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forged nitrided steel
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Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001761
EISBN: 978-1-62708-241-9
... Abstract An investigation of a damaged crankshaft from a horizontal, six-cylinder, in-line diesel engine of a public bus was conducted after several failure cases were reported by the bus company. All crankshafts were made from forged and nitrided steel. Each crankshaft was sent for grinding...
Abstract
An investigation of a damaged crankshaft from a horizontal, six-cylinder, in-line diesel engine of a public bus was conducted after several failure cases were reported by the bus company. All crankshafts were made from forged and nitrided steel. Each crankshaft was sent for grinding, after a life of approximately 300,000 km of service, as requested by the engine manufacturer. After grinding and assembling in the engine, some crankshafts lasted barely 15,000 km before serious fractures took place. Few other crankshafts demonstrated higher lives. Several vital components were damaged as a result of crankshaft failures. It was then decided to send the crankshafts for laboratory investigation to determine the cause of failure. The depth of the nitrided layer near fracture locations in the crankshaft, particularly at the fillet region where cracks were initiated, was determined by scanning electron microscope (SEM) equipped with electron-dispersive X-ray analysis (EDAX). Microhardness gradient through the nitrided layer close to fracture, surface hardness, and macrohardness at the journals were all measured. Fractographic analysis indicated that fatigue was the dominant mechanism of failure of the crankshaft. The partial absence of the nitrided layer in the fillet region, due to over-grinding, caused a decrease in the fatigue strength which, in turn, led to crack initiation and propagation, and eventually premature fracture. Signs of crankshaft misalignment during installation were also suspected as a possible cause of failure. In order to prevent fillet fatigue failure, final grinding should be done carefully and the grinding amount must be controlled to avoid substantial removal of the nitrided layer. Crankshaft alignment during assembly and proper bearing selection should be done carefully.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001252
EISBN: 978-1-62708-235-8
... Abstract An octagonal steel ingot weighing 13 tons made of manganese-molybdenum steel developed gaping cross-cracks on all eight sides in the forging press during initial pressure application. It was reported that the steel had been melted in a basic 12-ton arc furnace, oxygenated, furnished...
Abstract
An octagonal steel ingot weighing 13 tons made of manganese-molybdenum steel developed gaping cross-cracks on all eight sides in the forging press during initial pressure application. It was reported that the steel had been melted in a basic 12-ton arc furnace, oxygenated, furnished with 42 kg of 75% ferrosilicon and 12 kg aluminum additions, alloyed with 160 kg of 80% ferromanganese, and finally deoxidized in the ladle with 42 kg calcium silicon. For metallographic examination a plate approximately 100 mm thick was cut parallel to one of the eight planes. Platelet-like particles could be discerned on the conchoidal fracture planes with the SEM. The precipitates proved to be thin and partially transparent platelets of a hexagonal crystal lattice whose parameters resemble those of AIN. The precipitates were at least in part still undissolved in spite of the long holding period at high initial forging temperature. Another block melted under the same conditions and immediately after the defective one, was forged into a gear ring without any trouble. This ring was free of grain boundary precipitates, but it contained only 0.012 % AI and 0.0102 % N.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001256
EISBN: 978-1-62708-218-1
... Abstract There was a large incidence of surface defects on the crank pins and journals and other areas of crank shafts of a high power automotive engine. The steel used was a Cr-Mo type of nitriding steel. Metallographic observations conclusively proved that the defective areas were entrapment...
Abstract
There was a large incidence of surface defects on the crank pins and journals and other areas of crank shafts of a high power automotive engine. The steel used was a Cr-Mo type of nitriding steel. Metallographic observations conclusively proved that the defective areas were entrapment of foreign bodies, resulting from steel making/deoxidizing/teeming stages. The occasionally globular nature of the foreign particles suggested these were formed at the liquid condition of the steel. The ratio of Mn-Si as seen on electron probe microanalysis also suggested the globules high in Mn content might have resulted in deoxidizing stage. Particularly the absence of Fe in some areas in the inclusion was indicative of precipitation deoxidation by ferromanganese/ferrosilicon. The defects apparently did not have time to coalesce and rise up to the top.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006816
EISBN: 978-1-62708-329-4
... that cause a part to fail during heat treatment. The article discusses the problems associated with heating and furnaces, quenching media, quenching stresses, hardenability, tempering, carburizing, carbonitriding, and nitriding as well as potential stainless steel problems and problems associated...
Abstract
This article introduces some of the general sources of heat treating problems with particular emphasis on problems caused by the actual heat treating process and the significant thermal and transformation stresses within a heat treated part. It addresses the design and material factors that cause a part to fail during heat treatment. The article discusses the problems associated with heating and furnaces, quenching media, quenching stresses, hardenability, tempering, carburizing, carbonitriding, and nitriding as well as potential stainless steel problems and problems associated with nonferrous heat treatments. The processes involved in cold working of certain ferrous and nonferrous alloys are also covered.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001615
EISBN: 978-1-62708-235-8
... Abstract Carbon steel axle forgings were rejected due to internal cracks observed during final machining. To determine the cause of the cracks, the preforms of the forging were analyzed in detail at each stage of the forging. The analysis revealed a large central burst in the intermediate stage...
Abstract
Carbon steel axle forgings were rejected due to internal cracks observed during final machining. To determine the cause of the cracks, the preforms of the forging were analyzed in detail at each stage of the forging. The analysis revealed a large central burst in the intermediate stage of the forging preform, which subsequently increased in the final stage. A high upset strain during forging, especially in the final stage, accentuated the center burst by high lateral flow of the metal. It was concluded that the center burst of the axle forging resulted from a high concentration of nonmetallic inclusions in the central portion of the raw bar stock rather than the usual problem of improper forging temperature. Strict control over the inclusion content in the raw material by changing the vendor eliminated the problem.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0001814
EISBN: 978-1-62708-180-1
... martensite and unstable retained austenite, often fail by quench cracking. Figure 16(a) shows a 44-cm (17 1 2 -in.) OD × 33-cm (13-in.) ID × 5-cm (2-in.) thick ring forging made of AISI O1 tool steel that cracked during quenching. Temper color was present on the crack surface. The interior...
Abstract
This article describes the characteristics of tools and dies and the causes of their failures. It discusses the failure mechanisms in tool and die materials that are important to nearly all manufacturing processes, but is primarily devoted to failures of tool steels used in cold-working and hot-working applications. It reviews problems introduced during mechanical design, materials selection, machining, heat treating, finish grinding, and tool and die operation. The brittle fracture of rehardened high-speed steels is also considered. Finally, failures due to seams or laps, unconsolidated interiors, and carbide segregation and poor carbide morphology are reviewed with illustrations.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006818
EISBN: 978-1-62708-329-4
... in.) thick ring forging made of AISI O1 tool steel that cracked during quenching. Temper color was present on the crack surface. The interior microstructure ( Fig. 16b ) revealed an overaustenitized condition, coarse plate martensite, and retained austenite (white). The hardness was 61 to 62 HRC. A section...
Abstract
This article discusses failure mechanisms in tool and die materials that are very important to nearly all manufacturing processes. It is primarily devoted to failures of tool steels used in cold working and hot working applications. The processes involved in the analysis of tool and die failures are also covered. In addition, the article focuses on a number of factors that are responsible for tool and die failures, including mechanical design, grade selection, steel quality, machining processes, heat treatment operation, and tool and die setup.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001752
EISBN: 978-1-62708-241-9
... Abstract Results of failure analyses of two aircraft crankshafts are described. These crankshafts were forged from AMS 6414 (similar composition to AISI 4340) vacuum arc remelted steels with sulfur contents of 0.003% (low sulfur) and 0.0005% (ultra-low sulfur). A grain boundary sulfide...
Abstract
Results of failure analyses of two aircraft crankshafts are described. These crankshafts were forged from AMS 6414 (similar composition to AISI 4340) vacuum arc remelted steels with sulfur contents of 0.003% (low sulfur) and 0.0005% (ultra-low sulfur). A grain boundary sulfide precipitate was caused by overheat of the low sulfur steel, and an incipient melting of grain boundary junctions was caused by overheat of the ultra-low sulfur steel. The precipitates and incipient melting in these two failed crankshafts were observed during the examination. As expected, impact fractures from the low sulfur steel crankshaft contained planar dimpled facets along separated grain boundaries with a small spherical manganese sulfide precipitates within each dimple. In contrast, planar dimpled facets along separated grain boundaries of impact fractures from the ultra-low sulfur crankshaft steel contained a majority of small spherical particles consisting of nitrogen, boron, iron, carbon, and a small amount of oxygen. Some other dimples contained manganese sulfide precipitates. Fatigue samples machined from the ultra-low sulfur steel crankshaft failed internally at planar grain boundary facets. Some of the facets were covered with nitrogen, boron, iron, and carbon film, while other facets were relatively free of such coverage. Results of experimental forging studies defined the times and temperatures required to produce incipient melting overheat and facets at grain boundary junctions of ultra-low sulfur AMS 6414 steels.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c9001717
EISBN: 978-1-62708-217-4
... in accordance with the governing contractor engineering drawing. The component is part of the main landing gear and is located on the helicopter as shown in Figure 1 . This figure also shows the location of the failure (indicated by arrow). The component is forged from maraging 300 steel, and after heat...
Abstract
The US Army Research Laboratory performed a failure investigation on a broken main landing gear mount from an AH-64 Apache attack helicopter. A component had failed in flight, and initially prevented the helicopter from safely landing. In order to avoid a catastrophe, the pilot had to perform a low hover maneuver to the maintenance facility, where ground crews assembled concrete blocks at the appropriate height to allow the aircraft to safely touch down. The failed part was fabricated from maraging 300 grade steel (2,068 MPa [300 ksi] ultimate tensile strength), and was subjected to visual inspection/light optical microscopy, metallography, electron microscopy, energy dispersive spectroscopy, chemical analysis, and mechanical testing. It was observed that the vacuum cadmium coating adjacent to the fracture plane had worn off and corroded in service, thus allowing pitting corrosion to occur. The failure was hydrogen-assisted and was attributed to stress corrosion cracking (SCC) and/or corrosion fatigue (CF). Contributing to the failure was the fact that the material grain size was approximately double the required size, most likely caused from higher than nominal temperatures during thermal treatment. These large grains offered less resistance to fatigue and SCC. In addition, evidence of titanium-carbo-nitrides was detected at the grain boundaries of this material that was prohibited according to the governing specification. This phase is formed at higher thermal treatment temperatures (consistent with the large grains) and tends to embrittle the alloy. It is possible that this phase may have contributed to the intergranular attack. Recommendations were offered with respect to the use of a dry film lubricant over the cadmium coated region, and the possibility of choosing an alternative material with a lower notch sensitivity. In addition, the temperature at which this alloy is treated must be monitored to prevent coarse grain growth. As a result of this investigation and in an effort to eliminate future failures, ARL assisted in developing a cadmium brush plating procedure, and qualified two Army maintenance facilities for field repair of these components.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006835
EISBN: 978-1-62708-329-4
... of wrought products. The article addresses the types of flaws or defects that can be introduced during the steel forging process itself, including defects originating in the ingot-casting process. Defects found in nonferrous forgings—titanium, aluminum, and copper and copper alloys—also are covered...
Abstract
The primary purpose of this article is to describe general root causes of failure that are associated with wrought metals and metalworking. This includes a brief review of the discontinuities or imperfections that may be common sources of failure-inducing defects in the bulk working of wrought products. The article addresses the types of flaws or defects that can be introduced during the steel forging process itself, including defects originating in the ingot-casting process. Defects found in nonferrous forgings—titanium, aluminum, and copper and copper alloys—also are covered.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0001808
EISBN: 978-1-62708-180-1
... of operating conditions and environment or failure to recognize their significance, but it may also be the result of abuse or misuse of the product under service conditions for which it was not intended. Surface treatments can cause hydrogen to be dissolved in high-strength steels and may cause shafts...
Abstract
This article discusses failures in shafts such as connecting rods, which translate rotary motion to linear motion, and in piston rods, which translate the action of fluid power to linear motion. It describes the process of examining a failed shaft to guide the direction of failure investigation and corrective action. Fatigue failures in shafts, such as bending fatigue, torsional fatigue, contact fatigue, and axial fatigue, are reviewed. The article provides information on the brittle fracture, ductile fracture, distortion, and corrosion of shafts. Abrasive wear and adhesive wear of metal parts are also discussed. The article concludes with a discussion on the influence of metallurgical factors and fabrication practices on the fatigue properties of materials, as well as the effects of surface coatings.
Book Chapter
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003507
EISBN: 978-1-62708-180-1
.... The article provides a discussion on the imperfections found in steel forgings. The problems encountered in sheet metal forming are also discussed. The article concludes with information on the causes of failure in cold formed parts. anisotropy blisters centerline shrinkage chemical segregation cold...
Abstract
This article describes the general root causes of failure associated with wrought metals and metalworking. This includes a brief review of the discontinuities or imperfections that may be the common sources of failure-inducing defects in bulk working of wrought products. The article discusses the types of imperfections that can be traced to the original ingot product. These include chemical segregation; ingot pipe, porosity, and centerline shrinkage; high hydrogen content; nonmetallic inclusions; unmelted electrodes and shelf; and cracks, laminations, seams, pits, blisters, and scabs. The article provides a discussion on the imperfections found in steel forgings. The problems encountered in sheet metal forming are also discussed. The article concludes with information on the causes of failure in cold formed parts.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006810
EISBN: 978-1-62708-329-4
... are steel; however, many other materials are used in shaft applications. Moving shafts are often classified as either transmission shafts or machine shafts. Transmission shafts are generally cylindrical, and they transfer motion through attached componentry such as gears, pulleys, and so on. Machine...
Abstract
In addition to failures in shafts, this article discusses failures in connecting rods, which translate rotary motion to linear motion (and conversely), and in piston rods, which translate the action of fluid power to linear motion. It begins by discussing the origins of fracture. Next, the article describes the background information about the shaft used for examination. Then, it focuses on various failures in shafts, namely bending fatigue, torsional fatigue, axial fatigue, contact fatigue, wear, brittle fracture, and ductile fracture. Further, the article discusses the effects of distortion and corrosion on shafts. Finally, it discusses the types of stress raisers and the influence of changes in shaft diameter.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003532
EISBN: 978-1-62708-180-1
... be difficult to determine where the nickel plating ends and the surface begins, as shown in Fig. 11(d) . Figure 12 shows an example of ion-nitrided hot work die steel with a brittle white-etching iron nitride surface layer that is quite visible when mounted in Epomet resin but would probably be very hard...
Abstract
This article provides a discussion on the metallographic techniques used for failure analysis, and on fracture examination in materials, with illustrations. It discusses various metallographic specimen preparation techniques, namely, sectioning, mounting, grinding, polishing, and electrolytic polishing. The article also describes the microstructure examination of various materials, with emphasis on failure analysis, and concludes with information on the examination of replicas with light microscopy.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006765
EISBN: 978-1-62708-295-2
... contrast, it may be difficult to determine where the nickel plating ends and the surface begins, as shown in Fig. 3 (d). Figure 4 shows an example of ion-nitrided hot work die steel with a brittle white-etching iron nitride surface layer that is quite visible when mounted in a mineral-filled epoxy resin...
Abstract
Metallographic examination is one of the most important procedures used by metallurgists in failure analysis. Typically, the light microscope (LM) is used to assess the nature of the material microstructure and its influence on the failure mechanism. Microstructural examination can be performed with the scanning electron microscope (SEM) over the same magnification range as the LM, but examination with the latter is more efficient. This article describes the major operations in the preparation of metallographic specimens, namely sectioning, mounting, grinding, polishing, and etching. The influence of microstructures on the failure of a material is discussed and examples of such work are given to illustrate the value of light microscopy. In addition, information on heat-treatment-related failures, fabrication-/machining-related failures, and service failures is provided, with examples created using light microscopy.
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001788
EISBN: 978-1-62708-241-9
... industrial practice in an aluminum extrusion plant, nitriding is commonly used to surface harden the extrusion dies. In the case of H13 hot-work tool steel, the hardness of the nitrided surface may reach to approximately 56–62 HRC. Therefore, tensile strength values are attained at 56 RC hardness at selected...
Abstract
Several failed dies were analyzed and the results were used to evaluate fatigue damage models that have been developed to predict die life and aid in design and process optimization. The dies used in the investigation were made of H13 steels and fractured during the hot extrusion of Al-6063 billet material. They were examined to identify critical fatigue failure locations, determine corresponding stresses and strains, and uncover correlations with process parameters, design features, and life cycle data. The fatigue damage models are based on Morrow’s stress and strain-life models for flat extrusion die and account for bearing length, fillet radius, temperature, and strain rate. They were shown to provide useful information for the analysis and prevention of die failures.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003540
EISBN: 978-1-62708-180-1
... along elongated grains in heavily worked material, such as severely extruded alloys, or along the parting lines of some forgings ( Fig. 2b ). Grain facets may also be masked, such as by oxides, as is common of IG creep fracture surfaces. Fig. 1 SEM images of (a) IG fracture in ion-nitrided layer...
Abstract
This article briefly reviews the various metallurgical or environmental factors that cause a weakening of the grain boundaries and, in turn, influence the occurrence of intergranular (IG) fractures. It discusses the mechanisms of IG fractures, including the dimpled IG fracture, the IG brittle fracture, and the IG fatigue fracture. The article describes some typical embrittlement mechanisms that cause the IG fracture of steels.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001535
EISBN: 978-1-62708-232-7
..., corroborates the segregation promoting tendency of W. The retained austenite content (6.29%) in the failed roll is low and, being within acceptable limits for forged and hardened steel rolls, is therefore unlikely to aggravate spalling propensity. The role of tempered martensite in accentuating spalling...
Abstract
Although a precise understanding of roll failure genesis is complex, the microstructure of a broken roll can often unravel intrinsic deficiencies in material quality responsible for its failure. This is especially relevant in circumstances when, even under a similar mill-operating environment, the failure involves a particular roll or a specific batch of rolls. This paper provides a microstructural insight into the cause of premature breakage of a second-intermediate Sendzimir mill drive roll used at a stainless steel sheet rolling plant under the Steel Authority of India Limited. Microstructural issues influencing roll quality, such as characteristics of carbides, tempered martensite, retained austenite, etc., have been extensively studied through optical and scanning electron microscopy, electron-probe microanalysis, image analysis, and x-ray diffractometry. These are discussed to elucidate specific microstructural inadequacies that accentuated the failure. The study reveals that even through retained austenite content is low (6.29 vol%) and martensite is non-acicular, the roll breakage is a consequence of intergranular cracking caused by improper carbide morphology and distribution.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001255
EISBN: 978-1-62708-232-7
... Abstract Several back up rolls of 1400 mm barrel diam from a broad strip mill broke after a relatively short operating time as a result of bending stresses when the rolls were dismantled. The fracture occurred in the conical region of the neck at about 600 mm diam. The rolls were shaped steel...
Abstract
Several back up rolls of 1400 mm barrel diam from a broad strip mill broke after a relatively short operating time as a result of bending stresses when the rolls were dismantled. The fracture occurred in the conical region of the neck at about 600 mm diam. The rolls were shaped steel castings with 0.8 to 1.0% C, 1% Mn, 1% Cr, 0.5% Mo and 0.4% Ni and were heat treated to a tensile strength of 950 N/sq mm. Because the bending stress on mounting was only 42 N/sq mm in the fracture cross section, it was evident at the outset that material defects had promoted the fracture. In the case of this roll and the other broken rolls, the cracking and fracture were promoted by various casting defects. Investigation of the rolls showed that both the breaking off of the neck and the disintegration of the barrel edges was caused by material defects, more exactly casting defects. The fractures on the other rolls examined were so badly rusted or contaminated that they were incapable of yielding any information.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003510
EISBN: 978-1-62708-180-1
... Copper … 0.10 Prior Steel Structure The structure of the steel prior to hardening, for example, extruded, cast, forged, cold formed, and so on, may enhance the potential for cracking during the quench. Each as-formed structure requires a specific time and temperature cycle to condition...
Abstract
This article provides an overview of the effects of various material- and process-related parameters on residual stress, distortion control, cracking, and microstructure/property relationships as they relate to various types of failure. It discusses phase transformations that occur during heat treating and describes the metallurgical sources of stress and distortion during heating and cooling. The article summarizes the effect of materials and the quench-process design on distortion and cracking and details the effect of cooling characteristics on residual stress and distortion. It also provides information on the methods of minimizing distortion and tempering. The article concludes with a discussion on the effect of heat treatment processes on microstructure/property-related failures.
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