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Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001289
EISBN: 978-1-62708-215-0
.... Subsurface cracks were found to be zigzag and discontinuous as well as intergranular in nature. A mixed mode of fracture involving ductile and brittle flat facets was observed. Micropores and rod-shaped manganese sulfide inclusions were also noted. The material had a hydrogen content of 22 ppm, and cracking...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001839
EISBN: 978-1-62708-241-9
.... Potential sources of hydrogen are considered as are remedial measures for controlling hydrogen content in steels. steel coils delayed hydrogen cracking austenitic stainless steel grain facets stepwise microcracking inert gas fusion analysis stacking fault energy 0.1%C-14.7%Cr-9.3%Mo-0.2%Si (low...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.conag.c0047474
EISBN: 978-1-62708-221-1
... hydrogen content. Two steps were taken to combat this type of failure. First, when service conditions did not require high hardness to combat wear, the links were produced of a steel having a yield strength of about 690 MPa (100 ksi) rather than 1034 M Chains Fatigue Hydrogen embrittlement ASTM...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003507
EISBN: 978-1-62708-180-1
... discusses the types of imperfections that can be traced to the original ingot product. These include chemical segregation; ingot pipe, porosity, and centerline shrinkage; high hydrogen content; nonmetallic inclusions; unmelted electrodes and shelf; and cracks, laminations, seams, pits, blisters, and scabs...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001174
EISBN: 978-1-62708-220-4
...Abstract Abstract A cooler of an ammonia synthesis plant was destroyed after three years of service due to the rupture of a distribution manifold. Synthesis gas under high pressure and at about 300 deg C, consisting of 10% NH3 and unconverted gas of 25% N2 and 75% H2 content, was water-cooled...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.conag.c0047508
EISBN: 978-1-62708-221-1
..., hydrogen embrittlement, or both. At subzero temperatures, the steel was below its ductile-to-brittle transition temperature. These circumstances suggest a brittle condition. Steps to avoid this type of failure: For cold conditions, the steel plate should have a low carbon content and a high manganese...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.petrol.c9001166
EISBN: 978-1-62708-228-0
... of corrosion product from each pipe section were analyzed for carbon, sulfur, and iron and were found to consist mainly of iron sulfide mixed with soot and rust. The damage resulted from a high content of hydrogen sulfide in the gas (6% CO2, 20% CO, 8 to 12% H2, 0.5 to 1.5% CH4, remainder N2). To process...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.petrol.c9001179
EISBN: 978-1-62708-228-0
... with it by shrinkage at 530 deg C. The connectors were made of SAE 4140 Cr-Mo steel. The material for the rod pipes was Fe-0.4C-1Mn steel. Structural stresses played a role in the cracking. Iron sulfide formed on the fracture planes and flake-like stress cracks occurred in the steel. The hydrogen sulfide content...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001494
EISBN: 978-1-62708-235-8
... be seen as grain-boundary network and within the grains. Abstract Abstract Diode leads that were to be made from OFHC copper were instead made from copper with high oxygen content. The leads had a nickel underplating, a gold final plating, and were brazed to the diode package in a hydrogen...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c0046915
EISBN: 978-1-62708-232-7
... boundaries and the hydrogen that readily promoted decarburization with the use of dry (2 to 3% moisture content) coke. Maintaining a thick layer of coke over the entire surface of molten lead in the pan would exclude atmospheric oxygen from the grain boundaries. Decarburizing Lead (metal) Liquid...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001685
EISBN: 978-1-62708-235-8
... lower ductile values than specimens with lower hydrogen content. The role of hydrogen becomes more complicated in the presence of inclusion clusters and slower strain rate conditions. The preponderance of erratic ductile behavior observed in the specimens with higher hydrogen content and tested...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001707
EISBN: 978-1-62708-217-4
... in the shrink link was the result of hydrogen embrittlement, the hydrogen contents of the failed shrink link and a second cracked link were measured by the hot extraction method. This method measures the total hydrogen content of a part. For comparison purposes, the hydrogen contents of a crack-free shrink link...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047192
EISBN: 978-1-62708-235-8
... a hydrogen content in the range of those generally associated with hydrogen embrittlement (>1 ppm). Also, these data indicate a localized hydrogen concentration rather than a uniform distribution throughout the ring. Results of the examination point to a brittle fracture mechanism, as evidenced...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.petrol.c0047537
EISBN: 978-1-62708-228-0
... that initiated at the root and propagated through 50% of wall thickness. 4×. (b) Detail showing crack-initiation site due in part to incomplete fusion on pipe side wall. 12.5× Conclusions In this failure, the hydrogen content will be relatively high because of the nature of cellulosic electrodes...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001447
EISBN: 978-1-62708-235-8
... = 75,000 psi). 1 Intercrystalline cracks appear subsequently and their development is influenced by such factors as the temperature and duration of the heat treatment, the hydrogen content of the atmosphere and the oxygen content and constitution of the copper or alloy. In Figure 1 are shown...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001556
EISBN: 978-1-62708-218-1
... subjected to instrumental gas analysis and the hydrogen gas content was found to be of the order of 18 ppm. Summary and Conclusions Reference Reference 1. Lothar Engle and Hermann Klesigele “An Atlas of Metal Damage” (English version), p. 121 , 122 & 123 , Wolfe Publishing Ltd. , Conway...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001570
EISBN: 978-1-62708-220-4
... to form hydrides if the temperature is sufficiently high. The formation of titanium hydrides becomes significant as the hydrogen content increases above approximately 20 ppm 7 . The hydriding of titanium occurs at higher rates with increasingly higher titanium-dissimilar metal area ratio in the galvanic...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006766
EISBN: 978-1-62708-295-2
... that cover carbon ranges from ~10 ppm to 4% or higher, and sulfur ranges from ~10 ppm to 0.4% or higher. The requisite skill level is comparable to that of the OES technique. Analyses of metal samples to determine nitrogen, oxygen, and hydrogen contents are accomplished by using inert gas fusion...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003552
EISBN: 978-1-62708-180-1
... residual deoxidizer contents—C12000, for example—may contain Cu 2 O but contain less than tough pitch coppers. These deoxidized coppers are not immune to hydrogen embrittlement. Deoxidized coppers with high residual deoxidizer contents, however, are not susceptible to hydrogen embrittlement, because...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006784
EISBN: 978-1-62708-295-2
... coppers with low residual deoxidizer contents—C12000, for example—may contain Cu 2 O but contain less than tough pitch coppers. These deoxidized coppers are not immune to hydrogen embrittlement. Deoxidized coppers with high residual deoxidizer contents, however, are not susceptible to hydrogen...