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intergranular cracking
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Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001086
EISBN: 978-1-62708-214-3
... in a highly sensitized state. The sensitized material lost corrosion resistance, became embrittled along the grain boundaries, and finally failed by intergranular cracking. Use of type 410 martensitic stainless steel was recommended. Embrittlement Heat-affected zone Sensitizing Vanes Welded joints...
Abstract
Two Z-shape impeller vanes failed. The vane material was 14-hard type 301 stainless steel. The vanes were of two-piece construction, with a longitudinal weld. Analyses indicated that the vanes had not been solution annealed after welding, leaving the heat-affected zone above the welds in a highly sensitized state. The sensitized material lost corrosion resistance, became embrittled along the grain boundaries, and finally failed by intergranular cracking. Use of type 410 martensitic stainless steel was recommended.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0048751
EISBN: 978-1-62708-235-8
... Abstract The presence of subsurface cracks in a longitudinal weld seam of an AISI type 316 stainless steel heat-exchanger shell was revealed by radiographic testing. Numerous intergranular cracks associated with the root pass of the weld, which had propagated both parallel and normal...
Abstract
The presence of subsurface cracks in a longitudinal weld seam of an AISI type 316 stainless steel heat-exchanger shell was revealed by radiographic testing. Numerous intergranular cracks associated with the root pass of the weld, which had propagated both parallel and normal to the weld seam, were revealed by metallographic examination (hot shortness). It was indicated by energy-dispersive spectroscopy that type 316 electrode was not used for the root pass and instead a nickel-copper alloy electrode was employed. It was thus concluded that cracking was caused due to the use of an incorrect electrode for the root pass as these electrodes are crack sensitive if overheated. The weld seam was completely ground out and replaced with the correct electrode material as a corrective measure.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047632
EISBN: 978-1-62708-235-8
..., and inspection. The crack indications were found only on one side of the boss and on the lower portion of the hot-spun dome region. The metallographic specimens revealed triangular voids and severe intergranular cracks. The cracks displayed the glossy surfaces typical of melted and resolidified material...
Abstract
An air bottle, machined from a solid block of aluminum alloy 2219-T852, displayed liquid-penetrant crack indications after assembly welding. The air bottle was machined to rough shape, a 3.8 mm (0.15 in.) wall thickness cylindrical cup with a 19 mm (3/4 in.) wall thickness integral boss on one side. After annealing, hot spinning, annealing a second time, and tack welding a port fitting, the assembly was torch preheated to 120 to 150 deg C (250 to 300 deg F). The port fitting was then welded in place. Final full heat treatment to the T62 temper was followed by machining, testing, and inspection. The crack indications were found only on one side of the boss and on the lower portion of the hot-spun dome region. The metallographic specimens revealed triangular voids and severe intergranular cracks. The cracks displayed the glossy surfaces typical of melted and resolidified material. The localized cracks in the air bottle were from grain-boundary eutectic melting caused by local torch overheating used in preparation for assembly welding of a port fitting. A change in design was scheduled to semiautomatic welding without the use of preheating for the joining of the port fitting for the dome opening.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c0048791
EISBN: 978-1-62708-234-1
... were located in wide bands running circumferentially below the cross-to-cap weld and above the cap-to-discharge-pipe weld. The material was found to conform to the requirements both in terms of hardness and strength. Intergranular cracks filled with oxide were observed on metallographic analysis...
Abstract
Linear indications on the outer surface of a cross in a piping system were revealed by dye-penetrant examination. The cross was specified to be SA403 type WP 304 stainless steel. The cross had been subjected to induction-heating stress improvement. The linear indications on the cross were located in wide bands running circumferentially below the cross-to-cap weld and above the cap-to-discharge-pipe weld. The material was found to conform to the requirements both in terms of hardness and strength. Intergranular cracks filled with oxide were observed on metallographic analysis of a sectioned and oxalic acid etched sample. The grain size was found to exceed the ASTM standard. No indications of sensitization were observed during testing with practice A of ASTM A 262. Definitive evidence of contaminants to support SCC as the failure mechanism was not disclosed during analysis. It was concluded that overheating or burning of the forging, which classically results in large grain size, intergranular fractures, and fine oxide particles dispersed throughout the grains was the possible reason for the failure.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c0046252
EISBN: 978-1-62708-229-7
... examination of sections etched with Vilella's reagent supports the conclusions that failure of the bellows occurred by intergranular fatigue cracking. Secondary degrading effects on the piping existed as well. Recommendations included the acceptability of Type 321 stainless steel (provided open-cycle testing...
Abstract
A type 321 stainless steel bellows expansion joint on a 17-cm (6 in.) OD inlet line (347 stainless) in a gas-turbine test facility cracked during operation. The line carried high-purity nitrogen gas at 1034 kPa (150 psi) with a flow rate of 5.4 to 8.2 kg/s (12 to 18 lb/s). Cracking occurred in welded joints and in unwelded portions of the bellows. The bellows were made by forming the convolution halves from stainless steel sheet, then welding the convolutions together. Evidence from visual examination, liquid penetrant inspection chemical analysis, hardness tests, and metallographic examination of sections etched with Vilella's reagent supports the conclusions that failure of the bellows occurred by intergranular fatigue cracking. Secondary degrading effects on the piping existed as well. Recommendations included the acceptability of Type 321 stainless steel (provided open-cycle testing does not result in surface oxidation and crevices) Although type 347 stainless steel would be better, and Inconel 600 would be an even better choice. Welds would also need modified processing for reheating and annealing. Prevention of oil leakage into the system would minimize carburization of the piping and bellows.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001060
EISBN: 978-1-62708-214-3
... was caused by intergranular corrosion/stress-corrosion cracks that initiated from the external surface of the pipe reducer section. Contributory factors were the sensitized condition of the flange and the concentration of corrosive elements from the bleach stock plant environment on the external surface...
Abstract
A type 316 stainless steel pipe reducer section failed in service of bleached pulp stock transfer within 2 years in a pulp and paper mill. The reducer section fractured in the heat-affected zone of the flange-to-pipe weld on the flange side. The pipe reducer section consisted of 250 and 200 mm (10 and 8 in.) diam flanges welded to a tapered pipe section. The tapered pipe section was 3.3 mm (0.13 in.) thick type 316 stainless steel sheet, and the flanges were 5 mm (0.2 in.) thick CF8M (type 316) stainless steel castings. Visual and metallographic analysis indicated that the fracture was caused by intergranular corrosion/stress-corrosion cracks that initiated from the external surface of the pipe reducer section. Contributory factors were the sensitized condition of the flange and the concentration of corrosive elements from the bleach stock plant environment on the external surface. In the absence of the sensitized condition of the flange, the service of the pipe reducer section was acceptable. A type 316L stainless steel reducer section was recommended to replace the 316 component because of its superior resistance to sensitization.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001317
EISBN: 978-1-62708-215-0
... Abstract Two AISI type 316 stainless steel dished ends failed through the formation of intergranular stress-corrosion cracks (IGSCC) within a few months of service. The dished ends failed in the straight portions near the circumferential welds that joined the ends to the cylindrical portions...
Abstract
Two AISI type 316 stainless steel dished ends failed through the formation of intergranular stress-corrosion cracks (IGSCC) within a few months of service. The dished ends failed in the straight portions near the circumferential welds that joined the ends to the cylindrical portions of the vessel. Both dished ends were manufactured from the same batch and were supplied by the same manufacturer One of the dished ends had been exposed to sodium at 550 deg C (1020 deg F) for 500 h before failure due to sodium leakage was detected. The other dished end was used to fabricate a second vessel that was kept in storage for 1 year Clear evidence of sensitization was found in areas where IGSCC occurred. Sensitization was extensive in the dished end that had been exposed to sodium at high temperature, and it occurred in a narrow band similar to that typical of weld decay in the dished end that had been kept in storage. Solution annealing was recommended to relieve residual stress, thereby reducing the probability of failure. It was also recommended that the carbon content of the steel be lowered, i.e., that a 316L grade be used.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001561
EISBN: 978-1-62708-229-7
... Abstract An intergranular stress-corrosion cracking failure of 304 stainless steel pipe in 2000 ppm B as H3BO3 + H2O at 100 deg C was investigated. Constant extension rate testing produced an intergranular type failure in material in air. Chemical analysis was performed on both the base metal...
Abstract
An intergranular stress-corrosion cracking failure of 304 stainless steel pipe in 2000 ppm B as H3BO3 + H2O at 100 deg C was investigated. Constant extension rate testing produced an intergranular type failure in material in air. Chemical analysis was performed on both the base metal and weld material, in addition to fractography, EPR testing and optical microscopy in discerning the mode of failure. Various effects of Cl-, O2 and MnS are discussed. Results indicated that the cause of failure was the severe sensitization coupled with probable contamination by S and possibly by Cl ions.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001061
EISBN: 978-1-62708-214-3
... and heat-affected zones (HAZs). Fracture/crack morphology was brittle and primarily intergranular and deposits at crack tips were primarily iron oxides with significant amounts of sodium compounds. On these bases, the cracking was characterized as intergranular stress-corrosion cracking (IGSCC). Corrosion...
Abstract
Schedule 80 low-carbon steel pipes used to transfer kraft liquor in a Kamyr continuous pulp digester failed within 18 months after installation. Visual and metallographic examinations established that the cracking initiated on the internal surfaces of the equalizer pipes in the welds and heat-affected zones (HAZs). Fracture/crack morphology was brittle and primarily intergranular and deposits at crack tips were primarily iron oxides with significant amounts of sodium compounds. On these bases, the cracking was characterized as intergranular stress-corrosion cracking (IGSCC). Corrosion-related deterioration was not found, indicating that the material was generally suitable for the intended service. High residual tensile stresses in the welds and HAZS, resulting from field welding under highly constrained conditions using inadequate weld procedures, were the most probable cause of the failures. Minimizing residual stresses through use of welding procedures that include appropriate preweld and interpass temperatures and postweld stress relief heat treatment at 650 deg C (1200 deg F) was recommended to prevent further failures.
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in Failure Analysis of Railroad Components
> Analysis and Prevention of Component and Equipment Failures
Published: 30 August 2021
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Published: 01 January 2002
Fig. 4 Typical creep deformation and intergranular cracking in a jet-engine turbine blade. Courtesy of J. Schijve
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in Stress-Corrosion Cracking of a High-Strength Steel Frame in a Fighter Aircraft
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1992
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in Stress-Corrosion Cracking of a Teflon-Lined Steel Pipe in Sulfuric Acid Service
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1992
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in Condition Assessment and Improvement of a Steam Turbine Rotor
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1992
Fig. 5 Typical “rock candy” fracture appearance with intergranular cracking exhibited by temper-embrittled materials. 136×.
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in Stress-Corrosion Cracking Caused by Residual Stresses in Chromium Silicon Alloy Steel Helical Compression Springs
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1992
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in Metallurgical Failure Analysis of Various Implant Materials Used in Orthopedic Applications
> Handbook of Case Histories in Failure Analysis
Published: 01 December 2019
Fig. 10 Intergranular cracking by selective attack on the external surface of the plate near the fracture origin
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Published: 15 January 2021
Fig. 5 Typical creep deformation and intergranular cracking in a jet-engine turbine blade. Courtesy of J. Schijve
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in Intergranular Cracking in an Air Bottle Because of Torch Overheating Before Welding
> ASM Failure Analysis Case Histories: Processing Errors and Defects
Published: 01 June 2019
Fig. 1 Aluminum alloy air bottle that failed by intergranular cracking caused by overheating before assembly welding. (a) Machined air bottle showing hot-spun region, circumferential butt weld, and location of crack indications. Dimensions given in inches. (b) Longitudinal intergranular crack
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in Liquid Metal Embrittlement of Bronze Rupture Discs
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1993
Fig. 8 SEM micrograph showing secondary intergranular cracking on the cylinder side of the failed disc. Arrow indicates primary fracture surface. 239×
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in Mercury Liquid Embrittlement Failure of 5083-O Aluminum Alloy Piping
> Handbook of Case Histories in Failure Analysis
Published: 01 December 1993
Fig. 7 SEM micrograph showing intergranular cracking near the inside surface of the pipe weld. 67×
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