Chain link, a part of a mechanism for transferring hot or cold steel blooms into and out of a reheating furnace, broke after approximately four months of service. The link was cast from 2% Cr austenitic manganese steel and was subjected to repeated heating to temperatures of 455 to 595 deg C (850 to 1100 deg F). Examination included visual inspection, macrograph of a nital-etched specimen from an as-received chain link 1.85x, micrographs of a nital-etched specimen from an as-received chain link 100x/600x, normal microstructure of as-cast standard austenitic manganese steel 100x, micrograph of a nital-etched specimen that had been austenitized 20 min at 1095 deg C (2000 deg F) and air cooled 315x, and micrograph of the same specimen after annealing 68 h at 480 deg C (900 deg F) 1000x). Investigation supported the conclusions that the chain link failed in a brittle manner, because the austenitic manganese steel from which it was cast became embrittled after being reheated in the temperature range of 455 to 595 deg C (850 to 1100 deg F) for prolonged periods of time. The alloy was not suitable for this application, because of its metallurgical instability under service conditions.

This paper deals with disk drive failures that occur in the interface area between the head and disk. The failures often lead to the loss of stored data and are characterized by circumferential microscratches that are usually visible to the unaided eye. The recording media in disk drives consists of a metal, glass, ceramic, or plastic substrate coated with a magnetic material. Data errors are classified as ‘soft’ or ‘hard’ depending on their correctability. Examination has shown that hard errors are the result of an abrasive wear process that begins with contact between head and disk asperities. The contact generates debris that, as it accumulates, increases contact pressure between the read-write head and the surface of the disk. Under sufficient pressure, the magnetic coating material begins wearing away, resulting in data loss.

An investigation of a Stirling engine after an aborted test run revealed that the regenerator screens had suffered substantial damage. During the run, the individual screens oscillated as the helium working fluid was shuttled through the regenerator. In localized areas, the 41 mu m (1600 mu in.) diam type 304 stainless steel wire screening had been torn and pieces were missing. Scanning electron microscope revealed that the fracture had occurred at wire crossover locations by a fatigue mechanism. The problem was solved by sintering the individual screens into a single unit.

Failure occurred in a type 304 stainless steel leaf spring attached to the undercarriage assembly of an airport shuttle train. Failure analysis showed that the fracture was caused by low-cycle, reversed bending fatigue. The stresses leading to failure were imposed by poor alignment. It was recommended that improved assembly procedures be used and that, if another failure occurred, a steel of higher fatigue strength be used.

The 1040 steel crankshaft in a reciprocating engine cracked within one year of operation. The journals of the main and crankpin bearings were inspected by the magnetic-particle method. Three to six indications of 1.5 to 9.5 mm long discontinuities were observed in at least four of the main-bearing journals. A crack along the fillet, almost entirely through the web, was observed in one of the main-bearing journals. Numerous coarse segregates, identified as sulfide inclusions, were identified by macroetching the surface during metallographic examination of a section taken through the main-bearing journal at the primary crack. Fatigue cracking with low-stress high-cycle characteristics was disclosed during macroscopic examination of the crack surface. Sulfide inclusions, which acted as stress raisers, were found to be present in the region where cracking originated. As a corrective measure, ultrasonic inspection was used in addition to magnetic-particle inspection to detect discontinuities.

A crane long-travel worm drive shaft was found to be chipped during unpacking after delivery. Chemical analysis showed that the steel (EN36A with a case depth of 1 mm, or 0.04 inch did not meet specifications. Magnetic particle inspection revealed a crack on the side of the shaft opposite the chip. Metallographic examination indicated that the case depth was approximately 2 mm (0.08 in.) and that a repair weld of an earlier chip had been made in the cracked area. The chipping was attributed to excessive case depth and rough handling. It was recommended that the shaft be returned to the manufacturer and a replacement requested.

Cracks formed on cylinder inserts from a water-cooled locomotive diesel engine, on the water side in the neck between the cylindrical part and the collar. Cracks were revealed by magnetic-particle inspection. As a rule, several parallel cracks had appeared, some of which were very fine. The part played by corrosion in the formation of the cracks was demonstrated with the help of metallographic techniques. The surface regions of the cracks widened into funnel form, which is a result of the corrosive influence of the cooling water. Actual corrosion pits could not be found indicating that the vibrational stresses had a greater share in the damage than the corrosive influence. Cracks appeared initially only in those engines in which no corrosion inhibitor had been added to the cooling water. The cracking was caused by corrosion fatigue. The combined presence of a corrosive medium and cyclical operating stress was needed to cause cracks. No cracks appeared when corrosion inhibitor was added to the cooling water.

This article presents tools, techniques, and procedures that engineers and material scientists can use to investigate plastic part failures. It also provides a brief survey of polymer systems and the key properties that need to be measured during failure analysis. It describes the characterization of plastics by infrared and nuclear magnetic resonance spectroscopy, differential scanning calorimetry, differential thermal analysis, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis. The article also discusses the use of X-ray diffraction for analyzing crystal phases and structures in solid materials.

Numerous flaws were detected in a steam turbine rotor during a scheduled inspection and maintenance outage. A fracture-mechanics-based analysis of the flaws showed that the rotor could not be safely returned to service. Material, samples from the bore were analyzed to evaluate the actual mechanical properties and to determine the metallurgical cause of the observed indications. Samples were examined in a scanning electron microscope and subjected to chemical analysis and several mechanical property tests, including tensile, Charpy V-notch impact, and fracture toughness. The material was found to be a typical Cr-Mo-V steel, and it met the property requirements. No evidence of temper embrittlement was found. The analyses showed that the observed flaws were present in the original forging and attributed them to lack of ingot consolidation. A series of actions, including overboring of the rotor to remove indications close to the surface and revision of starting procedures, were implemented to extend the remaining life of the rotor and ensure its fitness for continued service.

The repeated occurrence of random cracks in the fillet radius portion of low-alloy steel (38KhA) end frame forgings following heat treatment was investigated. Microstructural analyses were carried out on both the failed part and disks of the rolled bar from which the part was made. Subsurface cracks were found to be zigzag and discontinuous as well as intergranular in nature. A mixed mode of fracture involving ductile and brittle flat facets was observed. Micropores and rod-shaped manganese sulfide inclusions were also noted. The material had a hydrogen content of 22 ppm, and cracking was attributed to hydrogen embrittlement. Measurement of hydrogen content in the raw material prior to fabrication was recommended. Careful control of acid pickling procedures for descaling of the hot-rolled bars was also deemed necessary.

The heads of two AISI 8740 steel bolts severed while being installed into an Army tank recoil mechanism. Both broke into two pieces at the head-to-shank radius and the required torque value had not been attained nor exceeded prior to the failure. A total of 69 bolts from inventory and the field were tested by magnetic particle inspection. One inventory bolt failed because of a transverse crack near the head-to-shank radius. It was deduced that either a 100% magnetic particle inspection had not been conducted during bolt manufacturing, or the crack went undetected during the original inspection. Optical and electron microscopy of the broken bolts revealed topographies and the presence of black oxide consistent with quench cracking. The two bolts failed during installation due to the presence of pre-existing quench cracks. Recommendations to prevent future failures include: ensuring that 100% magnetic particle inspections are conducted after bolts are tempered; using dull cadmium plate or an alternative to the electrode position process, such as vacuum cadmium plate or ion-plate or ion-plated aluminum, to mitigate the potential for delayed failures due to hydrogen embrittlement or stress-corrosion cracking; ensuring that the radius at the shoulder/shank interface conforms to specifications; and replacing all existing bolts with new or reinspected inventory bolts.

A number of machined end frame steel forgings made of Cr-Si-Mn alloy showed tiny cracks during magnetic particle inspection after heat treatment. The cracks were mostly confined to base edges and fillet radius. No significant abnormality was observed in chemical composition and microstructure. SEM, optical microscopy, and gas analysis revealed that the subsurface discontinuous cracks at the bore edges and in the fillet radius of the heat-treated end frame component had occurred due to hydrogen embrittlement, and not because of faulty heat treatment. This conclusion was supported by the presence of cracklike indications in machined bore surface of the annealed part.

Several heavy truck Cr-Mo steel steering arms in service less than three years fractured during stationary or low-speed turning maneuvers that required power-assisted steering. Metallographic examination of the cracked AISI 4135 arms, heat treated to a hardness of 285 to 341 HB, revealed that fatigue crack initiation occurred from the tip of oxide scale inclusions forged into the U-shaped arm at the inside radius. Corrective action involved redesigning the steering arm to increase the minimum forging radius and reduce the stress level at the inner-bend radius, and reducing the level of power assistance to the wheels to encourage the driver to put the vehicle in motion prior to turning.

A failed spiral gear and pinion set made from 4320H Ni-Cr-Mo alloy steel operating in a high-speed electric traction motor gear unit driving a rapid transit train were submitted for analysis. The pinion was intact, but the gear had broken into two sections that resulted when two fractured areas went through the body of the gear. Wheel mileage of the assembly was 34,000 miles at the time of failure. All physical and metallurgical characteristics were well within specified standards, and both parts should have withstood normal loading conditions. The primary mode of failure was tooth bending fatigue of the gear from the reverse direction near the toe end. The cause of failure was a crossed-over tooth bearing condition that placed loads at the heel end when going forward and at the toe end when going in reverse. The condition was too consistent to be a deflection under load; therefore, it most likely was permanent misalignment within the assembly.

Six cracked A36 steel gusset plates that formed part of the roof trusses of a large manufacturing facility were discovered during a routine final inspection of a new building construction. Two different-size plates from different locations in the building were removed and tested. It was determined that the gusset plates failed in the heat-affected zone via an intergranular microcracking mode due to hydrogen-assisted underbead and toe-weld cracking. Proper nondestructive testing techniques for magnetic particle and radiographic inspection of the plate-weld gusset areas were recommended.

A 4340 steel piston engine crankshaft in a transport aircraft failed catastrophically during flight. The fracture occurred in the pin radius zone. Fractographic studies established the mode of failure as fatigue under a complex combination of bending and torsional stresses. SEM examination revealed that the fracture origin was a subsurface defect-a hard refractory (Al2O3) inclusion—in the zone close to the pin radius. Chemical analysis showed the crankshaft material to be of inferior quality. It was recommended that magnetic particle inspection using the dc method be used to cheek for cracks during periodic maintenance overhauls.

Radial cracking occurred adjacent to 11 vanes in a 19-vane impeller operating in a chemical plant environment. The impeller vanes were fillet welded to both the disk and the cover Cracks were next to the fillet welds and near the cover outer diameter They generally did not extend to the outer diameter. The entire impeller surface was tested by the dry magnetic particle method. Visual and microstructural examinations revealed intergranular cracking. Energy-dispersive spectroscopy of corrosion products contained in the cracks disclosed the presence of chlorine and sulfur The failure was attributed to stress-corrosion cracking caused by a corrosive atmosphere.

As the result of a leak detected in a plate-formed header at PENELEC'S Shawville Unit No. 3, an extensive failure investigation was initiated to determine the origin of cracking visible along the longitudinal weld seam. Fabricated from SA387-D material and designed for a superheater outlet temperature of 566 deg C, the 11.4 cm thick header had operated for approximately 187,000 h at the time of the failure. Discussion focuses on the results of a metallographic examination of boat samples removed from the longitudinal seam weldment in the vicinity of the failure and at other areas of the header where peak temperatures were believed to have been reached. The long-term mechanical properties of the service-exposed base metal and creep-damaged weld metal were determined by creep testing. Based on the utility's decision to replace the header within one to three years, an isostress overtemperature lead specimen approach was taken, whereby failure of a test specimen in the laboratory would precede failures in the plant. These tests revealed approximately a 2:1 difference in life for the base metal as compared to weld metal.

A cracked, martensitic stainless steel, low-pressure turbine blade from a 623 MW turbine generator was found to exhibit fatigue cracks during a routine turbine inspection. The blade was cracked at the first notch of the fir tree and the cracks initiated at pits induced by chloride attack. Examination of the blade microstructure at the fracture origins revealed oxide-filled pits and transgranular cracks. The oxide filled cracks appeared to have originated at small surface pits and probably propagated in a fatigue or corrosion-fatigue fracture mode. It was recommended that the sources of the chlorides be eliminated and that the remaining blades be inspected at regular maintenance intervals for evidence of cracking.

A crankshaft flange from a marine diesel engine illustrated a less-common case of fretting-fatigue cracking. The crankshaft was from a main engine of a sea-going passenger/vehicle ferry. The afterface of the flange was bolted to the flange of a shaft driving the gearbox. Cracks observed were sharp, transgranular, and not associated with any decarburization or other microstructural anomalies in the steel. Cracking of this main engine crankshaft flange was very likely a consequence of fatigue cracking initiated at fretting damage. The cause of the fretting was from loosening of the bolts.