This article focuses on characterizing the fracture-surface appearance at the microscale and contains some discussion on both crack nucleation and propagation mechanisms that cause the fracture appearance. It begins with a discussion on microscale models and mechanisms for deformation and fracture. Next, the mechanisms of void nucleation and void coalescence are briefly described. Macroscale and microscale appearances of ductile and brittle fracture are then discussed for various specimen geometries (smooth cylindrical and prismatic) and loading conditions (e.g., tension compression, bending, torsion). Finally, the factors influencing the appearance of a fracture surface and various imperfections or stress raisers are described, followed by a root-cause failure analysis case history to illustrate some of these fractography concepts.

Two outer valve springs made from air-melted 6150 pretempered steel wire broke during production engine testing. The springs were 50 mm in OD and 64 mm in free length, had five coils and squared-and-ground ends, and were made of 5.5 mm diam wire. It was revealed that fracture was nucleated by an apparent longitudinal subsurface defect. The defect was revealed by microscopic examination to be a large pocket of nonmetallic inclusions (alumina and silicate particles) at the origin of the fracture. Partial decarburization of the steel was observed at the periphery of the pocket of inclusions. Torsional fracture was indicated by the presence of beach marks at a 45 deg angle to the wire axis. It was established that the spring fractured by fatigue nucleated at the subsurface defect.

Examination of a cracked nose landing gear cylinder made of AISI 4340 Cr-Mo-Ni alloy steel proved that the part started to fail on the inside diam. When the nucleus of the stress-corrosion crack was studied in detail, iron oxide was found on the fracture surface. A 6500x micrograph revealed this area also displayed an intergranular texture. One of a group of small grinding cracks on the ID of the cylinder nucleated the failure. Other evidence indicated the cracks developed when the cylinder was ground during overhaul.

An articulated rod (made from 4337 steel (AMS 6412) forging, quenched and tempered to 36 to 40 HRC) used in an overhauled aircraft engine was fractured after being in operation for 138 h. Visual examination revealed that the rod was broken into two pieces 6.4 cm from the center of the piston-pin-bushing bore. The fracture was nucleated at an electroetched numeral 5 on one of the flange surfaces. A notch, caused by arc erosion during electroetching, was revealed by metallographic examination of a polished-and-etched section through the fracture origin. A remelted zone and a layer of untempered martensite constituted the microstructure of the metal at the origin. Small cracks, caused by the high temperatures developed during electro-etching, were observed in the remelted area. It was concluded that fatigue fracture of the rod was caused by the notch resulting from electroetching and thus electroetched marking of the articulated rods was discontinued as a corrective measure.

Severe pitting corrosion of a carbon steel tube was observed in the air preheater of a power plant, which runs on rice straw firing. Approximately 1450 tubes were removed from Stage 3 of the preheater (air inlet and flue gas outlet) due to corrosion and local bursting. Samples from Stage 2 (where corrosion was low) and Stage 3 (severe corrosion) were taken and subjected to visual inspection, SEM, x-ray diffraction, microhardness measurement, and chemical and microstructural analysis. It was determined that extended non-operation of the plant resulted in the settlement of corrosive species on the tubes in Stage 3. The complete failure of the tube occurred due to diffusion of these elements into the base metal and precipitation of potassium and chlorine compounds along the grain boundaries, with subsequent dislodging of grains. The nonmetallic inclusions acted as nucleating sites for local pitting bursting. Nonuniform heat transfer in Stage 3 operation accelerated the selective corrosion of front-end tubes. The relatively high heat transfer in this stage resulted in condensation of some corrosive gases and consequent corrosion. Continuous operation of the plant with some precautions during assembly of the tubes reduced the corrosion problem.

The genesis of failure of 6.1 mm thick electric resistance welded API 5L X-46 pipes during pretesting at a pressure equivalent to 90% of specified minimum yield strength was investigated. Cracks were found to initiate on the outer surface of the pipes in the fusion zone and propagate along the through-thickness direction. The presence of extensive decarburization and formation of a soft ferrite band within the fusion zone may have contributed to the nucleation of the cracks. Crack propagation was aided by the presence of exogenous inclusions entrapped within the fusion zone. Analysis of these inclusions confirmed the presence of Fe, Si, Ca, and O, indicating slag entrapment to be the most probable culprit.

The electroplated tappet adjusting screws used in diesel engines failed during initial bend testing. The analysis of the failure showed that the fracture was nucleated from the subsurface of the screw. The fracture surface was intergranular at the ID and OD region and microvoid coalescence in the center. The improper baking after electroplating of the screw led to H2-induced blistering/cracking. The high strength of the threaded region of the adjusting screw increased the failure propensity.

Two broken ball-mill liners from a copper-mine ore operation were submitted for failure analysis. These liners failed prematurely, having reached less than 20% of their expected life. The chemical composition of the liners was within specifications for high-chromium white cast iron. The two broken liners were sand blasted for visual inspection and subsequent metallography and hardness testing. Many cracks were found externally and on the undersides. There were also signs of mechanical damage that occurred inside the mill before detection of the failures. The underside cracking is significant because the user advised that the liners were not backed in the installation. Cracking was present in the microstructures of both liners. These cracks tend to fracture the brittle carbide phase first; once nucleated, the sharp cracks can propagate and grow to critical dimensions, which eventually induces complete failure to the load-bearing section. The premature failure of these liners was caused by severe localized overstress conditions due to localized impact in service. Proper backing of shell liners should be ensured to reduce the effect of impact forces in the ball mill.

Gross wastage and embrittlement were observed in plain carbon steel desuperheaters in five new Naval power plants. The gross wastage could be duplicated in laboratory bomb tests using sodium hydroxide solutions and was concluded to be caused by free caustic concentrated by high heat flux. The embrittlement was shown to be caused by the flow of corrosion generated hydrogen which converted the cementite to methane which nucleated voids in the steel. A thermodynamic estimate indicated that a small amount of chromium would stabilize the carbides against decomposition by hydrogen in this temperature range, and laboratory tests with 2-14% Cr steel verified this.

The damage to a screw on the head of a 1.8 liter personal car engine was nucleated as the result of common disadvantageous environmental influences and reversed loads leading to corrosion fatigue.

Within about one month, several knuckle pins (AMS 6470 steel failed, and required to have a minimum case hardness of 92 h15N, a case depth of 0.4 to 0.5 mm (0.017 to 0.022 in.), and a core hardness of 285 to 341 HRB) used in engines failed over a range of 218 to 463 h in operation. Visual examination revealed beach marks typical of fatigue cracks that had nucleated at the base of the longitudinal oil hole. Micrographs of sections revealed a remelt zone and an area of untempered martensite within the region of the cracks. However, review of inspection procedures disclosed the pins had been magnetic-particle inspected by inserting a probe into the longitudinal hole. Evidence found supports the conclusions that the knuckle pins failed by fatigue fracture. The circular cracks at the longitudinal holes were the result of improper technique in magnetic-particle inspection. Thermal transformation of the metal also causes a stress concentration that may lead to fatigue failure. Recommendations included insulating the conductor to prevent arc burning at the base of the longitudinal oil hole. Also, a borescope or metal monitor could be used to inspect the hole for evidence of arc burning from magnetic-particle inspection.

Two A6 tool steel (free machining grade) shafts, parts of a clamping device used for bending 5.7 cm OD tubing on an 8.6 cm radius, failed simultaneously under a maximum clamping force of 54,430 kg. The shaft was imposed with cyclic tensile stresses due to the clamping force and unidirectional bending stresses resulting from the nature of operation. Nonmetallic oxide-sulfide segregation was indicated by microscopic examination of the edge of the fracture surface. Both smooth and granular areas were revealed on visual examination of the fracture. The shaft was subjected to a low overstress as the smooth-textured fatigue zone was relatively large compared with the crystalline textured coarse final-fracture zone. The fatigue crack was nucleated by the nonmetallic inclusion that intersected the surface and initiated in the 0.25 mm radius fillet at a change in section due to stress concentration. To minimize this stress concentration, a larger radius fillet shaft at the critical change in section was suggested as corrective measure.

A structure had been undergoing fatigue testing for several months when a post-like member heat treated to a tensile strength of 1517 to 1655 MPa (220 to 240 ksi) ruptured. The fracture occurred in the fillet of the post that contacted the edge of a carry-through box bolted to the member. At failure, the part was receiving a second set of loads up to 103.6% of design load. Visual investigations showed rubbing and galling of the fillet. Microscopic and metallographic examination revealed beach marks on the fracture surface and evidence of cold work and secondary cracking in the rubbed and galled area. Electron fractography confirmed that cracking had initiated at a region of tearing and that the cracks had propagated by fatigue. Mechanical properties of all specimens exceeded the minimum values specified for the post. This evidence supports the conclusion that fatigue was the primary cause of failure. Rubbing of the faying surfaces worked the interference area on the post until small tears developed. These small tears became stress-concentration points that nucleated fatigue cracks. Recommendations included rounding the edge of the box in the area of contact with the post to ensure a tangency fit.

This article discusses the failure of cylinder clamping rods in single cylinder diesel engines. The AISI 4140 hardened and tempered steel clamping rods were failing after 200 to 250 h of operation. The fatigue failures initiated at the root of the last thread on the clamping rod that was engaged in a blind hole in the cylinder block. The failures were caused by loose tolerances on the threads that resulted in a non-uniform distribution of load. The load was concentrated on the last threads to engage, thus causing fatigue crack nucleation at the thread root and propagation until the rod broke by overload. Changing the tolerance on the threads virtually eliminated the fatigue problem.

This article describes the visual, fractographic, and metallographic evidence typically encountered when analyzing stress rupture of turbine airfoils. Stress-rupture fractures are generally heavily oxidized, tend to be rough in texture, and are primarily intergranular and/or interdendritic in appearance compared to smoother, transgranular fatigue type fractures. Often, gross plastic yielding is visible on a macroscopic scale. Commonly observed microstructural characteristics include creep voiding along grain boundaries and/or interdendritic regions. Internal voids can also nucleate at carbides and other microconstituents, especially in single crystal castings that do not possess grain boundaries.

Recurring, premature failures occurred in TiN-coated M2 gear hobs used to produce carbon steel ring gears. Fractographic and metallographic examination, microhardness testing, and chemical analysis by means of EDS revealed that the primary cause of failure was a coarse cellular carbide network, which created a brittle path for fracture to occur longitudinally. As the cellular carbide network must be dispersed and refined during hot working of the original bar of material, the hobs were not salvageable. Minor factors contributing to the hob failures were premature wear resulting from lower matrix hardness and high sulfur content of the material, which contributed to lower ductility through increased nucleation sites. It was recommended that the hob manufacturer specify a minimum amount of required reduction for the original bar of tool steel material, to provide for sufficient homogenization of the carbides in the resultant hob, and lower sulfur content.

A carbon-molybdenum (ASTM A209 Grade T1) steel superheater tube section in an 8.6 MPa (1250 psig) boiler cracked because of long-term overheating damage that resulted from prolonged exposure to metal temperatures between 482 deg C (900 deg F) and 551 deg C (1025 deg F). The outer diameter of the tube exhibited a crack (fissure) oriented approximately 45 deg to the longitudinal axis and 3.8 cm (1.5 in.) long. The inner diameter surface showed a fissure in the same location and orientation. Microstructure at the failure near the outer diameter surface exhibited evidence of creep cracking and creep void formation at the fissure. A nearly continuous band of graphite nodules was observed on the surface of the fissure. In addition to the graphite band formation, the microstructure near the failure exhibited carbide spheroidization from long-term overheating in all the tube regions examined. It was concluded that preferential nucleations of graphite nodules in a series of bands weakened the steel locally, producing preferred fracture paths. Formation of these graphite bands probably expedited the creep failure of the tube. Future failures may be avoided by using low-alloy steels with chromium additions such as ASTM A213 Grade T11 or T22, which are resistant to graphitization damage.