This article provides an overview of fractography and explains how it is used in failure analysis. It reviews the basic types of fracture processes, namely, ductile, brittle, fatigue, and creep, principally in terms of fracture appearances, such as microstructure. The article also describes the general features of fatigue fractures in terms of crack initiation and fatigue crack propagation.

Engineering component and structure failures manifest through many mechanisms but are most often associated with fracture in one or more forms. This article introduces the subject of fractography and aspects of how it is used in failure analysis. The basic types of fracture processes (ductile, brittle, fatigue, and creep) are described briefly, principally in terms of fracture appearances. A description of the surface, structure, and behavior of each fracture process is also included. The article provides a framework from which a prospective analyst can begin to study the fracture of a component of interest in a failure investigation. Details on the mechanisms of deformation, brittle transgranular fracture, intergranular fracture, fatigue fracture, and environmentally affected fracture are also provided.

This article commences with a summary of fatigue processes and mechanisms. It focuses on fractography of fatigue. Characteristic fatigue fracture features that can be discerned visually or under low magnification are described. Typical microscopic features observed on structural metals are presented subsequently, followed by a brief discussion of fatigue in nonmetals. The article reviews the various macroscopic and microscopic features to characterize the history and growth rate of fatigue in metals. It concludes with a description of fatigue of polymers and composites.

Fatigue failure of engineering components and structures results from progressive fracture caused by cyclic or fluctuating loads. Fatigue is an important potential cause of mechanical failure, because most engineering components or structures are or can be subjected to cyclic loads during their lifetime. This article focuses on fractography of fatigue. It provides an abbreviated summary of fatigue processes and mechanisms: fatigue crack initiation, fatigue crack propagation, and final fracture,. Characteristic fatigue fracture features that can be discerned visually or under low magnification are then described. Typical microscopic features observed on structural metals are presented subsequently, followed by a brief discussion on fatigue in polymers and polymer-matrix composites.

This article focuses on characterizing the fracture-surface appearance at the microscale and contains some discussion on both crack nucleation and propagation mechanisms that cause the fracture appearance. It begins with a discussion on microscale models and mechanisms for deformation and fracture. Next, the mechanisms of void nucleation and void coalescence are briefly described. Macroscale and microscale appearances of ductile and brittle fracture are then discussed for various specimen geometries (smooth cylindrical and prismatic) and loading conditions (e.g., tension compression, bending, torsion). Finally, the factors influencing the appearance of a fracture surface and various imperfections or stress raisers are described, followed by a root-cause failure analysis case history to illustrate some of these fractography concepts.

The shaft of an exciter that was used with a diesel-driven electric generator broke at a fillet after ten hours of service following resurfacing of the shaft by welding. The fracture surface contained a dull off-center region of final ductile fracture surrounded by regions of fatigue that had been subjected to appreciable rubbing. The fracture appeared to be typical of rotary bending fatigue under conditions of a low nominal stress with a severe stress concentration. It appeared that the fatigue cracks initiated in the surface-weld layer. The weld deposit in the original keyway displays a lack of fusion at the bottom corner. Fatigue fracture of the shaft resulted from stresses that were created by vibration acting on a crack or cracks formed in the weld deposit because of the lack of preheating and postheating. Rebuilding of exciter shafts should be discontinued, and the support plate of the exciter should be braced to reduce the amount of transmitted vibration. Also, the fillet in the exciter shaft should be carefully machined to provide an adequate radius.

An investigation was conducted to determine what caused a bearing sleeve in a locomotive turbocharger to fail. The sleeve, which is made of nitrided 38CrMoAl steel, fractured at the transition fillet between the cylinder and plate. Visual examination revealed significant wear on the external surface of the cylinder, with multiple origin fatigue fracture appearing to be the dominant fracture mechanism. Metallurgical examination indicated that the nitrided layer was not as deep as it was supposed to be and had worn away on the outer surface of the sleeve, exposing the soft matrix underneath. This led to further wear and an increase in friction between the sleeve and bearing bush. Fatigue crack initiation occurred at the root fillet because of stress concentration and large frictional forces. Insufficient nitriding depth facilitated the propagation of fatigue cracks.

Fractography is the means and methods for characterizing a fractured specimen or component. This includes the examination of fracture-exposed surfaces and the interpretation of the fracture markings as well as the examination and interpretation of crack patterns. This article describes the former of these two parts of fractography. It presents the techniques of fractography and explains fracture markings using glass and ceramic examples. The article also discusses the fracture modes in ceramics and provides examples of fracture origins.

Failure analysis was performed on threaded Ti-6Al-4V fasteners that had fractured in the threads during installation. Scanning electron microscopy (SEM) and optical metallography revealed that the fractures initiated in circumferential shear bands present at the thread roots. The fractures propagated by microvoid coalescence typical of that observed in notched tensile specimen fractures of the same material. For comparison, Ti-6Al-4V fasteners from various commercial sources were tested to failure in uniaxial tension and examined in the SEM. In all cases, the fracture appearances were similar to that exhibited by the fasteners that failed during installation. In addition, results of optical microscopy indicated that the geometry and extent of the shear bands appeared to depend on the fabrication process employed by the individual manufacturers. Causes of shear band formation are discussed along with potential methods to eliminate these microstructural in homogeneities.

This article provides a description of the microscale models and mechanisms for deformation and fracture. Macroscale and microscale appearances of ductile and brittle fracture are discussed for various specimen geometries and loading conditions. The article reviews the general geometric factors and materials aspects that influence the stress-strain behavior and fracture of ductile metals. It highlights fractures arising from manufacturing imperfections and stress raisers. The article presents a root cause failure analysis case history to illustrate some of the fractography concepts.

Two aircraft-engine tailpipes of 19-9 DL stainless steel (AISI type 651) developed cracks along longitudinal gas tungsten arc butt welds after being in service for more than 1000 h. Binocular-microscope examination of the cracks in both tailpipes revealed granular, brittle-appearing surfaces confined to the HAZs of the welds. Microscopic examination of sections transverse to the weld cracks showed severe intergranular corrosion in the HAZ. The fractures appeared to be caused by loss of corrosion resistance due to sensitization, that could have been induced by the temperatures attained during gas tungsten arc welding. Tests demonstrated the presence of sensitization in the HAZ of the gas tungsten arc weld. The aircraft engine tailpipe failures were due to intergranular corrosion in service of the sensitized structure of the HAZs produced during gas tungsten arc welding. All gas tungsten arc welded tailpipes should be postweld annealed by re-solution treatment to redissolve all particles of carbide in the HAZ. Also, it was suggested that resistance seam welding be used, because there would be no corrosion problem with the faster cooling rate characteristic of this technique.

A rocket-motor case made of consumable-electrode vacuum arc remelted D-6ac alloy steel failed during hydrostatic proof-pressure testing. Close visual examination, magnetic-particle inspection, and hardness tests showed cracks that appeared to have occurred after austenitizing but before tempering. Microscopic examinations of ethereal picral etched sections indicated that the cracks appeared before or during the final tempering phase of the heat treatment and that cracking had occurred while the steel was in the as-quenched condition, before its 315 deg C (600 deg F) snap temper. Chemical analysis of the cracked metal showed a slightly higher level of carbon than in the component that did not crack. X-ray diffraction studies of material from the fractured dome showed a very low level of retained austenite, and chemical analysis showed a slightly higher content of carbon in the metal of the three cracked components. Bend tests verified the conclusion that the most likely mechanism of delayed quench cracking was isothermal transformation of retained austenite to martensite under the influence of residual quenching stresses. Recommendations included modifying the quenching portion of the heat-treating cycle and tempering in the salt pot used for quenching, immediately after quenching.

Cracks were discovered in the cast 17-4 PH stainless steel outboard leading edge flap support of an aircraft wing during overhaul inspection. Failure analysis focused on an apparently intergranular area of fracture surface. It was determined that the original mode of crack growth was cleavage, probably caused by cast-in hydrogen. The intergranular appearance resulted from heat treatment of the already cracked part, which caused the formation of grain-boundary “growth figures” on the exposed crack surfaces. It was recommended that the castings be more closely inspected for defects before further processing and that foundry practices be reviewed to correct deficiencies leading to excessive hydrogen absorption during melting and casting.

This article briefly reviews the factors that influence the occurrence of intergranular (IG) fractures. Because the appearance of IG fractures is often very similar, the principal focus is placed on the various metallurgical or environmental factors that cause grain boundaries to become the preferred path of crack growth. The article describes in more detail some typical mechanisms that cause IG fracture. It discusses the causes and effects of IG brittle cracking, dimpled IG fracture, IG fatigue, hydrogen embrittlement, and IG stress-corrosion cracking. The article presents a case history on IG fracture of steam generator tubes, where a lowering of the operating temperature was proposed to reduce failures.

Following a freight train derailment, part of a fractured side frame was retained for study because a portion of its fracture surface exhibited a rock candy appearance and black scale. It was suspected of having failed, thereby precipitating the derailment. Metallography, scanning electron microscopy, EDXA, and x-ray mapping were used to study the steel in the vicinity of this part of the fracture surface. It was found to be contaminated with copper. Debye-Scherrer x-ray diffraction patterns obtained from the scale showed that it consisted of magnetite and hematite. It was concluded that some copper was accidentally left in the mold when the casting was poured. Liquid copper, carrying with it oxygen in solution, penetrated the austenite grain boundaries as the steel cooled. The oxygen reacted with the steel producing a network of scale outlining the austenite grain structure. When the casting fractured as a result of the derailment, the fracture followed the scale in the contaminated region thus creating the “rock candy” fracture.

Silver solid-state bonded components containing uranium failed under zero or low applied load several years after manufacture. The final operation in their manufacture was a proof loading that applied a sustained tensile stress to the bond, which all components passed. The components comprised circular cylinders fabricated by plating a thin layer of silver on each of the contact surfaces (uranium and stainless steel) and pressing the parts together at elevated temperature to solid-state bond the two silver surfaces. The manufacturing process produced a high level of residual stress at the bond. The failures appeared to be predominantly located between the silver layer and the uranium substrate. Normal fracture location of specimens taken from similar components was at the silver/silver bond interface. Laboratory testing revealed that the uranium/silver joint was susceptible to premature failure by stress-corrosion cracking under sustained loading if the atmosphere was saturated with water vapor.

SAE grade 5 U-bolts were used to fasten auxiliary dual wheels to the axles on a farm tractor. Under typical farm usage, the bolts are expected to have infinite life. However, several U-bolts made of 29 mm diam rod broke after less than 100 h of service. The bolt legs in which the failures occurred were all in the same position relative to the direction of wheel rotation. Visual examination showed the break was a fairly flat transverse fracture in the threaded section between the washer and the nut. The appearance of the fracture surfaces was characteristic of failure by low-cycle fatigue, with a smooth matte fatigue failure region showing beach marks and generally extending over about 40 to 60% of the fracture surface, which indicated severe overload. The point of initiation of fatigue was at the root of the last thread at the edge of the nut on the side toward this washer. The U-bolts fractured in fatigue because the bolt material had poor hardenability relative to the diam of the bolts. The bolt material was changed from 1045 steel to 1527 steel, a warm-finished low-alloy steel. The diameter of the bolts was reduced to 27.2 mm and the threads were rolled rather than cut.

A forged aluminum alloy 2014-T6 catapult-hook attachment fitting (anodized by the chromic acid process to protect it from corrosion) from a naval aircraft broke in service. Spectrographic analysis, visual examination, microscopic examination, and tensile analysis showed minute cracks on the inside surface of a bearing hole, and small areas of pitting corrosion were visible on the exterior surface of the fitting. The analysis also revealed a small number of rosettes, suggestive of eutectic melting, in an otherwise normal structure. These examinations and analyses support the conclusion that the presence of chromic acid stain on the fracture surface proved that the forging had cracked before anodizing. This suggest that the crack initiated during straightening, either after machining or after heat treatment. The structure and composition of the alloy appear to have been acceptable. Ductility was acceptable so rosettes found in the microstructure are believed to have been nondamaging. Had they contributed to the failure, the ductility would have been very low. The recommendations included inspection for cracks and revising the manufacturing process to include a fluorescent liquid-penetrant inspection before anodizing, because chromic acid destroys the penetrant. This inspection would reduce the possibility of cracked parts being used in service.

An aluminum alloy propeller blade that had been cold straightened to correct deformation incurred in service fractured soon after being returned to service. Visual examination revealed that crack initiation occurred at the top surface in an area containing numerous surface pits. Macroscopic appearance of the surface was of brittle fracture. X-ray stress analysis did not detect any residual stress in the top surface of the propeller blade adjacent to the fracture. However, a spanwise tensile stress of approximately 51 MPa (7.4 ksi) was indicated in the same surface of the unfailed mating blade at the location of the initial bend. Evidence found supports the conclusions that the residual stress probably originated with straightening, and the apparent absence of stress in the fractured blade was the result of relaxation through fracture. Because no prior crack damage could be attributed to the initial deformation or to straightening, rapid fracture may have been induced by residual stresses contributing to the normal spectrum of cyclic stresses. Recommendations included stress-relief annealing after cold straightening, refinishing of the surface, thus reducing fracturing of propeller blades that were cold straightened to correct deformation experienced in service.

During the lifting of a piece of machinery by means of an overhead travelling crane the hook fractured suddenly. The load was attached to the hook by means of fiber rope slings and rupture occurred in a plane which appeared to coincide with the sling loop nearest to the back of the hook. The rated capacity of the crane was 15 tons. At the time of the mishap it was being used to lift one end of a hydraulic cylinder with a total weight of about 27 tons. Fracture was of the cleavage type throughout. There was no evidence of any prior deformation of the material in the vicinity, nor was there any indication of a pre-existing crack or major discontinuity at the point of origin. A sulfur print suggested the hook had been forged from a billet cogged down from an ingot of semi-killed steel. Failure of this hook was attributed to strain-age embrittlement of the material at the surface of the intrados.