetrated the pipe wall, were responsible for leaks detected in a hydrostatic test performed during a general inspection after seven years of service. Investigation (visual inspection, visual and ultrasonic weld examination, water analysis, and chemical analysis) supported the conclusion that the failure was caused by SCC due to stress, sensitization, and environment. Recommendations included replacing all pipe sections and installing them using low-heat-input, multiple-pass welding procedures.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001469
EISBN: 978-1-62708-229-7
... Abstract In a main range in a power station, steam was conveyed at a pressure of 645 psi, and a temperature of 454 deg C (850 deg F). Pipe diameter was 9 in. and the joints were of the bolted type in which a thin steel ring, serrated on both sides, was inserted between plain flanges. Thin...
Abstract
In a main range in a power station, steam was conveyed at a pressure of 645 psi, and a temperature of 454 deg C (850 deg F). Pipe diameter was 9 in. and the joints were of the bolted type in which a thin steel ring, serrated on both sides, was inserted between plain flanges. Thin jointing material was interposed between the serrated faces and the flanges. The first intimation of trouble was the onset of a high pitched noise audible over a radius of a quarter of a mile. The noise arose from violent lateral vibration of the serrated ring, which attained an amplitude and persisted for a sufficient number of cycles to produce an extensive system of fatigue cracks that resulted in partial disintegration of the ring. Microscopic examination of the material showed it to be a mild steel of satisfactory quality. The trouble was started by slight leakage, possibly resulting from a relaxation of the interfacial pressure on the joint faces, which eroded away the joint material locally at one face of the serrated ring. This reduced interfacial pressure at the opposite face of the ring, with resultant leakage and erosion of the joint material on this side.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001422
EISBN: 978-1-62708-229-7
... Abstract During a hydraulic test on one of the boilers in a range, leakage occurred from the lower surface of a horizontal S bend in the main steam pipe between the drum connector box and the junction valve. The pipe in question was 15 in. bore and had been in service for about 50 years...
Abstract
During a hydraulic test on one of the boilers in a range, leakage occurred from the lower surface of a horizontal S bend in the main steam pipe between the drum connector box and the junction valve. The pipe in question was 15 in. bore and had been in service for about 50 years. Specimens were prepared for microscopical examination to include the defective zone and a section through a circumferential crack. The defective zone was found to contain numerous inclusions of slag and oxides of globular form. Regions surrounding the inclusions were decarburized, the indications being that this region of the plate had been heated to an excessively high temperature. A corrosion-fatigue fissure was at one location, this having originated at the internal surface of the pipe and run into an inclusion in the defective zone. The failure resulted from the development of corrosion-fatigue fissures which originated at a zone containing defects introduced at the time of manufacture. These may have had their origin in the ingot from which the plate was rolled or, alternatively, be indicative of a zone which suffered overheating and local burning at the time the forge weld was made.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001227
EISBN: 978-1-62708-235-8
... of the core zone were noted. It was also possible that the pipe was resting on a cold plate during bending or that it came in touch with a cold tool. This apparently caused the strains at the transition to the cross-sectional part that had been cooled more slowly. The location of the crack at just this point...
Abstract
An elbow of 70 mm OD and 10 mm wall thickness made from St 35.29, and exposed to 315 atmospheres internal pressure in an oil hydraulic shear installation, cracked lengthwise after a short operating period. Because the stress was not sufficient to explain the fracture of this elbow under this pressure, an investigation was conducted to establish whether material or processing errors had occurred. Microscopic examination showed that a ferritic-pearlitic structure in select locations was very fine-grained. Other signs of fast cooling as compared to normally formed structure of the core zone were noted. It was also possible that the pipe was resting on a cold plate during bending or that it came in touch with a cold tool. This apparently caused the strains at the transition to the cross-sectional part that had been cooled more slowly. The location of the crack at just this point gave rise to the conclusion that it was formed either by the sole or contributive effect of these stresses.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001421
EISBN: 978-1-62708-235-8
... Abstract The bottom flange of a vertical pipe coupled to an isolating valve in a steam supply line to a turbine failed. Steam pressure was 1,500 psi and the temperature 416 deg C (780 deg F). Multiple cracking occurred in the bore of the flange. A quarter-segment was cut out and examined...
Abstract
The bottom flange of a vertical pipe coupled to an isolating valve in a steam supply line to a turbine failed. Steam pressure was 1,500 psi and the temperature 416 deg C (780 deg F). Multiple cracking occurred in the bore of the flange. A quarter-segment was cut out and examined. The cracks were located in the part of the flange that formed a continuation of the pipe bore. The majority of them originated at the end of the flange bore and extended axially along the pipe and radially across the flange face. Magnetic crack detection revealed a further number of cracks in the weld deposit. While the fracture in the weld metal was of the ductile type exhibiting a fine fibrous appearance, that in the flange material was of the cleavage type. Microscopic examination revealed that the cracks were blunt-ended fissures of the type characteristic of corrosion-fatigue. It was concluded that cracking was due to corrosion-fatigue, which arose from the combined effect of a fluctuating tensile stress in the presence of a mildly corrosive environment.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.pulp.c9001564
EISBN: 978-1-62708-230-3
... Abstract An 8 in. diam stainless steel black liquor feed pipe to a carbon steel digester had failed within one year of service. The material was type 316 molybdenum-containing austenitic stainless steel. The service environment was alkaline black liquor at 175 deg C (350 deg F). The pipe had...
Abstract
An 8 in. diam stainless steel black liquor feed pipe to a carbon steel digester had failed within one year of service. The material was type 316 molybdenum-containing austenitic stainless steel. The service environment was alkaline black liquor at 175 deg C (350 deg F). The pipe had developed cracks on the inside surface coincident with an external support gusset. The cracks initiated at wide corrosion grooves. The early stages were corrosion-assisted fatigue cracks. The cracks initiated at the corrosion grooves and propagated as transgranular SCC with characteristic branching. Evaluation indicated the cracks were localized in an area of high cyclic stresses as a consequence of geometrical constraints on the piping and unsupported cantilever loads. No cracks were found elsewhere in the pipe. In the absence of highly localized service stresses (exceeding yield strength of the material), the corrosion grooving and subsequent SCC would not have occurred in this service environment. The pipe support system was modified with additional gussets to reduce the magnitude of cyclic stresses at the critical areas. The modification was apparently successful.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c0091292
EISBN: 978-1-62708-219-8
... Abstract A 25 mm (1 in.) copper coupling had been uniformly degraded around most of the circumference of the bell and partially on the spigot end. One penetration finally occurred through the thinned area on the spigot end of the pipe. Investigation supported the conclusion that although...
Abstract
A 25 mm (1 in.) copper coupling had been uniformly degraded around most of the circumference of the bell and partially on the spigot end. One penetration finally occurred through the thinned area on the spigot end of the pipe. Investigation supported the conclusion that although the pipe was buried in noncorrosive sandy soil, it was found to incur stray currents at 2 Vdc in relation to a Cu/CuSO4 half cell. Recommendations included eliminating, moving, or shielding the source of stray current.
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