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material failure analysis
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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001636
EISBN: 978-1-62708-217-4
... Abstract A Lynx helicopter from the Royal Netherlands Navy lost a rotor blade during preparation for take-off. The blade loss was due to failure of a rotor hub arm by fatigue. The arm was integral to the titanium alloy rotor hub. An extensive material based failure analysis covered the hub...
Abstract
A Lynx helicopter from the Royal Netherlands Navy lost a rotor blade during preparation for take-off. The blade loss was due to failure of a rotor hub arm by fatigue. The arm was integral to the titanium alloy rotor hub. An extensive material based failure analysis covered the hub manufacture, service damage, and estimates of service stresses. There was no evidence for failure due to poor material properties. However, fractographic and fracture mechanics analyses of the service failure, a full scale test failure, and specimen test failures indicated that the service fatigue stress history could have been more severe than anticipated. This possibility was subsequently supported by a separate investigation of the assumed and actual fatigue loads and stresses.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001833
EISBN: 978-1-62708-241-9
... material samples from the near-failure region and by thermodynamic analysis. A scanning Auger microprobe, SEM, and commercial thermodynamic software codes were used in the investigation. Results indicated that the boiler failure was caused by grain-boundary segregation of phosphorous, tin, and nitrogen...
Abstract
The failure of a boiler operating at 540 °C and 9.4 MPa was investigated by examining material samples from the near-failure region and by thermodynamic analysis. A scanning Auger microprobe, SEM, and commercial thermodynamic software codes were used in the investigation. Results indicated that the boiler failure was caused by grain-boundary segregation of phosphorous, tin, and nitrogen and the in-service formation of carbide films and granules on the grain boundaries.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.matlhand.9781627082242
EISBN: 978-1-62708-224-2
Book Chapter
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006797
EISBN: 978-1-62708-295-2
..., errors in the specification of the material, and faulty process and their corrective measures to meet specifications. It discusses the general process of material failure analysis and special types of distortion and deformation failure. deformation distortion material failure analysis...
Abstract
Distortion often is observed in the analysis of other types of failures, and consideration of the distortion can be an important part of the analysis. This article first considers that true distortion occurs when it was unexpected and in which the distortion is associated with a functional failure. Then, a more general consideration of distortion in failure analysis is introduced. Several common aspects of failure by distortion are discussed and suitable examples of distortion failures are presented for illustration. The article provides information on methods to compute load limits, errors in the specification of the material, and faulty process and their corrective measures to meet specifications. It discusses the general process of material failure analysis and special types of distortion and deformation failure.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001803
EISBN: 978-1-62708-241-9
... surface of the plate near the fracture origin Abstract Metallurgical SEM analysis provides many insights into the failure of biomedical materials and devices. The results of several such investigations are reported here, including findings and conclusions from the examination a total hip...
Abstract
Metallurgical SEM analysis provides many insights into the failure of biomedical materials and devices. The results of several such investigations are reported here, including findings and conclusions from the examination a total hip prosthesis, stainless steel and titanium compression plates, and hollow spinal rods. Some of the failure mechanisms that were identified include corrosive attack, corrosion plus erosion-corrosion, inclusions and stress gaps, production impurities, design flaws, and manufacturing defects. Failure prevention and mitigation strategies are also discussed.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.design.c0065826
EISBN: 978-1-62708-233-4
... • Miller B.A. , Materials Selection for Failure Prevention , Failure Analysis and Prevention , Vol 11 , ASM Handbook , ASM International , 2002 , p 24 – 39 10.31399/asm.hb.v11.a0003501 • Warke W. R. , Stress-Corrosion Cracking , Failure Analysis and Prevention , Vol 11 , ASM...
Abstract
The wires used in a wet precipitator for cleaning the gases coming off a basic oxygen furnace failed. The system consisted of six precipitators, three separate dual units, each composed of four zones. Each zone contained rows of wires (cold drawn AISI 1008 carbon steel) suspended between parallel collector plates. It was determined that the 1008 wires failed because of corrosion fatigue. It was decided to replace all of the wires in the two zones with the highest rates of failure with cold-drawn type 304 austenitic stainless steel wire. These expensive wires, however, failed after a week by transgranular SCC. Annealed type 430 ferritic stainless steel was subsequently suggested to prevent further failures.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003526
EISBN: 978-1-62708-180-1
... analysis microelectronics piping pressure vessel FAILURE of a structural or mechanical component usually can be associated with materials-related problems and/or design-related problems (which may include, depending on the definition of design, unexpected service environment). Materials failure...
Abstract
This article provides information on the development of finite element analysis (FEA) and describes the general-purpose applications of FEA software programs in structural and thermal, static and transient, and linear and nonlinear analyses. It discusses special-purpose finite element applications in piping and pressure vessel analysis, impact analysis, and microelectronics. The article describes the steps involved in the design process using the FEA. It concludes with two case histories that involve the use of FEA in failure analysis.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006773
EISBN: 978-1-62708-295-2
... Abstract When complex designs, transient loadings, and nonlinear material behavior must be evaluated, computer-based techniques are used. This is where the finite-element analysis (FEA) is most applicable and provides considerable assistance in design analysis as well as failure analysis...
Abstract
When complex designs, transient loadings, and nonlinear material behavior must be evaluated, computer-based techniques are used. This is where the finite-element analysis (FEA) is most applicable and provides considerable assistance in design analysis as well as failure analysis. This article provides a general view on the applicability of finite-element modeling in conducting analyses of failed components. It highlights the uses of finite-element modeling in the area of failure analysis and design, with emphasis on structural analysis. The discussion covers the general development and both general- and special-purpose applications of FEA. The special-purpose applications of FEA covered are piping and pressure vessel analysis, impact analysis, and microelectronic and microelectromechanical systems analysis. The article provides case histories that involved the use of FEA in failure analysis.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.9781627082952
EISBN: 978-1-62708-295-2
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003500
EISBN: 978-1-62708-180-1
..., design deficiencies, material defects, manufacturing/installation defects, and service life anomalies, with examples. The article describes several common charting methods that may be useful in performing an RCA. It also discusses other failure analysis tools, including review of all sources of input...
Abstract
This article briefly introduces the concepts of failure analysis and root cause analysis (RCA), and the role of failure analysis as a general engineering tool for enhancing product quality and failure prevention. It reviews four fundamental categories of physical root causes, namely, design deficiencies, material defects, manufacturing/installation defects, and service life anomalies, with examples. The article describes several common charting methods that may be useful in performing an RCA. It also discusses other failure analysis tools, including review of all sources of input and information, people interviews, laboratory investigations, stress analysis, and fracture mechanics analysis. The article concludes with information on the categories of failure and failure prevention.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006753
EISBN: 978-1-62708-295-2
..., and material, which are discussed in the following sections along with examples. The tools available for failure analysis are then covered. Further, the article describes the categories of mode of failure: distortion or undesired deformation, fracture, corrosion, and wear. It provides information...
Abstract
This article briefly introduces the concepts of failure analysis, including root-cause analysis (RCA), and the role of failure analysis as a general engineering tool for enhancing product quality and failure prevention. It initially provides definitions of failure on several different levels, followed by a discussion on the role of failure analysis and the appreciation of quality assurance and user expectations. Systematic analysis of equipment failures reveals physical root causes that fall into one of four fundamental categories: design, manufacturing/installation, service, and material, which are discussed in the following sections along with examples. The tools available for failure analysis are then covered. Further, the article describes the categories of mode of failure: distortion or undesired deformation, fracture, corrosion, and wear. It provides information on the processes involved in RCA and the charting methods that may be useful in RCA and ends with a description of various factors associated with failure prevention.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006759
EISBN: 978-1-62708-295-2
... failure analysis. It describes the general considerations for bulk and microscale chemical analysis in failure analysis, the most effective techniques to use for organic or inorganic materials, and examples of using these techniques. The article discusses the processes involved in the chemical analysis...
Abstract
Chemical analysis is a critical part of any failure investigation. With the right planning and proper analytical equipment, a myriad of information can be obtained from a sample. This article presents a high-level introduction to techniques often used for chemical analysis during failure analysis. It describes the general considerations for bulk and microscale chemical analysis in failure analysis, the most effective techniques to use for organic or inorganic materials, and examples of using these techniques. The article discusses the processes involved in the chemical analysis of nonmetallics. Advances in chemical analysis methods for failure analysis are also covered.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003525
EISBN: 978-1-62708-180-1
... plastic resin thermogravimetric analysis thermomechanical analysis visual examination THE ULTIMATE OBJECTIVE of a failure analysis is to ascertain the mode and the cause of the failure, regardless of the material from which the part was fabricated. The investigation is performed in generally...
Abstract
This article reviews the analytical techniques most commonly used in plastic component failure analysis. These include the Fourier transform infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis. The descriptions of the analytical techniques are supplemented by a series of case studies that include pertinent visual examination results and the corresponding images that aid in the characterization of the failures. The article describes the methods used for determining the molecular weight of a plastic resin. It explains the use of mechanical testing in failure analysis and also describes the considerations in the selection and use of test methods.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003573
EISBN: 978-1-62708-180-1
... and is commonly computed by classical design or limit analysis. This article discusses the common aspects of failure by distortion with suitable examples. Analysis of a distortion failure often must be thorough and rigorous to determine the root cause of failure and to specify proper corrective action...
Abstract
Distortion failure occurs when a structure or component is deformed so that it can no longer support the load it was intended to carry. Every structure has a load limit beyond which it is considered unsafe or unreliable. Estimation of load limits is an important aspect of design and is commonly computed by classical design or limit analysis. This article discusses the common aspects of failure by distortion with suitable examples. Analysis of a distortion failure often must be thorough and rigorous to determine the root cause of failure and to specify proper corrective action. The article summarizes the general process of distortion failure analysis. It also discusses three types of distortion failures that provide useful insights into the problems of analyzing unusual mechanisms of distortion. These include elastic distortion, ratcheting, and inelastic cyclic buckling.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001668
EISBN: 978-1-62708-232-7
... Abstract A detailed investigative failure analysis was conducted on an autoclave which blew apart in a furnace for no apparent reason. Bolt failure resulted in separation of the autoclave lid and subsequent destruction of the furnace. Analysis using metallography, fractography, mechanical...
Abstract
A detailed investigative failure analysis was conducted on an autoclave which blew apart in a furnace for no apparent reason. Bolt failure resulted in separation of the autoclave lid and subsequent destruction of the furnace. Analysis using metallography, fractography, mechanical testing and exemplar tests were performed on the bolt material. Mechanical engineering analysis and leak-before-break criteria were extensively analyzed. Results led to only one possible conclusion: that an explosion occurred within the autoclave. Suggestions for autoclave design are presented as a result of the analysis.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003518
EISBN: 978-1-62708-180-1
..., including those that come from a deficient design, poor material, or mistakes in manufacturing. Whether those “defects” exist in a given component that is being subjected to the failure analysis process can often only be determined by someone with a materials background. The reasons for this are related...
Abstract
Failure analysis is a process that is performed to determine the causes or factors that have led to an undesired loss of functionality. This article describes some of the factors and conditions that might be considered when approaching a failure analysis problem. It focuses on the key principles, objectives, practices, and procedures of failure analysis. The article provides guidelines on the preparation of a protocol for a failure analysis. It also demonstrates the proper approaches to failure analysis.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001297
EISBN: 978-1-62708-215-0
... Microstructural analysis of the spar revealed no material anomalies that would have contributed to the failure. Sections were taken through the failed spar to determine the extent of the corrosive attack. The sectioning revealed spherical pits at the surface of the cavity wall with isolated intergranular attack...
Abstract
A helicopter tail rotor blade spar failed in fatigue, allowing the blade to separate during flight. The 2014-T652 aluminum alloy blade had a hollow spar shank filled with lead wool ballast and a thermoset polymeric seal. A corrosion pit was present at the origin of the fatigue zone and numerous trails of corrosion pits were located on the spar cavity's inner surfaces. The corrosion pitting resulted from the failure of the thermoset seal in the spar shank cavity. The seal failure allowed moisture to enter into the cavity. The moisture then served as an electrolyte for galvanic corrosion between the lead wool ballast and the aluminum spar inner surface. The pitting initiated fatigue cracking which led to the spar failure.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001115
EISBN: 978-1-62708-214-3
... to Failure During a workover of the well in January 1984, the 9% Ni tubing parted three times as it was being pulled from the well. These failures were the first suffered by any of the 9% Ni tubing. A representative failure was selected for analysis. Visual Examination of General Physical Features...
Abstract
During a work over of an oil well, the 9% Ni steel production tubing parted three times as it was being pulled from the well. The tubing had performed satisfactorily for more than 30 years in the well A representative failure, a circumferential fracture in a connection, was analyzed. Reported to be a hydril CS connection, the pin end parted near the last threads. The external surface exhibited mechanical damage marks from the fishing operation. No signs of external corrosion or damage were detected. Visual surface examination revealed shear lips at the outside pipe, indicating that the fracture initiated at the inside surface and grew across the wall. Longitudinal cross sections revealed heavy corrosion damage to the inside pipe surface. Metallographic examination indicated that the tubing failed as a result of severe weakening from internal corrosion. Gray-colored corrosion deposits, which penetrated the pipe throughout the grain boundaries of the material and concentrated in the matrix in a layer near the inside surface of the pipe, were observed. The presence of H2S in the produced fluids and the appearance of the gray deposit indicated that the tube suffered H2S corrosion. Chemical analysis of the base metal and corrosion deposits did not detect iron or nickel sulfides, however Replacement of the remaining pipe strings according to a scheduled program was recommended. Because 9% Ni steel was not available, 13% Cr martensitic stainless steel was recommended as a replacement.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001042
EISBN: 978-1-62708-214-3
... for an extended time before complete failure occurred. Chemical Analysis/Identification Material Chemical analysis of the leaf spring was performed to determine the material composition. The leaf spring material contained 0.053% C, 1.39% Mn, 0.006% S, 18.4% Cr, and 9.6% Ni, typical of a normal grade...
Abstract
Failure occurred in a type 304 stainless steel leaf spring attached to the undercarriage assembly of an airport shuttle train. Failure analysis showed that the fracture was caused by low-cycle, reversed bending fatigue. The stresses leading to failure were imposed by poor alignment. It was recommended that improved assembly procedures be used and that, if another failure occurred, a steel of higher fatigue strength be used.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006754
EISBN: 978-1-62708-295-2
..., assemblies, or structures, and its approach is consistent with the knowledge base of a person trained in materials engineering. The contribution of the materials engineer to the advancement of the scientific foundation of failure analysis has been great in the last few decades. This is evidenced by the fact...
Abstract
Failure analysis is a process that is performed in order to determine the causes or factors that have led to an undesired loss of functionality. This article is intended to demonstrate proper approaches to failure analysis work. The goal of the proper approach is to allow the most useful and relevant information to be obtained. The discussion covers the principles and approaches in failure analysis work, objectives and scopes of failure analysis, the planning stages for failure analysis, the preparation of a protocol for a failure analysis, practices used by failure analysts, and procedures of failure analysis.