This article provides an overview of fractography and explains how it is used in failure analysis. It reviews the basic types of fracture processes, namely, ductile, brittle, fatigue, and creep, principally in terms of fracture appearances, such as microstructure. The article also describes the general features of fatigue fractures in terms of crack initiation and fatigue crack propagation.

Engineering component and structure failures manifest through many mechanisms but are most often associated with fracture in one or more forms. This article introduces the subject of fractography and aspects of how it is used in failure analysis. The basic types of fracture processes (ductile, brittle, fatigue, and creep) are described briefly, principally in terms of fracture appearances. A description of the surface, structure, and behavior of each fracture process is also included. The article provides a framework from which a prospective analyst can begin to study the fracture of a component of interest in a failure investigation. Details on the mechanisms of deformation, brittle transgranular fracture, intergranular fracture, fatigue fracture, and environmentally affected fracture are also provided.

This article briefly reviews the various metallurgical or environmental factors that cause a weakening of the grain boundaries and, in turn, influence the occurrence of intergranular (IG) fractures. It discusses the mechanisms of IG fractures, including the dimpled IG fracture, the IG brittle fracture, and the IG fatigue fracture. The article describes some typical embrittlement mechanisms that cause the IG fracture of steels.

This article describes the underlying fundamentals, applications, the relevance and necessity of performing proper stress analysis in conducting a failure analysis. It presents an introduction to the stress analysis of bodies containing crack-like imperfections and the topic of fracture mechanics. The fracture mechanics approach is an important part of stress analysis at the tips of sharp cracks or discontinuities. The article reviews fracture mechanics concepts, including linear elastic fracture mechanics, elastic-plastic fracture mechanics, and subcritical fracture mechanics. It also provides information on the applications of fracture mechanics in failure analysis.

This article reviews the mechanical behavior and fracture characteristics that discriminate structural polymers from metals. It provides information on deformation, fracture, and crack propagation as well as the fractography involving the examination and interpretation of fracture surfaces, to determine the cause of failure. The fracture modes such as ductile fractures and brittle fractures are reviewed. The article also presents a detailed account of various fracture surface features. It concludes with several cases of field failure in various polymers that illustrate the applicability of available analytical tools in conjunction with an understanding of failure mechanisms.

Fractography is the means and methods for characterizing a fractured specimen or component. This includes the examination of fracture-exposed surfaces and the interpretation of the fracture markings as well as the examination and interpretation of crack patterns. This article describes the former of these two parts of fractography. It presents the techniques of fractography and explains fracture markings using glass and ceramic examples. The article also discusses the fracture modes in ceramics and provides examples of fracture origins.

This article provides a description of the microscale models and mechanisms for deformation and fracture. Macroscale and microscale appearances of ductile and brittle fracture are discussed for various specimen geometries and loading conditions. The article reviews the general geometric factors and materials aspects that influence the stress-strain behavior and fracture of ductile metals. It highlights fractures arising from manufacturing imperfections and stress raisers. The article presents a root cause failure analysis case history to illustrate some of the fractography concepts.

This article commences with a summary of fatigue processes and mechanisms. It focuses on fractography of fatigue. Characteristic fatigue fracture features that can be discerned visually or under low magnification are described. Typical microscopic features observed on structural metals are presented subsequently, followed by a brief discussion of fatigue in nonmetals. The article reviews the various macroscopic and microscopic features to characterize the history and growth rate of fatigue in metals. It concludes with a description of fatigue of polymers and composites.

Following a fracture mechanics “fitness-for-purpose” analysis of petroleum industry cold service pressure vessels, using the British Standard PD 6493, it was realized that an analogous approach could be used for the failure analysis of a similar pressure vessel dome which had failed in service some years previously. The failed pressure vessel, with a diam of 2.5 m and several meters tall, had been made of 12 mm thick IZETT steel plate of the same type and heat treatment as used in the earlier fitness-for-purpose already measured. Examination of the fracture surfaces suggested, from fatigue striations manifested by SEM, that the vessel was subject to significant fatigue cracking, which was probably corrosion assisted. From COD measurements at the operating temperature of -130 deg C (-202 deg F), and a finite stress analysis, a fracture mechanics evaluation using BS PD6493 yielded realistic critical flaw sizes (in the range 51 to 150 mm). These sizes were consistent with the limited fracture surface observations and such flaws could well have been present in the vessel dome prior to catastrophic failure. For similar pressure vessels, an inspection program based on a leak-before-break philosophy was consequently regarded as acceptable.

U-shaped leaf springs, intended to serve as spacers between oil tank floats and the inner walls of the containers, broke while being fitted, or after a short time in use, in the bend of the U. The springs were made of tempered strip steel of type C 88 with 0.84 % C, bent at room temperature, and electroplated with cadmium for protection against corrosion. Each fracture showed seven or eight kidney-shaped cracks. At the origins of these cracks on the concave inner surface of the springs, crater-like depressions and beads of melted and resolidified material were found. Fracture of the springs was caused by stress cracks as a consequence of local hardening. The hardening caused by melting and resolidification, and therefore the cracks in the springs, was the result of a faulty procedure during cadmium electroplating.

A natural gas pipeline explosion and subsequent fire significantly altered the pipeline steel microstructure, obscuring in part the primary cause of failure, namely, coating breakdown at a local hard spot in the steel. Chemical analysis was made on pieces cut from the portion of the pipe that did not fracture during the explosion and from piece 5-1 which contained the fracture origin site. Both pieces were found to have 0.30% carbon and 1.2% Mn with sulfur and phosphorus impurities acceptably low. Fracture mechanics analysis used in conjunction with fractographic results confirmed the existence of a very hard spot in the steel prior to the explosion, which was softened significantly in the ensuing fire. This finding allowed the micromechanism leading to fracture to be identified as hydrogen embrittlement resulting from cathodic charging.

A series of poppet-valve stems fabricated from 17-4 PH (AISI type 630) stainless steel failed prematurely in service during the development of a large combustion assembly. The poppet valves were part of a scavenging system that evacuated the assembly after each combustion cycle. The function of the valve is to open and close a port; thus, the valve is subjected to both impact and tensile loading. Analysis (visual inspection, hardness testing, and stress analysis) supported the conclusions that the valve stems were impact loaded to stresses in excess of their yield strength. That they failed in the threaded portion also suggests a stress-concentration effect. Recommendations included changing the material spec to a higher-strength material with greater impact strength. In this case, it was recommended that the stems, despite any possible design changes, be manufactured from an alloy such as PH 13-8Mo, which can be processed to a yield strength of 1379 MPa (200 ksi), with impact energies of the order of 81 J (60 ft·lbf) at room temperature.

A structure had been undergoing fatigue testing for several months when a post-like member heat treated to a tensile strength of 1517 to 1655 MPa (220 to 240 ksi) ruptured. The fracture occurred in the fillet of the post that contacted the edge of a carry-through box bolted to the member. At failure, the part was receiving a second set of loads up to 103.6% of design load. Visual investigations showed rubbing and galling of the fillet. Microscopic and metallographic examination revealed beach marks on the fracture surface and evidence of cold work and secondary cracking in the rubbed and galled area. Electron fractography confirmed that cracking had initiated at a region of tearing and that the cracks had propagated by fatigue. Mechanical properties of all specimens exceeded the minimum values specified for the post. This evidence supports the conclusion that fatigue was the primary cause of failure. Rubbing of the faying surfaces worked the interference area on the post until small tears developed. These small tears became stress-concentration points that nucleated fatigue cracks. Recommendations included rounding the edge of the box in the area of contact with the post to ensure a tangency fit.

A pushrod made by inertia welding two rough bored pieces of bar stock installed in a mud pump fractured after two weeks in service. The flange portion was made of 94B17 steel, and the shaft was made of 8620 steel. It was disclosed by visual examination that the fracture occurred in the shaft portion at the intersection of a 1.3 cm thick wall and a tapered surface at the bottom of the hole. The fatigue crack was influenced by one-way bending stresses initiated at the inner surface and progressed around the entire inner circumference. A heavily decarburized layer was detected on the inner surface of the flange portion and sharp corner was found at the intersection of the sidewall and bottom of the hole. It was concluded that the stress raiser due to the abrupt section change was accentuated by decarburized layer. As a corrective measure, the design of the pushrod was changed to a one-piece forging and circulation of atmosphere during heat treatment was permitted through a hole drilled in the flange end of the rod to avoid decarburization.

The gun mount used in two types of self-propelled artillery consists of an oil-filled recoil cylinder and a sand-cast (MIL-I-11466, grade D7003) ductile-iron piston that connects to the gun tube through a threaded rod. The piston contains several orifices through which oil is forced as a means of absorbing recoil energy. During operation, the piston is stressed in tension, pulled by oil pressure on one end and the opposing force of the gun tube on the other. The casting specification stipulated that the graphite be substantially nodular and that metallographic test results be provided for each lot. Investigation (visual inspection, fatigue testing, 0.25x/0.35x/50x magnifications, 2% nital etched 60x/65x magnifications, and SEM views) showed that most of the service fractures occurred in pistons containing vermicular graphite. Recommendations included ultrasonic testing of pistons already in the field to identify and reject those containing vermicular graphite. In addition, metallographic control standards were suggested for future production lots.

Plunger shafts machined from 4150 steel bar stock were involved in a series of fatigue failures. The fractures consistently occurred at two locations on the shafts: the shaft fillet and either side of a machined notch. The material specification for the shafts required 41xx series steel with a carbon content of 0.38 to 0.53%, a hardness of 35 to 40 HRC for the shaft, and a hardness of 50 to 55 HRC for the notch (which was case hardened). Analysis (visual inspection, chemical analysis, hardness testing, and magnetic particle inspection) supported the conclusions that all the fractures were fatigue-induced failures due to sharp radii in the fillets. The stress-concentrating effects of the fillets caused fatigue cracks to initiate and grow under cyclic loading until the crack depth was critical, causing the shaft to fail and rendering the assembly inoperative. Recommendations included increasing the radii of the notch and shaft fillets. If fatigue cracking had continued to be a problem with this component, shot peening of the subject radii would be appropriate. This process produces residual compressive stresses in the surface of the part, thereby retarding initiation of fatigue cracks.

After only a short time in service, oil-fired orchard heaters made of galvanized low-carbon steel pipe, 0.5 mm (0.020 in.) in thickness, became sensitive to impact, particularly during handling and storage. Most failures occurred in an area of the heater shell that normally reached the highest temperature in service. A 400x etched micrograph showed a brittle and somewhat porous metallic layer about 0.025 mm (0.001 in.) thick on both surfaces of the sheet. Next to this was an apparently single-phase region nearly 0.05 mm (0.002 in.) in thickness. The examination supported the conclusion that prolonged heating of the galvanized steel heater shells caused the zinc-rich surface to become alloyed with iron and reduce the number of layers. Also, heating caused zinc to diffuse along grain boundaries toward the center of the sheet. Zinc in the grain boundaries reacted with iron to form the brittle intergranular phase, resulting in failure by brittle fracture at low impact loads during handling and storage. Recommendation included manufacture of the pipe with aluminized instead of galvanized steel sheet for the combustion chamber.

The fan drive support shaft, specified to be made of cold-drawn 1040 to 1045 steel, fractured after 2240 miles of service. It was revealed by visual examination of the shaft that the fracture had initiated near the fillet at an abrupt change in shaft diameter. The cracks originated at two locations approximately 180 deg apart on the outer surface of the shaft and propagated toward the center. Features typical of reversed-bending fatigue were exhibited by the fracture. A tensile specimen was machined from the center of the shaft and it indicated much lower yield strength (369 MPa) than specified. It was disclosed by metallographic examination that the microstructure was predominantly equiaxed ferrite and pearlite which indicated that the material was in either the hot-worked or normalized condition. An improvement of fatigue strength of the shaft by the development of a quenched-and-tempered microstructure was recommended.

Stainless steel liners (AISI type 321) used in bellows-type expansion joints in a duct assembly installed in a low-pressure nitrogen gas system failed in service. The duct assembly consisted of two expansion joints connected by a 32 cm (12 in.) OD pipe of ASTM A106 grade B steel. Elbows made of ASTM A234 grade B steel were attached to each end of the assembly, 180 deg apart. A 1.3 mm (0.050 in.) thick liner with an OD of 29 cm (11 in.) was welded inside each joint. The upstream ends were stable, but the downstream ends of the liners remained free, allowing the components to move with the expansion and contraction of the bellows. Investigation (visual inspection, hardness testing, and 30x fractographs) supported the conclusion that the liners failed in fatigue initiated at the intersection of the longitudinal weld forming the liner and the circumferential weld by which it attached to the bellows assembly. Recommendations included increasing the thickness of the liners from 1.3 to 1.9 mm (0.050 to 0.075 in.) in order to damp some of the stress-producing vibrations.

An LNG tanker experienced a fracture of the solid tail shaft, which is a section of the main drive shaft. The tail shaft was made of a forged low-carbon steel. In spite of two ultrasonic inspections, a large defect the size of a football in the center of the shaft was missed. During heat treating following forging, it was surmised that the defect led to the propagation of an internal brittle crack, or clink. A fatigue crack propagated from this origin to the outer surface of the shaft after about a year of service. Finally a last ligament of a few square inches held the shaft together and broke, leading to the separation of the shaft. The cause of failure was fatigue crack initiation and crack growth under reverse bending cyclic stresses. There was no indication that misalignment existed because there was no indication of fretting at the bolt holes in the flange at the end of the shaft. In the case of this shaft, a solution would have been to machine the core of the shaft to remove the brittle material or to use a tubular shaft.