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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c0048131
EISBN: 978-1-62708-225-9
... Abstract The springs formed from 3.8 mm diam cold-drawn carbon steel wire failed to comply with load-test requirements. A split wire in the spring was revealed by investigation. A smooth heat-tinted longitudinal zone was observed in the fracture. It was concluded that the spring failed...
Abstract
The springs formed from 3.8 mm diam cold-drawn carbon steel wire failed to comply with load-test requirements. A split wire in the spring was revealed by investigation. A smooth heat-tinted longitudinal zone was observed in the fracture. It was concluded that the spring failed in the load test due to the split wire. The reason for the condition was interpreted to be overdrawing which resulted in intense internal strains, high circumferential surface tension, and decreased ductility.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001846
EISBN: 978-1-62708-241-9
... chromium steel circumferential wear marks peel pits heat tinting fatigue striations SEM imaging fatigue strength 42CrMo (chromium-molybdenum alloy steel) 38CrMoAl (chromium-molybdenum-aluminum alloy steel) Background A locomotive turbocharger main shaft and a bearing sleeve assembled...
Abstract
The main shaft in a locomotive turbocharger fractured along with an associated bearing sleeve. Visual and fractographic examination revealed that the shaft fractured at a sharp-edged groove between two journals of different cross-sectional area. The dominant failure mechanism was low-cycle rotation-bending fatigue. The bearing sleeve failed as a result of abrasive and adhesive wear. Detailed metallurgical analysis indicated that the sleeve and its respective journal had been subjected to abnormally high temperatures, increasing the amount of friction between the sleeve, bearing bush, and journal surface. The excessive heat also softened the induction-hardened case on the journal surface, decreasing its fatigue strength. Fatigue crack initiation occurred at the root fillet of the groove because of stress concentration.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0091048
EISBN: 978-1-62708-235-8
... of the supplied sample revealed a single crack, transverse to the fillet weld axis. No bulk macroscopic plastic deformation was associated with the cracking. Relatively high heat input during welding was suggested by the extent of the oxide or heat tint discoloration. The underside of the weld joint contained...
Abstract
A welded ferritic stainless steel heat exchanger cracked prior to service. The welding filler metal was identified as an austenitic stainless steel and the joining method as gas tungsten arc welding. Investigation (visual inspection, SEM images, 5.9x images, and 8.9x/119x images etched with Vilella's reagent followed by electrolytic etching in 10% oxalic acid) supported the conclusion that the heat exchanger cracked due to weld cold cracking or postwelding brittle overload that occurred via flexure during fabrication. The brittle nature of the weld was likely due to a combination of high residual stresses, a mixed microstructure, inclusions, and gross grain coarsening. These synergistic factors resulted from extreme heat input during fillet welding. Recommendations included altering the welding variables such as current, voltage, and travel speed to substantially reduce the heat input.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c9001204
EISBN: 978-1-62708-219-8
... ). The previously mentioned unfavorable fiber direction of these pieces can also be seen from the secondary banded structure. The weld seams consisted of austenitic steel. They were permeated with hot tears ( Fig. 9 ) as could be concluded already from the heat tinting of the fractures. The transition zones were...
Abstract
Two bolts from the stressed structure of a church building that had broken during stressing were examined to establish the cause of fracture. The fracture of one of the first bolt occurred in a double-vee groove weld whose root was not completely welded. The second bolt had cracked outside of the weld seam closely under the head. Neither one had been particularly deformed before fracture. The composition of the head pieces corresponded approximately to manganese steel (Material No. 1 0845), a weldable construction steel with increased yield point and strength, while the shafts were made from Cr-Mo steel (Material No. 1.7225) according to DIN 17200. It was found that the bolts were not made from a suitable alloy steel, but were welded together from two unsuitable steels, one of which lacked sufficient strength. The austenitic weld seams showed hot tears and were not welded through to the root. Also, the pieces were not preheated before welding, so that stress cracks occurred in the transition zones. The second bolt was overstressed during the impact caused by the breaking of the first bolt.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c0048757
EISBN: 978-1-62708-234-1
... of the overheated tube disclosed blue-tinted areas and patches of flaky white, yellow, and brown oxide scale. There was a dark-gray scale on the inside surface with no evidence of corrosion. The presence of the colored scale on the outer and inner surfaces was an indication of heating to approximately 815 °C (1500...
Abstract
Brief overheating of the 89 mm OD 6.4 mm wall thickness titanium heater tubes (ASTM B337, grade 2) was caused by a flow stoppage in a leach heater. Blue-tinted areas and patches of flaky white, yellow, and brown oxide scale was revealed on visual examination. It was disclosed by subjecting the overheated tube to a flattening test that the tube no longer met ASTM B 337 specifications. Large grain size and numerous needlelike hydride particles were disclosed in the microstructure of the overheated tube. Heating to approximately 815 deg C was revealed by the presence of the flaky oxide and increased grain size. Hydrogen and oxygen absorption was revealed by the presence of hydrides and the shallow surface embrittlement and thus susceptibility to cracking at ambient temperatures was observed. It was concluded that the titanium tubes were embrittled due to overheating the tubes and the severe surface embrittlement resulted from oxygen absorption which made the surface layers susceptible to cracking under start up and shutdown. Replacement tubes made of a heat-resistant alloy (e.g., Hastelloy C-276) were recommended.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001754
EISBN: 978-1-62708-241-9
... was apparent on each, which varied in size among all the individual balls. Spalling was also visible in varying degrees. No heat tinting or elevated temperature indications were observed. Each bearing ball diameter was measured in three directions using a caliper. No significant ball reductions were observed...
Abstract
The case study presented in this article details the failure investigation of an M50 alloy steel bearing used in a jet engine gearbox drive assembly. It discusses the investigative steps and analytic tools used to determine the root cause, highlighting the importance of continuous, thorough questioning by the investigating activity. The combined analyses demonstrated that the bearing failed by a single event overload as evidenced by bulk deformation and traces of foreign material on the rolling elements. The anomalous transferred metal found on the rolling elements subsequently led to the discovery of overlooked debris in an engine chip detector, and thus resulted in a review of several maintenance practices.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001482
EISBN: 978-1-62708-229-7
... in the vicinity of the fissures and along the surface of the tube for a distance of about 5 8 in. from the weld. While copper particles were not to be seen within the main fissure or along the bore side of the tube with the specimen in the etched condition, heat-tinting at 300°C revealed them as shown...
Abstract
Penetration by molten copper occurred in the economizer of a large water-tube boiler. A cross section through a weld and the crack in the tube revealed a crack was an intergranular fissure. Small fissures of the same type also extended from its flanks. The main fissure was filled with an oxide scale in which were embedded particles having the appearance of metallic copper. It was concluded that the cracking that occurred at the time of re-welding was due to intergranular penetration by copper present in the deposit within the tubes, which had not been completely removed prior to welding. Subsequently, it was ascertained that trouble had been experienced with the centrifugal feed pumps, resulting in scuffing of some bronze rings. The presumption is that bronze particles had been carried in mechanical suspension in the feed water and deposited in the economizer tubes.
Book Chapter
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006804
EISBN: 978-1-62708-329-4
... to radiant heating, which is line-of-sight. Fig. 15 Example of melted aluminum cladding on an insulated vessel. Aluminum melts at 657 °C (1215 °F), which places the areas of melting in heat exposure zone V. Heat Tinting Following a fire, metal surfaces can often be found to be discolored...
Abstract
This article addresses the effects of damage to equipment and structures due to explosions (blast), fire, and heat as well as the methodologies that are used by investigating teams to assess the damage and remaining life of the equipment. It discusses the steps involved in preliminary data collection and preparation. Before discussing the identification, evaluation, and use of explosion damage indicators, the article describes some of the more common events that are considered in incident investigations. The range of scenarios that can occur during explosions and the characteristics of each are also covered. In addition, the article primarily discusses level 1 and level 2 of fire and heat damage assessment and provides information on level 3 assessment.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047756
EISBN: 978-1-62708-235-8
... extremities of a granular gold-tinted surface region adjacent to the tube-to-sleeve brazed joint and extending circumferentially were revealed by microscopic examination. Embrittlement of the tube caused by molten braze metal penetration along grain boundaries was evidenced by micrographs of a granular...
Abstract
Waspaloy (AMS 5586) fabricated inner ring of a spray-manifold assembly failed transversely through the manifold tubing at the edge of the tube and support sleeve brazed joint. The assembly was brazed with AWS BAu-4 filler metal (AMS 4787). Fatigue beach marks propagating from extremities of a granular gold-tinted surface region adjacent to the tube-to-sleeve brazed joint and extending circumferentially were revealed by microscopic examination. Embrittlement of the tube caused by molten braze metal penetration along grain boundaries was evidenced by micrographs of a granular portion of the fracture. It was revealed by the initial fracture profile that fatigue cracks begun as an intergranular separation and subsequently became transgranular. It was concluded that failure of the tube was caused by excessive alloying between the braze metal and the Waspaloy. Reduced temperatures during torch debrazing or rebrazing were recommended to minimize molten braze metal penetration.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001305
EISBN: 978-1-62708-215-0
... surface shwon in Fig. 1 after cleaning. Fracture initiated in the flange and propagated across the rim, plate, and hub. Although not evident in Fig. 2 , two zones exhibited definite signs of heating. The entire hub fracture surface was tinted blue, indicating it reached temperatures...
Abstract
An ASTM A 504 carbon steel railway car wheel that was used on a train in a metropolitan railway system failed during service, causing derailment. The wheel was completely fractured from rim to hub. Macrofractography of the fracture surface showed road grime, indicating that the crack had existed for a considerable time prior to derailment and initiated in the flange. Failure propagated from the flange across the rim and down the plate to the bore of the hub. Two zones that exhibited definite signs of heating were observed. The fracture initiation site was typical of fatigue fracture. No defects were found that could have contributed to failure. The wheel conformed to the chemical, microstructural, and hardness requirements for class A wheels. Failure was attributed to repeated severe heating and cooling of the rim and flange due to brake locking or misapplication of the hand brake. It was recommended that the brake system on the car be examined and replaced if necessary.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001773
EISBN: 978-1-62708-241-9
... B to Plate A. Furthermore, a dark line indicative of heat tint, identifies the HAZ relative to the side of the plate shown in Fig. 6 . A close-up view of the cracks in Plate A is shown in Fig. 7 , with the cracks observed to be fine and branched across the surface of the plate. The red material...
Abstract
A spiral heat exchanger made from 316L stainless steel developed a leak after eight years of service as a condenser on a distillation tower. Examination identified the leak as being located on the cooling water side in the heat affected zone (HAZ) of a weld joining two plates. Cooling water deposits were observed in a V-shaped corner formed by the weld. A metallurgical examination identified the presence of transgranular cracks in the HAZ on the cooling water side. Analysis of the cooling water revealed the presence of chlorides. Based on the metallurgical analysis and other findings, it was determined that the cracks and associated leak were the result of chloride stress-corrosion cracking.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001126
EISBN: 978-1-62708-214-3
... ( 1 4 in.) heat-strengthened, gray-tinted glass intended for installation with a backup wall. The specified glass product has a transparent metallic oxide coating on the outer surface and a solid color ceramic frit on the back surface. The installed glass differed from the specifications...
Abstract
The spontaneous breakage of tempered glass spandrel panels used to cover concrete wall panels on building facades was investigated. Between January 1988 and August 1990, 19 panel failures were recorded. The tinted panels were coated on their exterior surfaces with a reflective metal oxide and covered on the back surfaces with an adherent black polyethylene plastic. Macro fractography, SEM fractography, EDX analysis, and photo elasticimetry were conducted on four of the shattered panels. Small nickel sulfide inclusions were found at the failure origins. Failure of the panels was attributed to growth of the inclusions, coupled with high residual stresses. Fracture mechanics analysis showed that the residual stresses alone were high enough to cause fracture of the glass, with a flaw of the size observed.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006808
EISBN: 978-1-62708-329-4
... is not necessarily a defect. Welding is defined as a joining process producing coalescence of materials by heating them to the welding temperature, with or without the application of pressure or by the application of pressure alone, and with or without the use of filler material. So, welding may or may...
Abstract
This article describes some of the welding discontinuities and flaws characterized by nondestructive examinations. It focuses on nondestructive inspection methods used in the welding industry. The sources of weld discontinuities and defects as they relate to service failures or rejection in new construction inspection are also discussed. The article discusses the types of base metal cracks and metallurgical weld cracking. The article discusses the processes involved in the analysis of in-service weld failures. It briefly reviews the general types of process-related discontinuities of arc welds. Mechanical and environmental failure origins related to other types of welding processes are also described. The article explains the cause and effects of process-related discontinuities including weld porosity, inclusions, incomplete fusion, and incomplete penetration. Different fitness-for-service assessment methodologies for calculating allowable or critical flaw sizes are also discussed.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001713
EISBN: 978-1-62708-220-4
... (several millimeters) located near the off-loading port, that is most likely a result of the damage done to the blender during the accident. No local regions of melting or heat tinting were found. These findings indicate the chemical reactions did not initiate at the surface of the shell, where water from...
Abstract
On 21 April 1995, the contents of a large blender (6 cu m) reacted and caused an explosion that killed and injured a number of workers at a plant in Lodi, NJ. A mixture of sodium hydrosulfite and aluminum powder was being mixed at the time of the accident. This report focuses on evaluations of the blender to determine if material or mechanical failures were the cause of the accident. The results indicate that the mixing vessel was metallurgically sound and did not contribute to the initiation of the failure. However, the vessel was not designed for mixing chemicals that must be isolated from water and excessive heat. Water leaking into the vessel through a graphite seal may have initiated the reactions that caused the accident.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001799
EISBN: 978-1-62708-241-9
... also smeared at some locations. High-temperature color bands were present on fractured surface. These bands were due to heat tinting probably resulting from friction on the fracture surfaces prior to and after final failure. Dark bands were observed on the shaft on ‘motor side’ of the fractured surface...
Abstract
A high-speed pinion gear shaft, part of a system that compresses natural gas, was analyzed to determine why it failed. An abnormal wear pattern was observed on the shaft surface beneath the inner race of the support bearings. Material from the shaft had transferred to the bearing races, creating an imbalance (enough to cause noise and fumes) that operators noted two days before the failure. Macrofeatures of the fracture surface resembled those of fatigue, but electron microscopy revealed brittle, mostly intergranular fracture. Classic fatigue features such as striations were not found. To resolve the discrepancy, investigators created and tested uniaxial fatigue samples, and the microfeatures were nearly identical to those found on the failed shaft. The root cause of failure was determined to be fatigue, and it was concluded that cracks on the pinion shaft beneath the bearings led to the transfer of material.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001255
EISBN: 978-1-62708-232-7
... off neck. In the centre of the fracture is a darkly tinted excentric flaw ( Fig. 2 ). Such internal cracks occur when a cast or forged work piece is heated up too quickly and insufficiently thoroughly for the anneal. The thermal expansion of the outer zone puts the central core under tensile stress...
Abstract
Several back up rolls of 1400 mm barrel diam from a broad strip mill broke after a relatively short operating time as a result of bending stresses when the rolls were dismantled. The fracture occurred in the conical region of the neck at about 600 mm diam. The rolls were shaped steel castings with 0.8 to 1.0% C, 1% Mn, 1% Cr, 0.5% Mo and 0.4% Ni and were heat treated to a tensile strength of 950 N/sq mm. Because the bending stress on mounting was only 42 N/sq mm in the fracture cross section, it was evident at the outset that material defects had promoted the fracture. In the case of this roll and the other broken rolls, the cracking and fracture were promoted by various casting defects. Investigation of the rolls showed that both the breaking off of the neck and the disintegration of the barrel edges was caused by material defects, more exactly casting defects. The fractures on the other rolls examined were so badly rusted or contaminated that they were incapable of yielding any information.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001826
EISBN: 978-1-62708-241-9
... is greatly influenced by the amount of corrosion product deposited on the wall of the tube. The deposit buildups are most likely to occur where flow is disrupted by bends; welds with backing rings or protrusions; at regions of high heat flux; and on horizontal or slanted tubes that are heated from above...
Abstract
A back wall riser tube in a high pressure boiler failed, interrupting operations in a cogeneration plant. The failure occurred in a tube facing the furnace, causing eight ruptured openings over a 1.8 m section. The investigation consisted of an on-site visual inspection, nondestructive testing, energy dispersive x-ray analysis, and inductively coupled plasma mass spectrometry. The tube was made from SA 210A1 carbon steel that had been compromised by wall thinning and the accumulation of fire and water-side scale deposits. Investigators determined that the tube failed due to prolonged caustic attack that led to ruptures in areas of high stress. The escaping steam eroded the outer surface of the tube causing heavy loss of metal around the rupture points.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001082
EISBN: 978-1-62708-214-3
... fracture. This will be discussed below. Macrofractography The specimen shown in Fig. 4 was cut open to reveal the fracture surface ( Fig. 11 ). The fracture face exhibited intergranular fracture propagation. The crack surface contained pits and heat tinting. Fig. 11 Photomacrograph...
Abstract
Several large-diameter type 304L stainless steel impeller/propeller blades in a circulating water pump failed after approximately 8 months of operation. The impeller was a single casting that had been modified with a fillet weld buildup at the blade root. Visual examination indicated that the fracture originated near the blade-to-hub attachment in the area of the weld buildup. Specimens from four failed castings and from an impeller that had developed cracks prior to design modification were subjected to a complete analysis. A number of finite-element-method computer models were also constructed. It was determined that the blades failed by fatigue that had been accelerated by stress-corrosion cracking. The mechanism of failure was flow-induced vibration, in which the vortex-shedding frequencies of the blades were attuned to the natural frequency of the blade/hub configuration. A number of solutions involving material selection and impeller redesign were recommended.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003556
EISBN: 978-1-62708-180-1
... have shown that heat-tinted zones are especially vulnerable. These zones are created in a welding process where material above the scaling temperature is contacted by air. The result is a migration of chromium into the surface scale, leaving underlying material depleted and susceptible to corrosion...
Abstract
This article focuses on the mechanisms of microbially induced or influenced corrosion (MIC) of metallic materials as an introduction to the recognition, management, and prevention of microbiological corrosion failures in piping, tanks, heat exchangers, and cooling towers. It discusses the degradation of various protective systems, such as corrosion inhibitors and lubricants. The article describes the failure analysis of steel, iron, copper, aluminum, and their alloys. It also discusses the probes available to monitor conditions relevant to MIC in industrial systems and the sampling and analysis of conditions usually achieved by the installation of removable coupons in the target system. The article also explains the prevention and control strategies of MIC in industrial systems.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001020
EISBN: 978-1-62708-214-3
... in the fully heat-treated condition. Specimen Selection Figure 3 shows the affected strut cylinder and fractured lower drag-strut attachment lugs (smaller arrows). In Fig. 3 , the triangular drag-strut attachment yoke is shown rotated back about the still intact upper attachment lug pivot. The 25.4...
Abstract
The right landing gear on a twin-turboprop transport aircraft collapsed during landing. Preliminary examination indicated that the failure occurred at a steel-to-aluminum (7014) pinned drag-strut connection due to fracture of the lower set of drag-strut attachment lugs at the lower end of the oleo cylinder housing. Two lug fractures that were determined to be the primary fractures were analyzed. Results of various examinations indicated that stress-corrosion cracking associated with the origins of the principal fractures in the connection was the cause of failure. It was recommended that the design be modified to avoid dissimilar metal combinations of high corrosion potential.
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