This article provides an overview of fractography and explains how it is used in failure analysis. It reviews the basic types of fracture processes, namely, ductile, brittle, fatigue, and creep, principally in terms of fracture appearances, such as microstructure. The article also describes the general features of fatigue fractures in terms of crack initiation and fatigue crack propagation.

Engineering component and structure failures manifest through many mechanisms but are most often associated with fracture in one or more forms. This article introduces the subject of fractography and aspects of how it is used in failure analysis. The basic types of fracture processes (ductile, brittle, fatigue, and creep) are described briefly, principally in terms of fracture appearances. A description of the surface, structure, and behavior of each fracture process is also included. The article provides a framework from which a prospective analyst can begin to study the fracture of a component of interest in a failure investigation. Details on the mechanisms of deformation, brittle transgranular fracture, intergranular fracture, fatigue fracture, and environmentally affected fracture are also provided.

This article briefly reviews the various metallurgical or environmental factors that cause a weakening of the grain boundaries and, in turn, influence the occurrence of intergranular (IG) fractures. It discusses the mechanisms of IG fractures, including the dimpled IG fracture, the IG brittle fracture, and the IG fatigue fracture. The article describes some typical embrittlement mechanisms that cause the IG fracture of steels.

This article describes the underlying fundamentals, applications, the relevance and necessity of performing proper stress analysis in conducting a failure analysis. It presents an introduction to the stress analysis of bodies containing crack-like imperfections and the topic of fracture mechanics. The fracture mechanics approach is an important part of stress analysis at the tips of sharp cracks or discontinuities. The article reviews fracture mechanics concepts, including linear elastic fracture mechanics, elastic-plastic fracture mechanics, and subcritical fracture mechanics. It also provides information on the applications of fracture mechanics in failure analysis.

This article reviews the mechanical behavior and fracture characteristics that discriminate structural polymers from metals. It provides information on deformation, fracture, and crack propagation as well as the fractography involving the examination and interpretation of fracture surfaces, to determine the cause of failure. The fracture modes such as ductile fractures and brittle fractures are reviewed. The article also presents a detailed account of various fracture surface features. It concludes with several cases of field failure in various polymers that illustrate the applicability of available analytical tools in conjunction with an understanding of failure mechanisms.

Fractography is the means and methods for characterizing a fractured specimen or component. This includes the examination of fracture-exposed surfaces and the interpretation of the fracture markings as well as the examination and interpretation of crack patterns. This article describes the former of these two parts of fractography. It presents the techniques of fractography and explains fracture markings using glass and ceramic examples. The article also discusses the fracture modes in ceramics and provides examples of fracture origins.

This article provides a description of the microscale models and mechanisms for deformation and fracture. Macroscale and microscale appearances of ductile and brittle fracture are discussed for various specimen geometries and loading conditions. The article reviews the general geometric factors and materials aspects that influence the stress-strain behavior and fracture of ductile metals. It highlights fractures arising from manufacturing imperfections and stress raisers. The article presents a root cause failure analysis case history to illustrate some of the fractography concepts.

This article commences with a summary of fatigue processes and mechanisms. It focuses on fractography of fatigue. Characteristic fatigue fracture features that can be discerned visually or under low magnification are described. Typical microscopic features observed on structural metals are presented subsequently, followed by a brief discussion of fatigue in nonmetals. The article reviews the various macroscopic and microscopic features to characterize the history and growth rate of fatigue in metals. It concludes with a description of fatigue of polymers and composites.

An air blower in an electric power plant failed unexpectedly when a roller bearing in the drive motor fractured along its outer ring. Both rings, as well as the 18 rolling elements, were made from GCr15 bearing steel. The bearing also included a machined brass (MA/C3) cage and was packed with molybdenum disulfide (MoS 2 ) lithium grease. Metallurgical structures and chemical compositions of the bearing’s matrix materials were inspected using a microscope and photoelectric direct reading spectrometer. SEM/EDS was used to examine the local morphology and composition of fracture and contact surfaces. Chemical and thermal properties of the bearing grease were also examined. The investigation revealed that the failure was caused by wear due to dry friction and impact, both of which worsened as a result of high-temperature degradation of the bearing grease. Fatigue cracks initiated in the corners of the outer ring and grew large enough for a fracture to occur.

A felt guide roll fractured in-service on a paper manufacturing machine, damaging the belt as well as multiple dryer rolls, nearby felt guide rolls, and the frame of the machine. The investigation included visual and stereoscopic examination, chemical and microstructural analysis, microhardness and tensile testing, stress calculations, and vibration measurements. Based on the results, the roll fracture was attributed to high-cycle fatigue associated with a plug weld over one of the five threaded fasteners added to secure a balance weight inside the roll. The balance weight was installed to compensate for variations in wall thickness (i.e., weight distribution) of the pipe product used to make the roll. According to the investigation, resonance and vibration, which were initially considered, did not cause the failure.

An investigation was conducted to determine what caused a bearing sleeve in a locomotive turbocharger to fail. The sleeve, which is made of nitrided 38CrMoAl steel, fractured at the transition fillet between the cylinder and plate. Visual examination revealed significant wear on the external surface of the cylinder, with multiple origin fatigue fracture appearing to be the dominant fracture mechanism. Metallurgical examination indicated that the nitrided layer was not as deep as it was supposed to be and had worn away on the outer surface of the sleeve, exposing the soft matrix underneath. This led to further wear and an increase in friction between the sleeve and bearing bush. Fatigue crack initiation occurred at the root fillet because of stress concentration and large frictional forces. Insufficient nitriding depth facilitated the propagation of fatigue cracks.

The A2 tool steel mandrel, part of a rolling tool used for mechanically joining two tubes was fractured after making five rolled joints. A 6.4 mm diam hole was drilled by EDM through the square end of the hardened mandrel due to difficulty was experienced in withdrawing the tool. The fracture progressed into the threaded section and formed a pyramid-shape fragment after it was initiated at approximately 45 deg through the hole in the square end. An irregular zone of untempered martensite with cracks radiating from the surface of the hole (result of melting around hole) was revealed by metallographic examination. A microstructure of fine tempered martensite containing some carbide particles was exhibited by the core material away from the hole. Brittle fracture characteristics with beach marks were exhibited by the fracture surfaces which is characteristic of a torsional fatigue fracture. As a corrective measure, the hole through the square end of the mandrel was incorporated into the design of the tool and was drilled and reamed before heat treatment and specified hardness of the threaded portion and square end of the mandrel was reduced.

The specially designed sand-cast low-alloy steel jaws that were implemented to stretch the wire used in prestressed concrete beams fractured. The fractures were found to be macroscale brittle and exhibited very little evidence of deformation. The surface of the jaws was disclosed by metallographic examination to be case carburized. The case was found to be martensite with small spheroidal carbides while the core consisted of martensite plus some ferrite. The fracture was revealed to be related to shrinkage porosity. Tempering was revealed to be probably limited to about 150 deg C by the hardness values (close to the maximum hardness values attainable) for the core. It was interpreted that the low tempering temperature used may have contributed to the brittleness. The procedures used for casting the jaws were recommended to be revised to eliminate the internal shrinkage porosity. Tempering at a slightly higher temperature to reduce surface and core hardness was recommended.

A cross-recessed die of D5 tool steel fractured in service. The die face was found to be subjected to shear and tensile stresses as a result of the forging pressures from the material being worked. The presence of numerous slag stringers was revealed by microscopic examination of an unetched longitudinal section taken through the die. The pattern was microscopically revealed after etching with 5 % nital to be due to severe chemical segregation or banding. Considerable variation in the hardness, corresponding to the banded and non-banded regions across the face of the specimen was observed. The fracture was found to have originated near the high-stress region of the die face examination of the fracture surface. Failure of the die was concluded to have originated in an area of abnormally high hardness which is prone to microcracking during heat treatment for this grade of tool steel

To permit bolting of a 90 lb/yd. flat-bottomed rail to a steel structure, rectangular slots 2 in. wide x 1 in. deep were flame-cut in the base of the rail at 2 ft intervals to suit existing bolt holes. During subsequent handling, one of the rails (which were about 25 ft long) was dropped from a height of approximately 6 ft on to a concrete floor and it fractured into 11 pieces, each break occurring at a slot. The sample piece submitted for examination showed a wholly brittle fracture at each end, the fractures having originated at the sharp corners of the slots. During flame-cutting, a narrow band of material on each side of the cut was raised above the hardening temperature. When the torch had passed the rate of abstraction of heat from this zone by conduction into the cold mass of the rail was sufficiently rapid to amount to a quench and thus cause local hardening. The steel in the regions of the slots possessed little capacity for deformation, and fracturing of the martensitic layer, under cooling or impact stresses, would be likely to occur. The slots should have been cut mechanically.

A railway tank car developed a fracture in the region of the sill and shell attachment during operation at -34 deg C (-30 deg F). On either side of the sill-support member, cracking initiated at the weld between a 6.4 mm thick frontal cover plate and a 1.6 mm thick side support plate. The crack then propagated in a brittle manner upward through the side plate, through the welds attaching the side plate to a 25 mm (1 in.) thick shell plate (ASTM A212, grade B steel), and continued for several millimeters in the shell plate before terminating. Other plates involved were not positively identified but were generally classified as semi-killed carbon steels. Investigation (visual inspection, hardness testing, chemical analysis, Charpy V-notch testing, and drop-weight testing) supported the conclusions that the fracture was initiated by weld imperfections and propagated in a brittle manner as a result of service stresses acting on the plate having low toughness at the low service temperatures encountered. Recommendations included that the specifications for the steel plates be modified to include a toughness requirement and that improved welding and inspection practices be performed to reduce the incidence of weld imperfections.

Within about one month, several knuckle pins (AMS 6470 steel failed, and required to have a minimum case hardness of 92 h15N, a case depth of 0.4 to 0.5 mm (0.017 to 0.022 in.), and a core hardness of 285 to 341 HRB) used in engines failed over a range of 218 to 463 h in operation. Visual examination revealed beach marks typical of fatigue cracks that had nucleated at the base of the longitudinal oil hole. Micrographs of sections revealed a remelt zone and an area of untempered martensite within the region of the cracks. However, review of inspection procedures disclosed the pins had been magnetic-particle inspected by inserting a probe into the longitudinal hole. Evidence found supports the conclusions that the knuckle pins failed by fatigue fracture. The circular cracks at the longitudinal holes were the result of improper technique in magnetic-particle inspection. Thermal transformation of the metal also causes a stress concentration that may lead to fatigue failure. Recommendations included insulating the conductor to prevent arc burning at the base of the longitudinal oil hole. Also, a borescope or metal monitor could be used to inspect the hole for evidence of arc burning from magnetic-particle inspection.

Several of the welds in a hoist carriage tram-rail assembly fabricated by shielded metal arc welding the leg of a large T-section 1020 steel beam to the leg of a smaller T-section 1050 steel rail failed in one portion of the assembly. Four weld cracks and several indefinite indications were found by magnetic-particle inspection. The cracks were revealed by metallographic examination to have originated in the HAZs in the rail section. Cracks in welds and in HAZs resulting from arcing the electrode adjacent to the weld and weld spatter were also revealed. The tram-rail assembly was concluded to have failed by fatigue cracking in HAZs. The fatigue cracking was initiated and propagated by vibration of the tram rail by movement of the hoist carriage on the rail. As a corrective measure, welding procedures were improved and the replacement rail assemblies were preheated and postheated.

On 15 March 2000, a National Railroad Passenger Corporation (Amtrak) train traveling from Chicago to Los Angeles derailed in Carbondale, KS. After the initial on-scene investigation, 12 pieces of rail were sent to the materials laboratory for examination. Ten of them were from the point of derailment (POD). A vertical crack was observed in the head of the rail (vertical split head). The crack was at least 233 in. (591 cm) long, continuing through the entire lengths of most pieces recovered from the POD. The vertical fracture surface had features consistent with overstress fracture with short-term exposure to an oxygen-rich environment. Fracture features emanated from longitudinally-aligned inclusions rich in aluminum.

Following a freight train derailment, part of a fractured side frame was retained for study because a portion of its fracture surface exhibited a rock candy appearance and black scale. It was suspected of having failed, thereby precipitating the derailment. Metallography, scanning electron microscopy, EDXA, and x-ray mapping were used to study the steel in the vicinity of this part of the fracture surface. It was found to be contaminated with copper. Debye-Scherrer x-ray diffraction patterns obtained from the scale showed that it consisted of magnetite and hematite. It was concluded that some copper was accidentally left in the mold when the casting was poured. Liquid copper, carrying with it oxygen in solution, penetrated the austenite grain boundaries as the steel cooled. The oxygen reacted with the steel producing a network of scale outlining the austenite grain structure. When the casting fractured as a result of the derailment, the fracture followed the scale in the contaminated region thus creating the “rock candy” fracture.