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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.conag.c9001198
EISBN: 978-1-62708-221-1
... consisted of graphite in pearlitic-ferritic matrix. Casting stresses did not play a decisive role because of the simple shape of the pieces that were without substantial cross sectional variations. Two factors exerted an unfavorable effect in addition to comparatively low strength. First, the operating...
Abstract
Cast iron bearing caps in tractor engines fractured repeatedly after only short operating periods. The fracture originated in a cast-in groove and ran approximately radially to the shaft axis. The smallest cross section was at the point of fracture. The core structure of the caps consisted of graphite in pearlitic-ferritic matrix. Casting stresses did not play a decisive role because of the simple shape of the pieces that were without substantial cross sectional variations. Two factors exerted an unfavorable effect in addition to comparatively low strength. First, the operating stress was raised locally by the sharp-edged groove, and second, the fracture resistance of the cast iron was lowered at this critical point by the existence of a ferritic bright border. To avoid such damage in the future it was recommended to observe one or more of the following precautions: 1) Eliminate the grooves; 2) Remove the ferritic bright border; 3) Avoid undercooling in the mold and therefore the formation of granular graphite; 4) Inoculate with finely powdered ferrosilicon into the melt for the same purpose; and, 5) Anneal at lower temperature or eliminate subsequent treatment in consideration of the uncomplicated shape of the castings.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001202
EISBN: 978-1-62708-234-1
... Abstract Two damaged impellers made of austenitic cast iron came from a rotary pump used for pumping brine mixed with drifting sand. On one of the impellers, pieces were broken out of the back wall in four places at the junction to the blades. The fracture edges followed the shape of the blade...
Abstract
Two damaged impellers made of austenitic cast iron came from a rotary pump used for pumping brine mixed with drifting sand. On one of the impellers, pieces were broken out of the back wall in four places at the junction to the blades. The fracture edges followed the shape of the blade. Numerous cavitation pits were seen on the inner side of the front wall visible through the breaks in the back wall. The back wall of the as yet intact second impeller which did not show such deep cavitation pits was cracked in places along the line of the blades. The microstructure consisted of lamellar graphite and carbides in an austenitic matrix and was considered normal for the specified material GGL Ni-Cu-Cr 15 6 2. It was concluded that the cause of the damage was porosity at the junction between back wall and blades arising during the casting process. Cavitation did not contribute to fracture but also could have led to damage in the long term in the case of a sound casting. It is therefore advisable in the manufacture of new impellers to take care not only to avoid porosity but also to use alloy GGL Ni-Cu-Cr 15 6 3, which has a higher chromium content and is more resistant to cavitation.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006831
EISBN: 978-1-62708-329-4
... be revealed by etching to exhibit cell boundaries. Graphite The size, shape, orientation, and distribution of the eutectic graphite particles in castings of gray iron (and ductile and malleable irons) determine the mechanical properties of the castings. For any given gray iron composition, the rate...
Abstract
The information provided in this article is intended for those individuals who want to determine why a casting component failed to perform its intended purpose. It is also intended to provide insights for potential casting applications so that the likelihood of failure to perform the intended function is decreased. The article addresses factors that may cause failures in castings for each metal type, starting with gray iron and progressing to ductile iron, steel, aluminum, and copper-base alloys. It describes the general root causes of failure attributed to the casting material, production method, and/or design. The article also addresses conditions related to the casting process but not specific to any metal group, including misruns, pour shorts, broken cores, and foundry expertise. The discussion in each casting metal group includes factors concerning defects that can occur specific to the metal group and progress from melting to solidification, casting processing, and finally how the removal of the mold material can affect performance.
Book Chapter
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003508
EISBN: 978-1-62708-180-1
... and cavitation pits on the front wall. (b) Cracks following the shape of the blades on the back wall of impeller 2. Both 0.7×. Source: Ref 11 The microstructure shown in Fig. 7 , illustrating lamellar graphite and carbides in an austenitic matrix, can be considered normal for the specified material...
Abstract
This article focuses on the general root causes of failure attributed to the casting process, casting material, and design with examples. The casting processes discussed include gravity die casting, pressure die casting, semisolid casting, squeeze casting, and centrifugal casting. Cast iron, gray cast iron, malleable irons, ductile iron, low-alloy steel castings, austenitic steels, corrosion-resistant castings, and cast aluminum alloys are the materials discussed. The article describes the general types of discontinuities or imperfections for traditional casting with sand molds. It presents the international classification of common casting defects in a tabular form.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c0047220
EISBN: 978-1-62708-220-4
... well-shaped nodules of graphite generally surrounded by ferrite envelopes. The gray iron exhibited a pearlitic matrix containing type A graphite flakes. There were no metallurgical causes of failure other than the inherent brittleness of gray iron, and there was no evidence of machining imperfections...
Abstract
Two oil-pump gears broke after four months of service in a gas compressor that operated at 1000 rpm and provided a discharge pressure of 7240 kPa (1050 psi). The compressor ran intermittently with sudden starts and stops. The large gear was sand cast from class 40 gray iron with a tensile strength of 290 MPa (42 ksi) at 207 HRB. The smaller gear was sand cast from ASTM A536, grade 100-70-03, ductile iron with a tensile strength of 696 MPa (101 ksi) at 241 HRB. Analysis (metallographic examination) supported the conclusion that excessive beam loading and a lack of ductility in the gray iron gear teeth were the primary causes of fracture. During subsequent rotation, fragments of gray iron damaged the mating ductile iron gear. Recommendations included replacing the large gear material with ASTM A536, grade 100-70-03, ductile iron normalized at 925 deg C (1700 deg F), air cooled, reheated to 870 deg C (1600 deg F), and oil quenched. The larger gear should be tempered to 200 to 240 HRB, and the smaller gear to 240 to 280 HRB.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001713
EISBN: 978-1-62708-220-4
... be isolated from water and excessive heat. Water leaking into the vessel through a graphite seal may have initiated the reactions that caused the accident. Blenders Chemical processing equipment Explosions Stainless steel (Other, miscellaneous, or unspecified) failure Ductile fracture...
Abstract
On 21 April 1995, the contents of a large blender (6 cu m) reacted and caused an explosion that killed and injured a number of workers at a plant in Lodi, NJ. A mixture of sodium hydrosulfite and aluminum powder was being mixed at the time of the accident. This report focuses on evaluations of the blender to determine if material or mechanical failures were the cause of the accident. The results indicate that the mixing vessel was metallurgically sound and did not contribute to the initiation of the failure. However, the vessel was not designed for mixing chemicals that must be isolated from water and excessive heat. Water leaking into the vessel through a graphite seal may have initiated the reactions that caused the accident.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.9781627083294
EISBN: 978-1-62708-329-4
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006778
EISBN: 978-1-62708-295-2
... • Multiple intergranular cracks • Voids formed on grain boundaries or wedge-shaped cracks at grain triple points • Reaction scales or internal precipitation • Some cold flow in last stages of failure Contributing factors • Load exceeded the strength of the part • Check for proper alloy and processing...
Abstract
This article aims to identify and illustrate the types of overload failures, which are categorized as failures due to insufficient material strength and underdesign, failures due to stress concentration and material defects, and failures due to material alteration. It describes the general aspects of fracture modes and mechanisms. The article briefly reviews some mechanistic aspects of ductile and brittle crack propagation, including discussion on mixed-mode cracking. Factors associated with overload failures are discussed, and, where appropriate, preventive steps for reducing the likelihood of overload fractures are included. The article focuses primarily on the contribution of embrittlement to overload failure. The embrittling phenomena are described and differentiated by their causes, effects, and remedial methods, so that failure characteristics can be directly compared during practical failure investigation. The article describes the effects of mechanical loading on a part in service and provides information on laboratory fracture examination.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003551
EISBN: 978-1-62708-180-1
... layers or more with thicknesses varying from at least 100 mm (4 in.) up to 500 mm (20 in.) or more. Refractories are either shaped materials (bricks and various other formats, including lances, tubes, nozzles, and so forth) or unshaped or monolithic materials (delivered to the users in bags, sacks...
Abstract
This article provides a discussion on the structural ceramics used in gas turbine components, the automotive and aerospace industries, or as heat exchangers in various segments of the chemical and power generation industries. It covers the fundamental aspects of chemical corrosion and describes the corrosion resistance characteristics of specific classes of refractories and structural ceramics. The article also examines the prevention strategies that minimize corrosion failures of both classes of materials.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003543
EISBN: 978-1-62708-180-1
... at surface or brittle phases internally • Progressive zone: usually transgranular with little apparent distortion• Overload zone: may be either ductile or brittle • Microstructural change typical of overheating• Multiple intergranular cracks• Voids formed on grain boundaries or wedge shaped cracks at grain...
Abstract
Overload failures refer to the ductile or brittle fracture of a material when stresses exceed the load-bearing capacity of a material. This article reviews some mechanistic aspects of ductile and brittle crack propagation, including a discussion on mixed-mode cracking, which may also occur when an overload failure is caused by a combination of ductile and brittle cracking mechanisms. It describes the general aspects of fracture modes and mechanisms. The article discusses some of the material, mechanical, and environmental factors that may be involved in determining the root cause of an overload failure. It also presents examples of thermally and environmentally induced embrittlement effects that can alter the overload fracture behavior of metals.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006869
EISBN: 978-1-62708-395-9
... of (a) the compositions 5 vol% polytetrafluoroethylene + 5 vol% graphite + 15 vol% short carbon fiber (SCF) and (b) 5 vol% nano- titanium oxide + 5 vol% graphite + 15 vol% SCF at 2 MPa and 1 m/s. Adapted from Ref 56 . Courtesy of Elsevier Abstract Reinforced polymers (RPs) are widely used in structural...
Abstract
Reinforced polymers (RPs) are widely used in structural, industrial, automotive, and engineering applications due to their ecofriendly nature and the potential to manipulate their properties. This article addresses the technical synthesis of RPs, referring to their tribological behavior, to provide insights into the contribution and interaction of influential parameters on the wear behavior of polymers. It provides a brief discussion on the effects of significant parameters on RP tribology. The article describes abrasive and adhesive wear and provides a theoretical synthesis of the literature regarding the wear mechanisms of RPs. It also describes the synthesis of abrasive wear failure of different types of RPs and highlights the contribution of these influential parameters. The article addresses the synthesis of adhesive wear failure of different types of RPs.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001802
EISBN: 978-1-62708-241-9
... of Precipitated NiTi Shape Memory Alloys ,” Int. J. Fracture , 2001 , 109 , pp. 189 – 207 10.1023/A:1011069204123 . 2. Miao W. , Mi X. , Zhu M. , Guo J. , and Kou Y. : “ Effect of Surface Preparation on Mechanical Properties of a NiTi Alloy ,” Mater. Sci. Forum , 2002 , 394...
Abstract
Superelastic nitinol wires that fractured under various conditions were examined under a scanning electron microscope in order to characterize the fracture surfaces, produce reference data, and compare the findings with prior published work. The study revealed that nitinol fracture modes and morphologies are generally consistent with those of ductile metals, such as austenitic stainless steel, with one exception: Nitinol exhibits a unique damage mechanism under high bending strain, where damage occurs at the compression side of tight bends or kinks while the tensile side is unaffected. The damage begins as slip line formation due to plastic deformation, which progresses to cracking at high strain levels. The cracks appear to initiate from slip lines and extend in shear (mode II) manner.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.machtools.c0091853
EISBN: 978-1-62708-223-5
..., showing placement of the attrition mill wear plates In Fig. 2 , a new, unused grinding plate (left) is a 230 mm (9 in.) diameter and 25 mm (1 in.) thick disk of gray cast iron with a hardness of 338 HV and 0.1 mm (0.004 in.) graphite flakes, which are an excellent absorber of vibrations during...
Abstract
A 230 mm (9 in.) diameter disk attrition mill was scheduled to grind 6.35 mm (0.25 in.) diameter quartz particles to a 0.075 mm (0.003 in.) diameter powder. Due to severe wear on the grinding plates, however, the unit was unable to complete the task of grinding the rock. The mill consisted of a heavy gray cast iron frame, a gravity feeder port, a runner, and a heavy-duty motor. The frame and gravity feeder weighed over 200 kg (440 lb) and, in some areas, was over 25 mm (1 in.) thick. To obtain the operating speed of 200 rpm, a gear system was used to transmit the torque from the 2-hp motor. The runner consisted of a 50 mm (2 in.) diameter shaft and two gray cast iron grinding plates. Investigation (visual inspection, historical review, photographs, model testing of new plates, chemical analysis, hardness testing, optical macrographs, and optical micrographs) supported the conclusion that the primary feed material was harder than the grinding plates, causing wear and eventual failure. Recommendations included reducing the clearance between the flutes and possible material changes.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001598
EISBN: 978-1-62708-232-7
... liquid penetrant tested, and no indications were observed. The vessel was then placed in an induction furnace contained within a graphite crucible. Alumina powder was placed on the bottom of the graphite crucible to contrast any glass that might leak from the melter during the test. A prototypic charge...
Abstract
The metallurgical condition of a cylindrical induction melter (CIM) vessel was evaluated after approximately 375 h of operation over a two-year span at temperatures between 1400 to 1500 deg C. Wall thinning and significant grain growth was observed in the lower portion of the conical section and the drain tube. No through-wall penetrations were found in the cylindrical and conical sections of the CIM vessel and only one leak site was identified in the drain tube. Failure of the drain tube was associated with localized overheating and creep. The observed degradation resulted from cumulative service at elevated temperature. A recommendation was made to implement a support for the conical section of the CIM and to increase the wall thickness of the drain tube. Thus, the possibility of drain tube misalignment in the induction coils and localized over heating will be minimized. In addition, the use of grain stabilized Pt/Rh alloy should be evaluated as a method to prevent grain growth.
Book Chapter
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003548
EISBN: 978-1-62708-180-1
... denickelification desiliconification dezincification galvanic corrosion graphitic corrosion intergranular corrosion pitting corrosion selective leaching uniform corrosion velocity-affected corrosion CORROSION is the electrochemical reaction of a material and its environment. This article addresses...
Abstract
This article addresses the forms of corrosion that contribute directly to the failure of metal parts or that render them susceptible to failure by some other mechanism. It describes the mechanisms of corrosive attack for specific forms of corrosion such as galvanic corrosion, uniform corrosion, pitting and crevice corrosion, intergranular corrosion, and velocity-affected corrosion. The article contains a table that lists combinations of alloys and environments subjected to selective leaching and the elements removed by leaching.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006783
EISBN: 978-1-62708-295-2
... (the relative area, distance, and shape) of the components. Geometric Factors Effect of Surface Area The relative size of the anodic and cathodic surfaces is important. The intensity of galvanic attack is related to the relative size of the metals in electrical contact and the electrolyte. Large...
Abstract
Corrosion is the electrochemical reaction of a material and its environment. This article addresses those forms of corrosion that contribute directly to the failure of metal parts or that render them susceptible to failure by some other mechanism. Various forms of corrosion covered are galvanic corrosion, uniform corrosion, pitting, crevice corrosion, intergranular corrosion, selective leaching, and velocity-affected corrosion. In particular, mechanisms of corrosive attack for specific forms of corrosion, as well as evaluation and factors contributing to these forms, are described. These reviews of corrosion forms and mechanisms are intended to assist the reader in developing an understanding of the underlying principles of corrosion; acquiring such an understanding is the first step in recognizing and analyzing corrosion-related failures and in formulating preventive measures.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006808
EISBN: 978-1-62708-329-4
.... Fig. 3 Schematic of defects and discontinuities in welded joints Fig. 4 Weld discontinuities affecting weld shape and contour. (a) Undercut and overlap in a fillet weld. (b) Undercut and overlap in a groove weld. (c) and (d) Underfill in groove welds It is important to understand...
Abstract
This article describes some of the welding discontinuities and flaws characterized by nondestructive examinations. It focuses on nondestructive inspection methods used in the welding industry. The sources of weld discontinuities and defects as they relate to service failures or rejection in new construction inspection are also discussed. The article discusses the types of base metal cracks and metallurgical weld cracking. The article discusses the processes involved in the analysis of in-service weld failures. It briefly reviews the general types of process-related discontinuities of arc welds. Mechanical and environmental failure origins related to other types of welding processes are also described. The article explains the cause and effects of process-related discontinuities including weld porosity, inclusions, incomplete fusion, and incomplete penetration. Different fitness-for-service assessment methodologies for calculating allowable or critical flaw sizes are also discussed.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001543
EISBN: 978-1-62708-218-1
... with a carbide compound, providing it with a heat-resistant material where temperatures are extremely high. Second, pistons could be of an aluminum-graphite or aluminum-boron composite, eliminating surface melting because pure aluminum has a melting point 200 F higher than the interdendritic material...
Abstract
To determine the effect of severe service on cast 357 aluminum pistons, a metallurgical evaluation was made of four pistons removed from the engine of the Hawk-Offenhauser car which had been driven by Rich Muther in the first Ontario, California 500 race. The pistons were studied by visual inspection, hardness traverses, radiography, dye penetrant inspection, chemical analysis, macrometallography, optical microscopy, and electron microscopy. The crown of one piston had a rough, crumbly deposit, which was detachable with a knife. Two pistons had remains of carbonaceous deposits. The fourth was severely hammered. It was concluded that the high temperatures developed in this engine created an environment too severe for 357 aluminum. Surfaces were so hot that the low-melting constituent melted. Then, the alloy oxidized rapidly to form Al2O3, an abrasive which further aggravated problems. The temperature in much of the piston was high enough to cause softening by overaging, lowering strength.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003572
EISBN: 978-1-62708-180-1
... can be overcome efficiently by the right selection of reinforcements and fillers in the appropriate amount, combination, and processing technology. The tribological performance of reinforced polymers is governed by the type of base matrix, the nature of the filler (type, amount, size, shape...
Abstract
This article reviews the abrasive and adhesive wear failure of several types of reinforced polymers, including particulate-reinforced polymers, short-fiber reinforced polymers (SFRP), continuous unidirectional fiber reinforced polymers (FRP), particulate-filled composites, mixed composites (SFRP and particulate-filled), unidirectional FRP composites, and fabric reinforced composites. Friction and wear performance of the composites, correlation of performance with various materials properties, and studies on wear-of failure mechanisms by scanning electron microscopy are discussed for each of these types.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006793
EISBN: 978-1-62708-295-2
... of temperature over the range tested. However, the impact craters of the samples tested at lower temperatures showed more microcracks stemming from the opening of grain boundaries. Wear Debris The size and shape of wear debris particles arising from normal and compound wear vary depending on the material...
Abstract
Impact or percussive wear is defined as the wear of a solid surface that is due to percussion, which is a repetitive exposure to dynamic contact by another body. Impact wear, however, has many analogies to the field of erosive wear. The main difference is that, in impact wear situations, the bodies tend to be large and contact in a well-defined location in a controlled way, unlike erosion where the eroding particles are small and interact randomly with the target surface. This article describes some generic features and modes of impact wear of metals, ceramics, and polymers. It discusses the processes involved in testing and modeling of impact wear, and includes two case studies.
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