This paper deals with disk drive failures that occur in the interface area between the head and disk. The failures often lead to the loss of stored data and are characterized by circumferential microscratches that are usually visible to the unaided eye. The recording media in disk drives consists of a metal, glass, ceramic, or plastic substrate coated with a magnetic material. Data errors are classified as ‘soft’ or ‘hard’ depending on their correctability. Examination has shown that hard errors are the result of an abrasive wear process that begins with contact between head and disk asperities. The contact generates debris that, as it accumulates, increases contact pressure between the read-write head and the surface of the disk. Under sufficient pressure, the magnetic coating material begins wearing away, resulting in data loss.

Chain link, a part of a mechanism for transferring hot or cold steel blooms into and out of a reheating furnace, broke after approximately four months of service. The link was cast from 2% Cr austenitic manganese steel and was subjected to repeated heating to temperatures of 455 to 595 deg C (850 to 1100 deg F). Examination included visual inspection, macrograph of a nital-etched specimen from an as-received chain link 1.85x, micrographs of a nital-etched specimen from an as-received chain link 100x/600x, normal microstructure of as-cast standard austenitic manganese steel 100x, micrograph of a nital-etched specimen that had been austenitized 20 min at 1095 deg C (2000 deg F) and air cooled 315x, and micrograph of the same specimen after annealing 68 h at 480 deg C (900 deg F) 1000x). Investigation supported the conclusions that the chain link failed in a brittle manner, because the austenitic manganese steel from which it was cast became embrittled after being reheated in the temperature range of 455 to 595 deg C (850 to 1100 deg F) for prolonged periods of time. The alloy was not suitable for this application, because of its metallurgical instability under service conditions.

An integral coupling and gear (Cr-Mo steel), used on a turbine-driven main boiler-feed pump, was removed from service after one year of operation because of excessive vibration. Spectrographic analysis and metallographic examination revealed the fact that gritty material in the gear teeth (found at visual inspection) was composed of the same material as the metal in the coupling. Beach marks and evidence of cold work, typical of fatigue failure, were found on the fracture surface. Chips remaining in the analysis cut were difficult to remove, indicating a strong magnetic field in the part. Evidence found supports the conclusions that failure of the coupling was by fatigue and that incomplete demagnetization of the coupling following magnetic-particle inspection caused retention of metal chips in the roots of the teeth. Improper lubrication caused gear teeth to overheat and spall, producing chips that eventually overstressed the gear, causing failure. Because the oil circulation system was not operating properly, metal chips were not removed from the coupling. Recommendations included checking the replacement coupling for residual magnetism and changing or filtering the pump oil to remove any debris.

Alloy steel forgings used as structural members of a ski chair lift grip mechanism were identified to have contained forging laps (i.e., sharp-notched discontinuities) during an annual magnetic particle inspection of all chair lift grip structural members at a mountain resort. The material was confirmed to be 34Cr-Ni-Mo6. A heavy oxide on the dark area of one of the broken-open laps was revealed by scanning electron microscopy in conjunction with EDS. A bright area that contained ductile dimple rupture was observed adjacent to the dark area. The oxidized portion of the fracture was established to be the preexisting forging lap while the bright area was created during the breaking-open process. As a corrective action all forgings showing laps were recommended to be removed from service. Critical review and revision of the forging process and revisions to the nondestructive evaluation procedures at the forging supplier was recommended.

Hydraulic cylinder housings were being fabricated from 4140 grade seamless steel tubing. During production, magnetic-particle inspection indicated the presence of circumferential and longitudinal cracks in a large number of cylinders. Analysis (visual inspection, dye penetrant inspection, 50x/90x/400x SEM micrographs, and metallographic analysis) supports the conclusion that the cracking problem in these components was identified as quench cracks due to their brittle, intergranular nature and the characteristic temper oxide on the fracture surfaces. Although the steel met the compositional requirements of SAE 4140, the sulfur level was 0.022% and would account for the formation of the sulfide stringers observed. Apparently, the combination of the clustered, stringer-type inclusions and the quenching conditions were too severe for this component geometry. The result was a high incidence of quench cracks that rendered the parts useless. Recommendations included changing the specification, requiring the steel to have lower sulfur concentrations. Magnetic-particle cleanliness standards should be imposed that will exclude material with harmful clusters of sulfide stringers, for example, modified AMS 2301.

The silver layer on a thrust bearing face experienced electrostatic discharge attack (the bombardment of an in-line series of individual sparks onto the soft bearing face), which destroyed the integrity of the bearing surface. The electrical attack appeared as scratches to the naked eye. Macrophotography showed that the attack was more severe at one edge of each pad, resulting in deeper grooving and a buildup of deposits, mostly silver sulfides. Microstructural analysis of a cross section indicated that the interface between the silver overlay and the substrate (beryllium copper) was sound and free of voids and foreign material. Corrosion products contained a large quantity of sulfur. The probable cause of the attack was the presence of electrical current within the system, with sulfides a possible contributing factor. Elimination of residual magnetism and grounding of the rotating system at appropriate locations were recommended.

A heavily worked 304 stainless steel wire basket recrystallized and distorted while in service at 650 deg C (1200 deg F). This case study demonstrates that heavily cold worked austenitic stainless steel components can experience large losses in creep strength, and potentially structural collapse, under elevated temperature service, even at temperatures more than 300 deg C (540 deg F) below the normal solution annealing temperature. The creep strength of the recrystallized 304/304L steel was more than 1000 times less than that achievable with solution annealed 304H. These observations are consistent with limitations (2000 Addendum to ASME Boiler and Pressure Vessel Code) on the use of cold worked austenitic stainless steels for elevated temperature service.

Failure occurred by fatigue cracking of links from chains which were used to replace the ropes on grabs of the multirope type. In the first example, the links were made from high tensile steel rod. The fracture in the side of the link was duplex in appearance one half of the surface being discolored, indicative of a preexisting crack of the fatigue type, whilst the remaining portion was brightly crystalline, resulting from brittle fracture at the time of the mishap. In the second example, the fracture took place at a similar location adjacent to one of the butt welds situated at the mid-length of the sides. Brinell hardness values confirmed that the link was made from the higher tensile grade of material. The cracks were due to fatigue, there being no indications that the weld was initially defective.

The 14-cm diam main hoist shaft of a mobile shovel was found to have multiple crack indications when ultrasonically inspected in the field. A crack around the entire circumference at the change in section was revealed by magnetic-particle inspection of the shaft. The crack was found to coincide with the junction of the fillet and the smaller diam at this change in section. A slight step in the continuity of the fillet and some machining marks were noted at this junction. A fine crack extending 2.5 mm from the surface and originating at the machining marks was revealed by microscopic examination. The shaft was identified by chemical analysis to be 1040 steel (hardness 170 HRB) which was concluded to have insufficient fatigue strength. The step at the base of the fillet was revealed as the point of initiation of the fatigue crack. Shaft material was changed to 4140 steel oil-quenched and tempered to a hardness of 302 to 352 HRB and all machining discontinuities were removed.

A 9310 steel gear was found to be defective after a period of engine service. A linear crack approximately was discovered by routine magnetic-particle inspection of an electron beam welded joint that attached a hollow stub shaft to the web of the gear. The welding procedure had a cosmetic weld pass on top of the initial full-penetration weld. There were no other known service failures of gears were welded by this method. One zone of the welded joint showed incomplete fusion, surrounded by two zones containing fatigue beach marks This indicated that the incomplete-fusion zone was the site at which primary fracture originated. The possible causes of incomplete-fusion include localized magnetic deflection of the electron beam, a momentary arc-out of the electron beam, and eccentricity in the small weld diam. The failure was attributed to fatigue originating at the local unfused interface of the electron beam weld, which had been the result of a deviation in the welding procedure. Examination of the possible causes of failure gave no evidence that a recurrence of the defect had ever occurred. Thus, there was no basis on which to recommend a change in design, material, or welding procedure.

An explosion occurred in a portion of a horizontal, U-shaped expansion loop in a steam main approximately 10-in. diam which had been operating at 400 psi for six years. Steam conditions varied from 538 deg C (450 deg F) saturated to 343 deg C (650 deg F) superheated. Fracture occurred longitudinally through the upper wall over a length of approximately 68 in. The sample received for examination was ultrasonically tested, which indicated a band of internal defects extending 1 in. in from the edge. Subsequently, the portion of the pipe embodying the other side of the rupture was obtained for examination. Transverse sections through this and the mating portion already received, followed by magnetic crack detection, revealed the presence of defective zones. Subsequent ultrasonic examination of other sections of the steam main indicated suspect areas in a number of lengths of pipe. These defects were basically laminations of a similar form to those which resulted in the failure of the portion of pipe.

A 4340 steel piston engine crankshaft in a transport aircraft failed catastrophically during flight. The fracture occurred in the pin radius zone. Fractographic studies established the mode of failure as fatigue under a complex combination of bending and torsional stresses. SEM examination revealed that the fracture origin was a subsurface defect-a hard refractory (Al2O3) inclusion—in the zone close to the pin radius. Chemical analysis showed the crankshaft material to be of inferior quality. It was recommended that magnetic particle inspection using the dc method be used to cheek for cracks during periodic maintenance overhauls.

A connecting rod from a motor boat was broken in two places at the small end. At position I there was a fatigue fracture brought about by operational stress, whereas the fibrous fracture surface II was a secondary tensile fracture. Furthermore the transition on the other side of the rod was cracked symmetrically to the fatigue fracture (position III). Magnetic inspection showed indications of cracking at the transition between the rod and small end in six other connecting rods from the same batch. Metallographic investigation showed the connecting rods were rendered susceptible to fatigue by the notch effect of coarse scale-filled folds formed during forging.

The repeated occurrence of random cracks in the fillet radius portion of low-alloy steel (38KhA) end frame forgings following heat treatment was investigated. Microstructural analyses were carried out on both the failed part and disks of the rolled bar from which the part was made. Subsurface cracks were found to be zigzag and discontinuous as well as intergranular in nature. A mixed mode of fracture involving ductile and brittle flat facets was observed. Micropores and rod-shaped manganese sulfide inclusions were also noted. The material had a hydrogen content of 22 ppm, and cracking was attributed to hydrogen embrittlement. Measurement of hydrogen content in the raw material prior to fabrication was recommended. Careful control of acid pickling procedures for descaling of the hot-rolled bars was also deemed necessary.

Radial cracking occurred adjacent to 11 vanes in a 19-vane impeller operating in a chemical plant environment. The impeller vanes were fillet welded to both the disk and the cover Cracks were next to the fillet welds and near the cover outer diameter They generally did not extend to the outer diameter. The entire impeller surface was tested by the dry magnetic particle method. Visual and microstructural examinations revealed intergranular cracking. Energy-dispersive spectroscopy of corrosion products contained in the cracks disclosed the presence of chlorine and sulfur The failure was attributed to stress-corrosion cracking caused by a corrosive atmosphere.

Within about one month, several knuckle pins (AMS 6470 steel failed, and required to have a minimum case hardness of 92 h15N, a case depth of 0.4 to 0.5 mm (0.017 to 0.022 in.), and a core hardness of 285 to 341 HRB) used in engines failed over a range of 218 to 463 h in operation. Visual examination revealed beach marks typical of fatigue cracks that had nucleated at the base of the longitudinal oil hole. Micrographs of sections revealed a remelt zone and an area of untempered martensite within the region of the cracks. However, review of inspection procedures disclosed the pins had been magnetic-particle inspected by inserting a probe into the longitudinal hole. Evidence found supports the conclusions that the knuckle pins failed by fatigue fracture. The circular cracks at the longitudinal holes were the result of improper technique in magnetic-particle inspection. Thermal transformation of the metal also causes a stress concentration that may lead to fatigue failure. Recommendations included insulating the conductor to prevent arc burning at the base of the longitudinal oil hole. Also, a borescope or metal monitor could be used to inspect the hole for evidence of arc burning from magnetic-particle inspection.

An automobile manufacturer rejected several 1035 steel stub axles because of what appeared to be short longitudinal cracks in the surfaces of the pins. The cracks were found when six axles were examined for defects by magnetic-particle inspection. However, metallographic examination showed that these lines were not cracks but slag inclusions at and immediately below the surface. Analysis (visual inspection, metallographic examination, and 100x/500x magnetic-particle inspection) supported the conclusions that the inclusions consisted of pieces of fireclay from channel brick that were flushed into the ingot mold. Although no true cracks were present, rejection of the stub axles was nevertheless justified. Slag streaks could reduce the strength of the stub axles and lead to the formation of fatigue fractures during operation. No recommendations were made.

An investigation was conducted to determine the factors responsible for the occasional formation of cracks on the parting lines of medium plain carbon and low-alloy medium-carbon steel forgings. The cracks were present on as-forged parts and grew during heat treatment. Examination revealed that areas near the parting line exhibited a large grain structure not present in the forged stock. High-temperature scale was also found in the cracks. It was concluded that the cracks were caused by material being folded over the parting line. The folding occurred because of a mismatch in the forgings and from material flow during trimming and/or material flow during forging.

A number of machined end frame steel forgings made of Cr-Si-Mn alloy showed tiny cracks during magnetic particle inspection after heat treatment. The cracks were mostly confined to base edges and fillet radius. No significant abnormality was observed in chemical composition and microstructure. SEM, optical microscopy, and gas analysis revealed that the subsurface discontinuous cracks at the bore edges and in the fillet radius of the heat-treated end frame component had occurred due to hydrogen embrittlement, and not because of faulty heat treatment. This conclusion was supported by the presence of cracklike indications in machined bore surface of the annealed part.

Nondestructive testing (NDT), also known as nondestructive evaluation (NDE), includes various techniques to characterize materials without damage. This article focuses on the typical NDE techniques that may be considered when conducting a failure investigation. The article begins with discussion about the concept of the probability of detection (POD), on which the statistical reliability of crack detection is based. The coverage includes the various methods of surface inspection, including visual-examination tools, scanning technology in dimensional metrology, and the common methods of detecting surface discontinuities by magnetic-particle inspection, liquid penetrant inspection, and eddy-current testing. The major NDE methods for internal (volumetric) inspection in failure analysis also are described.