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inductively coupled plasma spectroscopy

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Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001843
EISBN: 978-1-62708-241-9
... of degradation that occurs at low temperatures. Based on the results of the investigation, which included SEM/EDS analysis, inductively coupled plasma spectroscopy, and x-ray diffraction, the metal surfaces contained less than 0.1% Bi and thus were not adequately protected against tin pest, which was confirmed...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001845
EISBN: 978-1-62708-241-9
... an investigation that included fractographic and microstructural analysis, hardness testing, inductively coupled plasma spectroscopy, and finite-element analysis. The fracture was shown to be brittle in nature and covered with oxide flakes, but no other flaws relevant to the failure were observed...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006766
EISBN: 978-1-62708-295-2
... Fig. 2 Schematic diagram of inductively coupled plasma optical emission spectroscopy system. RF, radio frequency. Source: Ref 3 Fig. 1 Schematic of spark emission spectroscopy system. Source: Ref 1 Abstract Identification of alloys using quantitative chemical analysis...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001809
EISBN: 978-1-62708-241-9
... erosion damage inductively coupled plasma spectroscopy corrosion resistance ASTM B148 (nickel-aluminum bronze) UNS C95800 References 1. Michels H.T. , Kain R.M. : Effect of composition and microstructure on the seawater corrosion resistance of nickel–aluminum...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001335
EISBN: 978-1-62708-215-0
... multiple trace chemical analyses by inductively coupled plasma spectroscopy that was specifically targeted for tellurium did detect a concentration level of 15 to 25 ppm in the embrittled tube. Tellurium could not be detected in the nonembrittled tube; the detectability limit for tellurium is estimated...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001826
EISBN: 978-1-62708-241-9
... testing, energy dispersive x-ray analysis, and inductively coupled plasma mass spectrometry. The tube was made from SA 210A1 carbon steel that had been compromised by wall thinning and the accumulation of fire and water-side scale deposits. Investigators determined that the tube failed due to prolonged...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.usage.c9001508
EISBN: 978-1-62708-236-5
..., processing, and packaging all became suspect. The bulk material composition was analyzed by inductively coupled plasma atomic emission spectroscopy and was found to meet applicable standards for this alloy. The Rockwell hardness was in the acceptable range for annealed 321 CRES. A section was taken...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001832
EISBN: 978-1-62708-241-9
... the XRD results. Even though the XRD results indicated the presence of iron phosphates, anionic phosphate species was below detectable in the IC analysis. Inductively-coupled plasma-emission spectroscopy (ICP-ES) was used to determine the relative concentrations of metallic ions in the dry deposits...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006759
EISBN: 978-1-62708-295-2
... that adequate calibrations have been upheld. Methods such as x-ray fluorescence (XRF), arc or spark optical emission spectroscopy (OES), and inductively coupled plasma OES (ICP-OES) can be considered quantitative methods. To obtain optimal quantitative results, the sample should be prepared according...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001717
EISBN: 978-1-62708-217-4
... the chemical composition of the alloy. The material was required to conform to the governing material specification. The composition was determined by the Leco combustion method (carbon and sulfur), and inductively coupled argon plasma emission spectroscopy. The material met the requirements...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003529
EISBN: 978-1-62708-180-1
... present, the less light will get through to the detector. Again, proper calibration is extremely important. Another method of wet chemical analysis is the inductively coupled plasma spectrometer. Again, a solution of dissolved metal is fed into the instrument. The solution is dispersed and heated...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001757
EISBN: 978-1-62708-241-9
... coupled plasma spectrometry (ICP), and energy-dispersive spectroscopy (EDS) in a field emission scanning electron microscope (FE-SEM) were used to verify the microchemical composition. The fractured surface of the blade was examined using visual stereoscopy and a FE-SEM, while Vickers microhardness...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006782
EISBN: 978-1-62708-295-2
... it with the specification requirements on the drawing. Otherwise, the alloy is identified using available standards. For metallic components, destructive analysis is performed using inductively coupled plasma/atomic or optical emission spectroscopy, an analytical technique for quantitative elemental analysis...
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001304
EISBN: 978-1-62708-215-0
... were also determined by inductively coupled plasma spectrometry to identify possible deviation in chemistry from material specifications. The failure analysis procedure clearly indicated that the weld joint in the diffuser intake flange (type 310 stainless steel to Corten steel) contained...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001850
EISBN: 978-1-62708-241-9
.... Chemical analysis of the sample collected from the bulged out portion of the blow pipe was carried out using inductively coupled plasma (ICP) spectrometer (Germany, model: ARCOS); carbon (C) and (S) content of the sample was determined using combustion infrared technique (LECO, TC600) as per standard...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006769
EISBN: 978-1-62708-295-2
... deliver clear, high-magnification images while also providing the user with the ability to obtain chemical compositions from samples when equipped for additional techniques, such as energy-dispersive x-ray spectroscopy. Recent developments ( Ref 2 ) also have greatly increased the capability of the SEM...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001583
EISBN: 978-1-62708-217-4
... composition was governed by AMS 5629. The material designated was precipitation hardened PH 13-8 Mo, heat treated to the H1050 condition. Inductively coupled plasma/atomic emission spectroscopy was utilized to determine the wt.% of each element. Samples were sectioned from each of the six rods under...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0001818
EISBN: 978-1-62708-180-1
... and storage must be considered because air and its contaminants may be corrosive. Field fabrication and erection practices should also be considered. Simple matters such as specifying and verifying the proper material and material condition are critical. One company has used portable spectroscopy equipment...