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Book Chapter
Hydrogen-Assisted Fracture of a 17-4PH Airplane Wing Component
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001026
EISBN: 978-1-62708-214-3
.... As-cast grain size can be construed from fracture surface contrast. (b) Diagram of significant features; arrows show fracture directions. Areas 1, 2, and 3 represent cleavage “flakes”. Cross-hatched area around flake 1 is overload fracture in same original cast grain as underlying flake. Stippled areas...
Abstract
Cracks were discovered in the cast 17-4 PH stainless steel outboard leading edge flap support of an aircraft wing during overhaul inspection. Failure analysis focused on an apparently intergranular area of fracture surface. It was determined that the original mode of crack growth was cleavage, probably caused by cast-in hydrogen. The intergranular appearance resulted from heat treatment of the already cracked part, which caused the formation of grain-boundary “growth figures” on the exposed crack surfaces. It was recommended that the castings be more closely inspected for defects before further processing and that foundry practices be reviewed to correct deficiencies leading to excessive hydrogen absorption during melting and casting.
Book Chapter
Fatigue Fracture Appearances
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003539
EISBN: 978-1-62708-180-1
... of the specimen, and uses minimal and relatively simple equipment. It does not destroy the specimen or alter fracture surfaces. Macroscopic examination is particularly useful in correlating fracture surface characteristics with part size and shape and with loading conditions. Fatigue origins are frequently...
Abstract
This article commences with a summary of fatigue processes and mechanisms. It focuses on fractography of fatigue. Characteristic fatigue fracture features that can be discerned visually or under low magnification are described. Typical microscopic features observed on structural metals are presented subsequently, followed by a brief discussion of fatigue in nonmetals. The article reviews the various macroscopic and microscopic features to characterize the history and growth rate of fatigue in metals. It concludes with a description of fatigue of polymers and composites.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003543
EISBN: 978-1-62708-180-1
... ductility can still experience crack initiation and growth since some slight plasticity may by present. Relatively brittle metals such as hardened steel and gray cast iron do not always form microscopically identifiable striations and macroscopic beach marks in cyclic failures. Transgranular Cleavage...
Abstract
Overload failures refer to the ductile or brittle fracture of a material when stresses exceed the load-bearing capacity of a material. This article reviews some mechanistic aspects of ductile and brittle crack propagation, including a discussion on mixed-mode cracking, which may also occur when an overload failure is caused by a combination of ductile and brittle cracking mechanisms. It describes the general aspects of fracture modes and mechanisms. The article discusses some of the material, mechanical, and environmental factors that may be involved in determining the root cause of an overload failure. It also presents examples of thermally and environmentally induced embrittlement effects that can alter the overload fracture behavior of metals.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006776
EISBN: 978-1-62708-295-2
... is accessible), requires little or no preparation of the specimen, and uses minimal and relatively simple equipment. It does not destroy the specimen or alter fracture surfaces. Macroscopic examination is particularly useful in correlating fracture surface characteristics with part size and shape...
Abstract
Fatigue failure of engineering components and structures results from progressive fracture caused by cyclic or fluctuating loads. Fatigue is an important potential cause of mechanical failure, because most engineering components or structures are or can be subjected to cyclic loads during their lifetime. This article focuses on fractography of fatigue. It provides an abbreviated summary of fatigue processes and mechanisms: fatigue crack initiation, fatigue crack propagation, and final fracture,. Characteristic fatigue fracture features that can be discerned visually or under low magnification are then described. Typical microscopic features observed on structural metals are presented subsequently, followed by a brief discussion on fatigue in polymers and polymer-matrix composites.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006778
EISBN: 978-1-62708-295-2
... polymers but not on a macroscopic scale in a metallic material. With regard to fatigue, materials with poor ductility can still experience crack initiation and growth, because some slight plasticity may by present. Relatively brittle metals such as hardened steel and gray cast iron do not always form...
Abstract
This article aims to identify and illustrate the types of overload failures, which are categorized as failures due to insufficient material strength and underdesign, failures due to stress concentration and material defects, and failures due to material alteration. It describes the general aspects of fracture modes and mechanisms. The article briefly reviews some mechanistic aspects of ductile and brittle crack propagation, including discussion on mixed-mode cracking. Factors associated with overload failures are discussed, and, where appropriate, preventive steps for reducing the likelihood of overload fractures are included. The article focuses primarily on the contribution of embrittlement to overload failure. The embrittling phenomena are described and differentiated by their causes, effects, and remedial methods, so that failure characteristics can be directly compared during practical failure investigation. The article describes the effects of mechanical loading on a part in service and provides information on laboratory fracture examination.
Book Chapter
Failure of a Mold for Centrifugal Casting of Gray- and Ductile-Iron Pipe
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c0089617
EISBN: 978-1-62708-232-7
... given in inches The spalls were found after 277 pipes had been cast. The average performance for molds of this size was about 2100 castings. Normal pouring temperatures were 1290 °C (2350 °F) for gray iron and 1370 °C (2500 °F) for ductile iron. Investigation Visual inspection of the bore...
Abstract
A forged 4130 steel cylindrical permanent mold, used for centrifugal casting of gray- and ductile-iron pipe, was examined after pulling of the pipe became increasingly difficult. In operation, the mold rotated at a predetermined speed in a centrifugal casting machine while the molten metal, flowing through a trough, was poured into the mold beginning at the bell end and ending with the spigot end being poured last. After the pipe had cooled, it was pulled out from the bell end of the mold, and the procedure was repeated. Investigation supported the conclusion that failure of the mold surface was the result of localized overheating caused by splashing of molten metal on the bore surface near the spigot end. In addition, the mold-wash compound (a bentonite mixture) near the spigot end was too thin to provide the proper degree of insulation and to prevent molten metal from sticking to the bore surface. Recommendations included reducing the pouring temperatures of the molten metal and spraying a thicker insulating coating onto the mold surface.
Book Chapter
Fracture Appearance and Mechanisms of Deformation and Fracture
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006774
EISBN: 978-1-62708-295-2
... ( Fig. 7 ), if present, are macroscopic surface features that indicate the region of crack initiation and propagation direction. They are common and dominant macroscopic features of the fracture of wrought metallic materials but are often absent or poorly defined in castings. The “v” of a chevron points...
Abstract
Engineering component and structure failures manifest through many mechanisms but are most often associated with fracture in one or more forms. This article introduces the subject of fractography and aspects of how it is used in failure analysis. The basic types of fracture processes (ductile, brittle, fatigue, and creep) are described briefly, principally in terms of fracture appearances. A description of the surface, structure, and behavior of each fracture process is also included. The article provides a framework from which a prospective analyst can begin to study the fracture of a component of interest in a failure investigation. Details on the mechanisms of deformation, brittle transgranular fracture, intergranular fracture, fatigue fracture, and environmentally affected fracture are also provided.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003522
EISBN: 978-1-62708-180-1
... Abstract This article focuses on the visual or macroscopic examination of damaged materials and interpretation of damage and fracture features. Analytical tools available for evaluations of corrosion and wear damage features include energy dispersive spectroscopy, electron probe microanalysis...
Abstract
This article focuses on the visual or macroscopic examination of damaged materials and interpretation of damage and fracture features. Analytical tools available for evaluations of corrosion and wear damage features include energy dispersive spectroscopy, electron probe microanalysis, Auger electron spectroscopy, secondary ion mass spectroscopy, and X-ray powder diffraction. The article discusses the analysis and interpretation of base material composition and microstructures. Preparation and examination of metallographic specimens in failure analysis are also discussed. The article concludes with a review of the evaluation of polymers and ceramic materials in failure analysis.
Book Chapter
Examination of Damage and Material Evaluation
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006757
EISBN: 978-1-62708-295-2
... candy” fracture. Fig. 9 Low-power light microscope view of a “rock candy” fracture in a tensile specimen taken from a cast steel that had aluminum nitrides segregated to the grain boundaries Macroscopic examination is commonly made using a low-power binocular stereomicroscope, which gives...
Abstract
Examination of a damaged component involves a chain of activities that, first and foremost, requires good observation and documentation. Following receipt and documentation, the features of damage can be recorded and their cause(s) investigated, as this article briefly describes, for typical types of damage experienced for metallic components. This article discusses the processes involved in visual or macroscopic examination of damaged material; the interpretation of fracture features, corrosion, and wear damage features; and the analysis of base material composition. It covers the processes involved in the selection of metallurgical samples, the preparation and examination of metallographic specimens in failure analysis, and the analysis and interpretation of microstructures. Examination and evaluation of polymers and ceramic materials in failure analysis are also briefly discussed.
Book Chapter
Fracture Appearance and Mechanisms of Deformation and Fracture
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003537
EISBN: 978-1-62708-180-1
... ( Fig. 6 ), if present, are macroscopic surface features that indicate the region of crack initiation and propagation direction. They are common and dominant macroscopic features of the fracture of wrought metallic materials but are often absent or poorly defined in castings. The “v” of a chevron points...
Abstract
This article provides an overview of fractography and explains how it is used in failure analysis. It reviews the basic types of fracture processes, namely, ductile, brittle, fatigue, and creep, principally in terms of fracture appearances, such as microstructure. The article also describes the general features of fatigue fractures in terms of crack initiation and fatigue crack propagation.
Book Chapter
Failures Related to Castings
Available to PurchaseSeries: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006831
EISBN: 978-1-62708-329-4
... by special methods, machining, or fracture of the casting B 111 (a) Internal, rounded cavities, usually smooth-walled, of varied size, isolated or grouped irregularly in all areas of the casting Blowholes, pinholes B 112 (a) As above, but limited to the vicinity of metallic pieces placed...
Abstract
The information provided in this article is intended for those individuals who want to determine why a casting component failed to perform its intended purpose. It is also intended to provide insights for potential casting applications so that the likelihood of failure to perform the intended function is decreased. The article addresses factors that may cause failures in castings for each metal type, starting with gray iron and progressing to ductile iron, steel, aluminum, and copper-base alloys. It describes the general root causes of failure attributed to the casting material, production method, and/or design. The article also addresses conditions related to the casting process but not specific to any metal group, including misruns, pour shorts, broken cores, and foundry expertise. The discussion in each casting metal group includes factors concerning defects that can occur specific to the metal group and progress from melting to solidification, casting processing, and finally how the removal of the mold material can affect performance.
Book Chapter
Practices in Failure Analysis
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003524
EISBN: 978-1-62708-180-1
... cracks. Sharp-bottomed tool marks can initiate fatigue fractures even though the general contour of the area has a generous radius. The shape, size, and cross section of a specimen or structural component can have a large effect on both the macroscopic and the microscopic appearance of the fracture...
Abstract
This article describes the preliminary stages and general procedures, techniques, and precautions employed in the investigation and analysis of metallurgical failures that occur in service. The most common causes of failure characteristics are described for fracture, corrosion, and wear failures. The article provides information on the synthesis and interpretation of results from the investigation. Finally, it presents key guidelines for conducting a failure analysis.
Book Chapter
Abrasive Wear Failures
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006790
EISBN: 978-1-62708-295-2
... chunks of rock. It is accompanied by heavy impact and by high bending and compressive forces on the wearing parts, which are made as heavy-section castings. As a result, the choice of ferrous alloys that can be used with confidence in these applications is limited. Traditionally, austenitic 12% Mn steels...
Abstract
Engineered components fail predominantly in four major ways: fracture, corrosion, wear, and undesirable deformation (i.e., distortion). Typical fracture mechanisms feature rapid crack growth by ductile or brittle cracking; more progressive (subcritical) forms involve crack growth by fatigue, creep, or environmentally-assisted cracking. Corrosion and wear are another form of progressive material alteration or removal that can lead to failure or obsolescence. This article primarily covers the topic of abrasive wear failures, covering the general classification of wear. It also discusses methods that may apply to any form of wear mechanism, because it is important to identify all mechanisms or combinations of wear mechanisms during failure analysis. The article concludes by presenting several examples of abrasive wear.
Book Chapter
Abrasive Wear Failures
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003560
EISBN: 978-1-62708-180-1
... and handling of large chunks of rock. It is accompanied by heavy impact and by high bending and compressive forces on the wearing parts, which are made as heavy section castings. As a result, the choice of ferrous alloys that can be used with confidence in these applications is limited. Traditionally...
Abstract
Wear, a form of surface deterioration, is a factor in a majority of component failures. This article is primarily concerned with abrasive wear mechanisms such as plastic deformation, cutting, and fragmentation which, at their core, stem from a difference in hardness between contacting surfaces. Adhesive wear, the type of wear that occurs between two mutually soluble materials, is also discussed, as is erosive wear, liquid impingement, and cavitation wear. The article also presents a procedure for failure analysis and provides a number of detailed examples, including jaw-type rock crusher wear, electronic circuit board drill wear, grinding plate wear failure analysis, impact wear of disk cutters, and identification of abrasive wear modes in martensitic steels.
Book Chapter
Failures Related to Casting
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003508
EISBN: 978-1-62708-180-1
... to the naked eye (blowholes, pinholes) B 110: Class B 100 cavities internal to the casting, not extending to the surface, discernible only by special methods, machining, or fracture of the casting B 111 (a) Internal, rounded cavities, usually smooth-walled, of varied size, isolated or grouped...
Abstract
This article focuses on the general root causes of failure attributed to the casting process, casting material, and design with examples. The casting processes discussed include gravity die casting, pressure die casting, semisolid casting, squeeze casting, and centrifugal casting. Cast iron, gray cast iron, malleable irons, ductile iron, low-alloy steel castings, austenitic steels, corrosion-resistant castings, and cast aluminum alloys are the materials discussed. The article describes the general types of discontinuities or imperfections for traditional casting with sand molds. It presents the international classification of common casting defects in a tabular form.
Book Chapter
Stress Corrosion Cracking Failures in Components Made of Austenitic Chromium Nickel Steels
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001163
EISBN: 978-1-62708-234-1
... of the pitted areas. Alternatively polishing and etching micro-sections for viewing at high magnification made crack detail more visible. Optical and scanning electron micrographs showed cracking in austenitic cast steel and cast iron due to both internal tensile and critical residual stresses; the latter...
Abstract
Practical examples of stress-corrosion cracking (SCC) and methods for its prevention were presented. Cracks in chloride-sensitive austenitic steels were very branched and transcrystalline. Etched cross sections of molybdenum-free samples showed chloride-induced cracks running out of the pitted areas. Alternatively polishing and etching micro-sections for viewing at high magnification made crack detail more visible. Optical and scanning electron micrographs showed cracking in austenitic cast steel and cast iron due to both internal tensile and critical residual stresses; the latter causes flake-like spalling. Measures to prevent SCC include stress reduction, use of austenitic steels or nickel alloys not susceptible to grain boundary attack, use of ferritic chromium steels, surface slag removal, control of temperature and chloride concentration, and cathodic protection.
Book Chapter
Prevention of Machining-Related Failures
Available to PurchaseSeries: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006826
EISBN: 978-1-62708-329-4
... (macroscopic and microscopic) Residual-tension stress distribution in surface layer Processing inclusions introduced Plastically deformed debris as a result of grinding Voids, pits, burrs, or foreign material inclusions in surface Physical Transformation of phases Grain size and distribution...
Abstract
The first part of this article focuses on two major forms of machining-related failures, namely machining workpiece (in-process) failures and machined part (in-service) failures. Discussion centers on machining conditions and metallurgical factors contributing to (in-process) workpiece failures, and undesired surface layers and metallurgical factors contributing to (in-service) machined part failures. The second part of the article discusses the effects of microstructure on machining failures and their preventive measures.
Book Chapter
Study on Failure Analyses and Material Characterizations of a Damaged Booster Pump
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001779
EISBN: 978-1-62708-241-9
... intensify the damages of surface [ 7 ]. In addition, some casting defects found in depth of casting by macroscopic examination which could trigger other defects and accelerate the damage mechanisms ( Fig. 3 ) [ 10 ]. These fabrication defects not only might be active zones for farther defects...
Abstract
Material samples collected from failed booster pumps were analyzed to determine the cause of failure and assess the adequacy of the materials used in the design. The pumps had been in service at a power plant, transporting feedwater from a deaerator to a main turbine boiler. Samples from critical areas of the pump were examined using optical and scanning electron microscopy, electrochemical analysis, and tensile testing. Based on microstructure and morphology, estimated corrosion rates, and particle concentrations in the feedwater, it was concluded that cavitation and erosion were the dominant failure mechanisms and that the materials and processes used to make the pumps were largely unsuited for the application.
Book Chapter
Stress-Rupture Characterization in Nickel-Based Superalloy Gas Turbine Engine Components
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001758
EISBN: 978-1-62708-241-9
... in an alloy is to increase the average grain size, which decreases the overall grain boundary area. Optical and SEM backscatter photographs documenting creep induced voiding along transverse grain boundaries within an equiaxed airfoil casting are shown in Fig. 13 . Over time, the internal voiding increases...
Abstract
This article describes the visual, fractographic, and metallographic evidence typically encountered when analyzing stress rupture of turbine airfoils. Stress-rupture fractures are generally heavily oxidized, tend to be rough in texture, and are primarily intergranular and/or interdendritic in appearance compared to smoother, transgranular fatigue type fractures. Often, gross plastic yielding is visible on a macroscopic scale. Commonly observed microstructural characteristics include creep voiding along grain boundaries and/or interdendritic regions. Internal voids can also nucleate at carbides and other microconstituents, especially in single crystal castings that do not possess grain boundaries.
Book Chapter
Mechanisms and Appearances of Ductile and Brittle Fracture in Metals
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006775
EISBN: 978-1-62708-295-2
...). Source: Ref 30 There is also a particle size distribution in high-strength, age-hardening aluminum alloys, but different behavior in an aluminum casting alloy has been reported ( Ref 31 ). The iron- and/or silicon-rich phases are the inclusions that are smaller than other phases created...
Abstract
This article focuses on characterizing the fracture-surface appearance at the microscale and contains some discussion on both crack nucleation and propagation mechanisms that cause the fracture appearance. It begins with a discussion on microscale models and mechanisms for deformation and fracture. Next, the mechanisms of void nucleation and void coalescence are briefly described. Macroscale and microscale appearances of ductile and brittle fracture are then discussed for various specimen geometries (smooth cylindrical and prismatic) and loading conditions (e.g., tension compression, bending, torsion). Finally, the factors influencing the appearance of a fracture surface and various imperfections or stress raisers are described, followed by a root-cause failure analysis case history to illustrate some of these fractography concepts.
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