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inductively coupled plasma spectroscopy

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Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001843
EISBN: 978-1-62708-241-9
... of degradation that occurs at low temperatures. Based on the results of the investigation, which included SEM/EDS analysis, inductively coupled plasma spectroscopy, and x-ray diffraction, the metal surfaces contained less than 0.1% Bi and thus were not adequately protected against tin pest, which was confirmed...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001845
EISBN: 978-1-62708-241-9
... an investigation that included fractographic and microstructural analysis, hardness testing, inductively coupled plasma spectroscopy, and finite-element analysis. The fracture was shown to be brittle in nature and covered with oxide flakes, but no other flaws relevant to the failure were observed...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001809
EISBN: 978-1-62708-241-9
... erosion damage inductively coupled plasma spectroscopy corrosion resistance ASTM B148 (nickel-aluminum bronze) UNS C95800 Background An impeller from a brackish water pump was removed from service after 4 years of use. The pump was a replacement for the original pump that lasted over 40 years...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001335
EISBN: 978-1-62708-215-0
..., but not always, present with the tellurium. The tellurium quickly disappeared during depth profiling; thus, the inclusions were probably quite thin. Subsequent multiple trace chemical analyses by inductively coupled plasma spectroscopy that was specifically targeted for tellurium did detect a concentration level...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006766
EISBN: 978-1-62708-295-2
... covers the operating principles, applications, advantages, and disadvantages of optical emission spectroscopy (OES), inductively coupled plasma optical emission spectroscopy (ICP-OES), X-ray spectroscopy, and ion chromatography (IC). In addition, information on combustion analysis and inert gas fusion...
Image
Published: 15 January 2021
Fig. 2 Schematic diagram of inductively coupled plasma optical emission spectroscopy system. RF, radio frequency. Source: Ref 3 More
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.usage.c9001508
EISBN: 978-1-62708-236-5
... Part Since the cracking was found in supposedly brand new shields which should not have been exposed to a chloride rich environment for a significant amount of time, the material, processing, and packaging all became suspect. The bulk material composition was analyzed by inductively coupled...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001832
EISBN: 978-1-62708-241-9
... particulate air filters. The failure analysis investigation concluded that nitrate-induced stress-corrosion cracking was the cause of the failure. vent pipe nitrate-induced stress-corrosion cracking welding defects galvanized low-carbon steel MnS inclusions ion-coupled plasma-emission spectroscopy...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006759
EISBN: 978-1-62708-295-2
... maintenance, including assurance that adequate calibrations have been upheld. Methods such as x-ray fluorescence (XRF), arc or spark optical emission spectroscopy (OES), and inductively coupled plasma OES (ICP-OES) can be considered quantitative methods. To obtain optimal quantitative results, the sample...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001826
EISBN: 978-1-62708-241-9
... testing, energy dispersive x-ray analysis, and inductively coupled plasma mass spectrometry. The tube was made from SA 210A1 carbon steel that had been compromised by wall thinning and the accumulation of fire and water-side scale deposits. Investigators determined that the tube failed due to prolonged...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001717
EISBN: 978-1-62708-217-4
... the chemical composition of the alloy. The material was required to conform to the governing material specification. The composition was determined by the Leco combustion method (carbon and sulfur), and inductively coupled argon plasma emission spectroscopy. The material met the requirements...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001757
EISBN: 978-1-62708-241-9
..., some specimens were prepared from the fractured blade. Optical microscopy was used to determine the microstructures of a blade, and energy-dispersive X-ray fluorescence, inductively coupled plasma spectrometry (ICP), and energy-dispersive spectroscopy (EDS) in a field emission scanning electron...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003529
EISBN: 978-1-62708-180-1
..., the more of a certain element present, the less light will get through to the detector. Again, proper calibration is extremely important. Another method of wet chemical analysis is the inductively coupled plasma spectrometer. Again, a solution of dissolved metal is fed into the instrument. The solution...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006782
EISBN: 978-1-62708-295-2
... to identify the material and to compare it with the specification requirements on the drawing. Otherwise, the alloy is identified using available standards. For metallic components, destructive analysis is performed using inductively coupled plasma/atomic or optical emission spectroscopy, an analytical...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001850
EISBN: 978-1-62708-241-9
... Analysis Chemical analysis of the sample collected from the bulged out portion of the blow pipe was carried out using inductively coupled plasma (ICP) spectrometer (Germany, model: ARCOS); carbon (C) and (S) content of the sample was determined using combustion infrared technique (LECO, TC600) as per...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001304
EISBN: 978-1-62708-215-0
... coupled plasma spectrometry to identify possible deviation in chemistry from material specifications. Nondestructive Evaluation Liquid Penetrant Inspection Liquid penetrant inspection showed that the diffuser intake flange exhibited a continuous fracture front, traveling along the type 310...
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006917
EISBN: 978-1-62708-395-9
... to reduce the crystallinity has enhanced the ESC resistance ( Ref 14 ), but others show better ESC resistance with higher levels of crystallinity, as achieved through slow cooling during injection molding ( Ref 15 ). It appears likely that the phenomenon is coupled in these studies. The presence...
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006824
EISBN: 978-1-62708-329-4
... abnormally hot). Chemical analysis by an inductively coupled plasma technique revealed that the blades were comprised of Nimonic 115 alloy, a nickel-base superalloy forging. The alloy composition was consistent with the reported nominal composition of the alloy, but the standard alloy for the application...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006769
EISBN: 978-1-62708-295-2
...-dispersive x-ray spectroscopy. Recent developments ( Ref 2 ) also have greatly increased the capability of the SEM to obtain crystallographic information from a sample. Thus, the analytical capabilities of an SEM cover a wide range of information, and accessories can be chosen to suit the particular...
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006939
EISBN: 978-1-62708-395-9
... psi) ( Ref 6 , 25 – 27 ). The different methods for producing CNTs are as follows ( Ref 25 – 27 , 29 ): Surface-mediated growth of vertically aligned tubes by plasma-enhanced vapor deposition Chemical vapor deposition Laser ablation High-pressure carbon monoxide Arc discharge...