Spalled fragments from the work rolls of a steel bar straightening machine were received for failure analysis. Visual inspection coupled with optical and scanning electron microscopy were used as the principal analytical techniques for the investigation. Fractographic analysis revealed the presence of a characteristic fatigue crack propagation pattern (beach marks) and radial chevron marks indicating the occurrence of final overload through a brittle intergranular fracture. The collected evidence suggests that surface-initiated cracks propagated by fatigue led to spalling, resulting in severe work roll damage as well as machine downtime and increased maintenance costs.

This article describes the general root causes of failure associated with wrought metals and metalworking. This includes a brief review of the discontinuities or imperfections that may be the common sources of failure-inducing defects in bulk working of wrought products. The article discusses the types of imperfections that can be traced to the original ingot product. These include chemical segregation; ingot pipe, porosity, and centerline shrinkage; high hydrogen content; nonmetallic inclusions; unmelted electrodes and shelf; and cracks, laminations, seams, pits, blisters, and scabs. The article provides a discussion on the imperfections found in steel forgings. The problems encountered in sheet metal forming are also discussed. The article concludes with information on the causes of failure in cold formed parts.

A clamp used for securing the hot-air ducting system on fighter aircraft fractured in an area adjacent to a slot near the end of the strap after two or three years of service. The strap was 0.8 mm (0.032 in.) thick, and the V-section was 1.3 mm (0.050 in.) thick; both were made of 19-9 DL heat-resisting alloy. The operating temperature of the duct surrounded by the clamp was 425 to 540 deg C (800 to 1000 deg F). The life of the clamp was expected to equal that of the aircraft. Investigation (visual inspection, chemical analysis, hardness testing, and 540x/2700x images etched with oxalic acid) supported the conclusion that the clamp fractured by SCC because the work metal was sensitized. Sensitization occurred during long-term exposure to the service temperature; the effects of sensitization were intensified as a result of cold forming. Recommendations included using a work metal that is less susceptible to intergranular carbide precipitation.

In a continuously cast aluminum press stud, two small foreign metal slivers were found that had caused difficulties with the cable sheathing press. Spectroscopic examination revealed the slivers consisted of a chromium-molybdenum-vanadium steel with minor (unintentional) additions of copper, nickel, and cobalt. A steel of similar composition, X38Cr-MoV5 1 (W-No. 2343) was used for hot working tools. The sliver originated from a damaged press tool.

The primary purpose of this article is to describe general root causes of failure that are associated with wrought metals and metalworking. This includes a brief review of the discontinuities or imperfections that may be common sources of failure-inducing defects in the bulk working of wrought products. The article addresses the types of flaws or defects that can be introduced during the steel forging process itself, including defects originating in the ingot-casting process. Defects found in nonferrous forgings—titanium, aluminum, and copper and copper alloys—also are covered.

Flow forming technology has emerged as a promising, economical metal forming technology due to its ability to provide high strength, high precision, thin walled tubes with excellent surface finish. This paper presents experimental observations of defects developed during flow forming of high strength SAE 4130 steel tubes. The major defects observed are fish scaling, premature burst, diametral growth, microcracks, and macrocracks. This paper analyzes the defects and arrives at the causative factors contributing to the various failure modes.

An integral coupling and gear (Cr-Mo steel), used on a turbine-driven main boiler-feed pump, was removed from service after one year of operation because of excessive vibration. Spectrographic analysis and metallographic examination revealed the fact that gritty material in the gear teeth (found at visual inspection) was composed of the same material as the metal in the coupling. Beach marks and evidence of cold work, typical of fatigue failure, were found on the fracture surface. Chips remaining in the analysis cut were difficult to remove, indicating a strong magnetic field in the part. Evidence found supports the conclusions that failure of the coupling was by fatigue and that incomplete demagnetization of the coupling following magnetic-particle inspection caused retention of metal chips in the roots of the teeth. Improper lubrication caused gear teeth to overheat and spall, producing chips that eventually overstressed the gear, causing failure. Because the oil circulation system was not operating properly, metal chips were not removed from the coupling. Recommendations included checking the replacement coupling for residual magnetism and changing or filtering the pump oil to remove any debris.

The accident at Three Mile Island Unit No. 2 on 28 March 1979 was the worst nuclear accident in US history. By Jan 1990, it was possible to electrochemically machine coupons from the lower head using a specially designed tool. The specimens contained the ER308L stainless steel cladding and the A533 Grade B plate material to a depth of about mid-wall. The microstructures of these specimens were compared to that of specimens cut from the Midland, Michigan reactor vessel, made from the same grade and thickness but never placed in service. These specimens were subjected to known thermal treatments between 800 and 1100 deg C for periods of 1 to 100 min. Microstructural parameters in the control specimens and in those from TMI-2 were quantified. Selective etchants were used to better discriminate desired microstructural features, particularly in the cladding. This report is a progress report on the quantification of changes in both the degree of carbide precipitation and delta ferrite content and shape in the cladding as a function of temperature and time to refine the estimates of the maximum temperatures experienced.

A roll assembly consisting of a forged AISI type 440A stainless steel sleeve shrink fitted over a 4340 steel shaft and further secured with tapered keys on opposite ends was crated and shipped by air. Upon arrival, the sleeve was found to have cracked longitudinally between the keyways. A roll manufacturer had successfully used the above procedure for many years to make them. Analysis (visual inspection; 150x micrograph of sections etched with a mixture of 2 parts HNO3, 2 parts acetic acid, and 3 parts HCI; electron microscopy; and stress testing) supported the conclusion that superficial working of the metal, probably insufficient hot working, produced a microstructure in which the carbide particles were not broken up and evenly distributed. As a result, the grains were totally surrounded with brittle carbide particles. This facilitated the formation of a crack at a fillet in the keyway. Crack growth was rapid once the crack had initiated, causing brittle fracture to occur.

Two water pumps were taken out of service because of reduced output. Visual inspection revealed considerable material loss in both impellers, which were 25.4 cm (10 in.) in diam x 1.3 cm (0.5 in.) wide and made from a cast bronze alloy. Several similar water pumps operating under nearly identical conditions, drawing water from an open tank through a standpipe, had no observable failures. Etched micrographs 100x of samples taken from the impellers showed clean, pockmarked, severely eroded surfaces, characteristic of cavitation damage. Investigation also revealed that considerable quantities of air were being drawn into the system when water in the supply tank dropped below a certain level. It was concluded that cavitation erosion (due to the uptake of air) caused metal removal and microstructural damage in the impellers. Recommendations included adding a water-level control to the piping system and excluding air from the pump inlet.

The center portions of two adjacent low-carbon steel boiler tubes (made to ASME SA-192 specifications) ruptured during a start-up period after seven months in service. It was indicated by reports that there had been sufficient water in the boiler two hours before start-up. The microstructure near the rupture edge was revealed by metallographic examination to consist of ferrite and acicular martensite or bainite. The microstructure and the observed lack of cold work indicated a temperature above the transformation temperature of 727 deg C had been reached. Swelling of the tubes was disclosed by the wall thickness and OD of the tubing. The tubes were concluded to have failed due to rapid overheating.

Forged austenitic steel rings used on rotor shafts in two 100,000 kW generators burst from overstressing in a region of ventilation holes. A variety of causes contributed to the brittle fractures in the ductile austenitic alloy, including stress concentration by holes, work hardened metal in the bores, and a variable pattern of residual stress.

A cold-formed Grade TP 304 stainless steel swaged region of a reheater tube in service for about 8000 hours cracked because of sulfur-induced stress-corrosion cracking (SCC). Cracking initiated from the external surface and a high sulfur content was detected in the outer diameter and crack deposits. Comparison of the microstructure and hardness of the swaged region and unswaged Grade TP 304 stainless steel tube metal indicated that the swaged section was not annealed to reduce the effects of cold working. The high hardness created during swaging increased the stainless steel's susceptibility to sulfur-induced SCC. Because SCC requires water to be present, cracking most likely occurred during downtime or startups. To prevent future failures, the boiler should be kept dry during downtime to avoid formation of sulfur acids, and the swaged sections of the tubes should be heat treated after swaging to reduce or eliminate strain hardening of the metal.

A portable propane container with a name-plate soldered onto it exploded in service. When the vessel was inspected afterwards, it was found to have developed a crack in the top end plate. A portion of the end plate cut out to include the midlength and one termination of the crack was examined microscopically. This revealed that the crack was associated with intergranular penetration by molten metal. The microstructure in general was indicative of a good-quality mild steel. It was evident from that solder that was responsible for the penetration and that fused brass from the hand wheel had not played any part. Tensile stress was present at the time of the failure sufficiently high to enable solder penetration to take place. The use of soft solder as a medium for attaching name-plates directly on to stressed steel parts is not recommended. It would be preferable to use a welded-on patch plate or to employ one of the high-strength, non-metallic adhesives.

A spoon that was twisted and broken by a person claiming to possess parapsychic powers was submitted for failure analysis. Exemplar tests were conducted on material taken from the bowl region of the same spoon. In addition, tests on other unbroken samples of spoons were evaluated in order to establish both macroscopic and microscopic comparative behavior. These controlled tests produced known failure mechanisms and their respective fracture morphology in this material. A direct comparison could then be made with the unknown failure. The paper identifies a method of analysis that should be applied when analyzing failures of unknown origin.

Metal-framed polycarbonate (PC) ophthalmic lenses shattered from acetone solvent-induced cracking. The lenses exhibited primary and secondary cracks with solvent swelling and crazing. A laboratory accident splashed acetone onto the lenses. The metal frames gripped approximately two-thirds of the lenses' periphery and introduced an unevenly distributed force on the lenses. To prevent future failures, it was recommended to protect PC from service environments with solvents, such as acetone; or from marking pens, adhesives or soaps which contain undesirable solvents; and to not apply excessive stress on ophthalmic lenses in the form of working or residual stresses.

Nineteen out of 26 bolts in a multistage water pump corroded and cracked after a short time in a severe working environment containing saline water, CO 2 , and H 2 S. The failed bolts and intact nuts were to be made from a special type of stainless steel as per ASTM A 193 B8S and A 194. However, the investigation (which included visual, macroscopic, metallographic, SEM, and chemical analysis) showed that austenitic stainless steel and a nickel-base alloy were used instead. The unspecified materials are more prone to corrosion, particularly galvanic corrosion, which proved to be the primary failure mechanism in the areas of the bolts directly exposed to the working environment. Corrosion damage on surfaces facing away from the work environment was caused primarily by chloride stress-corrosion cracking, aided by loose fitting threads. Thread gaps constitute a crevice where an aggressive chemistry is allowed to develop and attack local surfaces.

A CrN coated restrike punch was made of WR-95 (similar to H-11), which was fluidized bed nitrided. The coated punch was used on hot Inconel at about 1040 deg C (1900 deg F). However, a water-soluble graphite coolant was used to maintain the punch temperature at 230 deg C (450 deg F). Visual and binocular inspection at 64+ revealed presence of cracks and complete washout of coating in the working area of the failed punch. Comparison of metallographic cross sections of used and unused punches revealed a significant microstructural transformation in case of the used punch. Presence of a yellow porous layer was clearly evident between the nitrided layer and the coating, in case of the used punch. Cracks were observed to propagate from the outer surface into the bulk. Oxidation was evident along the cracks. The microstructural transformation observed in the case of the used punch was a clear indication of high temperature exposure (due to insufficient cooling) during application. The most probable cause of failure was thermal fatigue.

While a chain sling was being used to lift a casting one of the links ruptured. The sling, reputed to be of the electrically-welded steel type, was at least eight years old and had been overhauled several times during its working life. Examination showed the links were scarf-welded. Furthermore, the welds were at the ends and not at the sides as is usual in the case of electrically-welded chains. A transverse section from one side of a link was examined microscopically. This showed the material to be wrought-iron of satisfactory quality. It was concluded this chain sling had been made from wrought-iron, forge welded in the usual manner, and that it was not electrically-welded steel as had been supposed. Failure was attributed to embrittlement in service of the surface material of the links. If it had been realized that the sling was made from wrought-iron then it would doubtless have been subjected to periodical annealing in accordance with Statutory requirements, which would have restored the ductility of the surface material.