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Book Chapter
Metal Waves or Laking on Zinc-Based Diecastings
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001199
EISBN: 978-1-62708-235-8
... of production. Castings examined were of an automobile name-plate holder with two flat sides of approximately 113 sq cm. All castings produced during a trial showed laking defects, the number and position varying from casting to casting. It was found that formation of metal waves and lakes depended primarily...
Abstract
Lakes in zinc die castings are areas encompassed by irregular lines or waves on flat or slightly contoured surfaces which are intended to look uniform. The laked areas have to be removed by polishing before the castings can be plated. This adds considerably to the overall cost of production. Castings examined were of an automobile name-plate holder with two flat sides of approximately 113 sq cm. All castings produced during a trial showed laking defects, the number and position varying from casting to casting. It was found that formation of metal waves and lakes depended primarily on the design of the gate and runner system and operating conditions. High flow efficiencies, with adequate feeding to all sections of the die, and short cavity fill times are desirable.
Book Chapter
Titanium Screw Head With Fretting Structure at Contact Area With Plate Hole
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.med.c0048421
EISBN: 978-1-62708-226-6
... Abstract Wear on a titanium screw head with a lip of material that that was transported by fretting at a plate-hole edge was studied. A flat fretting zone was visible on the screw surface over the material lip. A cellular wear structure containing wear debris was found. No morphological signs...
Abstract
Wear on a titanium screw head with a lip of material that that was transported by fretting at a plate-hole edge was studied. A flat fretting zone was visible on the screw surface over the material lip. A cellular wear structure containing wear debris was found. No morphological signs of corrosion were observed in connection with fretting structures.
Book Chapter
Processing-Induced Fatigue Fracture of a Helicopter Tail Rotor Blade
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001298
EISBN: 978-1-62708-215-0
..., there was an absence of significant amounts of corrosion product and all of the pits were filled with corrosion-preventative primer. This indicated that the pitting occurred during spar manufacture, prior to the application of the primer The pitting resulted from multiple nickel plating and defective plating removal...
Abstract
A helicopter tail rotor blade spar failed in fatigue, allowing the outer section of the blade to separate in flight. The 7075-T7351 aluminum alloy blade had fiberglass pockets. The blade spar was a hollow “D” shape, and corrosion pits were present on the inner surface of the hollow spar A single corrosion pit, 0.38 mm (0.015 in.) deep, led to a fatigue failure of the spar The failure initiated on the pylon side of the blade. Dimensional analysis of the spar near the failure revealed measurements within engineering drawing tolerances. Though corrosion pitting was present, there was an absence of significant amounts of corrosion product and all of the pits were filled with corrosion-preventative primer. This indicated that the pitting occurred during spar manufacture, prior to the application of the primer The pitting resulted from multiple nickel plating and defective plating removal by acid etching. Post-plating baking operations subsequently reduced the fatigue strength of the spar.
Book Chapter
Fatigue Fracture of a Helicopter Tail Rotor Blade Due to Field-Induced Corrosion
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001297
EISBN: 978-1-62708-215-0
.... Approximately 0.66×. Testing Procedure and Results Surface Examination Visual Visual examination of the spar fracture surface revealed a flat fracture with beach mark features typical of fatigue. The fatigue fracture initiated at the inner surface of the spar cavity and propagated outward until...
Abstract
A helicopter tail rotor blade spar failed in fatigue, allowing the blade to separate during flight. The 2014-T652 aluminum alloy blade had a hollow spar shank filled with lead wool ballast and a thermoset polymeric seal. A corrosion pit was present at the origin of the fatigue zone and numerous trails of corrosion pits were located on the spar cavity's inner surfaces. The corrosion pitting resulted from the failure of the thermoset seal in the spar shank cavity. The seal failure allowed moisture to enter into the cavity. The moisture then served as an electrolyte for galvanic corrosion between the lead wool ballast and the aluminum spar inner surface. The pitting initiated fatigue cracking which led to the spar failure.
Book Chapter
Fatigue Fracture of Aluminum Wires in High-Voltage Electrical Cables in Alaska
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001124
EISBN: 978-1-62708-214-3
... oil fields in Alaska. The transmission towers were 20 m (65 ft) high with a span length of 80 m (260 ft). The utilization of the current-carrying capacity of the transmission lines was 10 to 15%. The terrain was flat, featureless Alaskan tundra, with east-west winds up to 160 km/h (100 mi/h...
Abstract
Several wires in aluminum conductor cables fractured within 5 to 8 years of, service in Alaskan tundra. The cables were comprised of 19-wire strands; the wires were aluminum alloy 6201-T81. Visual and metallographic examinations of the cold-upset pressure weld joints in the wires established that the fractures were caused by fatigue loading attributable to wind/thermal factors at the joints. The grain flow at the joints was transverse to the wire axis, rendering the notches of the joints sensitive to fatigue loading. An additional contributory factor was intergranular corrosion, which assisted fatigue crack initiation/propagation. The failure was attributed to the departure of conductor quality from the requirements of ASTM B 398 and B 399, which specify that “no joints shall be made during final drawing or in the finished wire” and that the joints should not be closer than 15 m (50 ft). The failed cable did not meet either criterion. It was recommended that the replacement cable be inspected for strict compliance to ASTM requirements.
Book Chapter
Retrieval and Analysis of Surgical Implants in Brazil: The Need for Proper Regulation
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.med.c9001690
EISBN: 978-1-62708-226-6
... established as a consequence of the failure of medical implants in service. 6 The present U.S. legislation governing failure of medical devices is rigorous with respect to liability of the manufacturer. The manufacturers are considered legally responsible for the performance of the products and are often...
Abstract
This paper summarizes several cases of metallurgical failure analysis of surgical implants conducted at the Laboratory of Failure Analysis of IPT, in Brazil. Investigation revealed that most of the samples were not in accordance with ISO standards and presented evidence of corrosion assisted fracture. Additionally, some components were found to contain fabrication/processing defects that contributed to premature failure. The implant of nonbiocompatible materials results in immeasurable damage to patients as well as losses for the public investment. It is proposed that local sanitary regulation agencies create mechanisms to avoid commercialization of surgical implants that are not in accordance with standards and adopt the practice of retrieval analysis of failed implants. This would protect the public health by identifying and preventing the main causes of failure in surgical implants.
Book Chapter
Corrosion of Aluminum Alloy 7075-T6 Wing Panel
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0006402
EISBN: 978-1-62708-217-4
.... The expanding corrosion product had cracked and, in some places, had flaked away the anodized coating. The corrodent had penetrated the base aluminum in the form of subsurface intergranular attack to a depth of 0.035 mm (0.0014 in.). It was recommended that a vapor degreaser be used during cleaning prior...
Abstract
New aircraft wing panels extruded from 7075-T6 aluminum exhibited an unusual pattern of circular black interrupted lines, which could not be removed by scouring or light sanding. The panels, subsequent to profiling and machining, were required to be penetrated inspected, shot peened, H2SO4 anodized, and coated with MIL-C-27725 integral fuel tank coating on the rib side. Scanning electron microscopy and microprobe analysis (both conventional energy-dispersive and Auger analyzers) showed that the anodic coating was applied over an improperly cleaned and contaminated surface. The expanding corrosion product had cracked and, in some places, had flaked away the anodized coating. The corrodent had penetrated the base aluminum in the form of subsurface intergranular attack to a depth of 0.035 mm (0.0014 in.). It was recommended that a vapor degreaser be used during cleaning prior to anodizing. A hot inhibited alkaline cleaner was also recommended during cleaning prior to anodizing. The panels should be dichromate sealed after anodizing. The use of deionized water was also recommended during the dichromate sealing operation. In addition, the use of an epoxy primer prior to shipment of the panels was endorsed. Most importantly, surveillance of the anodizing process itself was emphasized.
Book Chapter
Stress-Corrosion Cracking of a Forged Aircraft Lug
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.aero.c0091678
EISBN: 978-1-62708-217-4
... to be corrosion products. Apparently, the origin of the failure was a tiny region of pitting corrosion on one flat surface of the lug (back surface, Fig. 1a ; arrow there shows location of pitting corrosion region). The opposite flat surface (front, Fig. 1a ) had a shear lip at the fracture edge. Fig. 1...
Abstract
During a routine shear-pin check, the end lug on the barrel of the forward canopy actuator on a naval aircraft was found to have fractured. The lug was forged from aluminum alloy 2014-T6. Investigation (visual inspection, 2x views, and 140X micrographs etched with Keller's reagent) supported the conclusion that the cause of failure was SCC resulting from exposure to a marine environment. The fracture occurred in normal operation at a point where damage from pitting and intergranular corrosion acted as a stress raiser, not because of overload. The pitting and intergranular attack on the lug were evidence that the surface protection of the part had been inadequate as manufactured or had been damaged in service and not properly repaired in routine maintenance. Recommendations included anodizing the lug and barrel in sulfuric acid and giving them a dichromate sealing treatment, followed by application of a coat of paint primer. During routine maintenance checks, a careful examination was suggested to look for damage to the protective coating, and any necessary repairs should be made by cleaning, priming, and painting. Severely corroded parts should be removed from service.
Book Chapter
Cause and Prevention of Fatigue Failures in Boiler Tubing
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001569
EISBN: 978-1-62708-229-7
..., transgranular crack with oxide products. 50×, Nital Etch. The side wall failures contained transverse cracking on both the hot side of the tube and in the membrane area ( Figure 4 ). The fractures were oxidized, crescent-shaped, flat with ratchet marks and propagated from the outside inward ( Figure 5...
Abstract
This paper reviews several fatigue failures from the waterwall, superheater, and economizer portions of the boiler, their causes and how they were mitigated and monitored. Some cases required simple field modifications by cutting or welding, repair of existing controls, and/or changes in maintenance. Nondestructive inspections by visual, magnetic particle, ultrasonic, and radiographic methods for detecting and monitoring damage are discussed. These failures are presented to provide hindsight that will help others in increasing the success rate for anticipating and analyzing the remaining life of other units.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.mech.c9001733
EISBN: 978-1-62708-225-9
... It is characterized by a flat transverse break and a fracture which has a smooth shear surface toward the outer periphery of the wire and a microvoid formation at the center. Fig. 4 Laboratory ductile torsion failure reveals a flat, transverse break having smooth shear surface and microvoid formation...
Abstract
Drive cables from a rubber processing machine were failing in less than 8 h of operation, the expected service life being much greater than 100 h. Comparison cables were tested to failure under known stress conditions, including tensile overload, torsional loading, reversed bending alternating stress, and buckling (compressive) cyclic loading. The mode of failure was found to be reversed bending fatigue caused by drive cables moving over guide pulleys of small radii. Modifications of the machinery and drive cable system were suggested.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006801
EISBN: 978-1-62708-329-4
... in quantifying the relationship with processing quality parameters in production. Factors known to influence the ability to expand a cut edge include: Sheet metal Sheet metal strength Edge-creation method (punching, laser, waterjet, etc.) Edge quality of the hole Hole diameter Punch/die...
Abstract
Sheet forming failures divert resources from normal business activities and have significant bottom-line impact. This article focuses on the formation, causes, and limitations of four primary categories of sheet forming failures, namely necks, fractures/splits/cracks, wrinkles/loose metal, and springback/dimensional. It discusses the processes involved in analytical tools that aid in characterizing the state of a formed part. In addition, information on draw panel analysis and troubleshooting of sheet forming failures is also provided.
Book Chapter
Fracture of an Accumulator Ring Due to Hydrogen Embrittlement
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c0047192
EISBN: 978-1-62708-235-8
... flat fracture surfaces with no apparent yielding, but the two large segments did show evidence of bending (yielding) near the fractures. In addition, some segments contained fine radial cracks. Analysis (visual inspection, optical microscopy on polished-and-etched specimens, hardness testing...
Abstract
Fracture of a cadmium-plated accumulator ring forged from 4140 steel was discovered during inspection and disassembly of a hydraulic-accumulator system stored at a depot. The ring had broken into five small and two large segments. The small segments of the broken ring displayed very flat fracture surfaces with no apparent yielding, but the two large segments did show evidence of bending (yielding) near the fractures. In addition, some segments contained fine radial cracks. Analysis (visual inspection, optical microscopy on polished-and-etched specimens, hardness testing, and chemical analysis) supported the conclusion that the failure was caused due to brittle fatigue, as evidenced by the intergranular nature of the fracture path. Also, hydrogen penetration occurred during the plating operation and was not relieved subsequently as required.
Book Chapter
Failure of a Service Water Pump Shaft
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001370
EISBN: 978-1-62708-215-0
... on the fracture surface. The fracture surface was helical in shape, smooth, and flat. Some portion of the fracture surface was found to have been rubbed. A cavity near the center was observed ( Fig. 3 ). The presence of corrosion deposits masked the macroscopic fracture details. After cleaning with 50...
Abstract
A service water pump in a nuclear reactor failed when its shaft gave way. The fracture originated in the threaded portion of the sleeve nut on the drive-end side of the shaft. Results of the failure analysis showed that the cracking initiated at the thread root as a result of corrosion fatigue. Crack propagation occurred either by corrosion or mechanical fatigue. Evidence was found indicating high rotary bending stresses on the shaft during operation. The nonstandard composition of the En 8 steel used in the shaft and irregular maintenance reduced the life of the shaft. Recommendations included use of a case-hardened En 8 steel with the correct composition and regular maintenance of the pump.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003529
EISBN: 978-1-62708-180-1
... was used in the subject component Microchemical analysis: to find evidence of contamination, to evaluate the composition of microphases revealed on a metallographic specimen, or to evaluate corrosion products Extreme care must be used in interpretation of chemical analysis work performed as part...
Abstract
This article describes some of the common elemental composition analysis methods and explains the concept of referee and economy test methods in failure analysis. It discusses different types of microchemical analyses, including backscattered electron imaging, energy-dispersive spectrometry, and wavelength-dispersive spectrometry. The article concludes with information on specimen handling.
Book Chapter
Stress-Corrosion Cracking Caused by Residual Stresses in Chromium Silicon Alloy Steel Helical Compression Springs
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001119
EISBN: 978-1-62708-214-3
... surfaces (one from each spring sample) revealed a fine intergranular structure in the flat region adjacent to the coil ID ( Fig. 3 and 4 ). No fatigue striations were seen at the magnifications used; higher magnifications were not effective because of the presence of iron-oxide corrosion products...
Abstract
To samples of helical compression springs were returned to the manufacturer after failing in service well short of the component design life. Spring design specifications required conformance to SAE J157, “Oil Tempered Chromium Silicon Alloy Steel Wire and Springs.” Each spring was installed in a separate heavy truck engine in an application in which spring failure can cause total engine destruction. The springs were composed of chromium-silicon steel, with a hardness ranging from 50 to 54 HRC. Chemical composition and hardness were substantially within specification. Failure initiated from the spring inside coil surface. Examination of the fracture surface using scanning electron microscopy showed no evidence of fatigue. Final fracture occurred in torsion. X-ray diffraction analysis revealed high inner-diameter residual stresses, indicating inadequate stress relief from spring winding. It was concluded that failure initiation was caused by residual stress-driven stress-corrosion cracking, and it was recommended that the vendor provide more effective stress relief.
Book Chapter
Metallurgical Evaluation of Prestressed Wire Failures
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c9001715
EISBN: 978-1-62708-219-8
...-hand side of the photograph, and a twist on the right-hand side of the photograph. Fig. 5 A split in sample SRS #9 is shown in cross section. The split depth is approximately equal to the radius of the wire. The split is full of corrosion products. Corrosion is occurring at inclusions...
Abstract
Microstructure, corrosion, and fracture morphologies of prestressed steel wires that failed in service on concrete siphons at the Central Arizona Project (CAP) are discussed. The CAP conveys water for municipal, industrial, and agricultural use through a system of canals, tunnels, and siphons from Lake Havasu to just south of Tucson, AZ. Six siphons were made from prestressed concrete pipe units 6.4 m (21 ft) in diam and 7.7 m long, making them the largest circular precast structures ever built. The pipe was manufactured on site and consisted of a 495-mm thick concrete core, wrapped with ASTM A648 steel prestressing wire. All of the CAP failures evaluated were attributed to corrosion. Longitudinal splits reduced the service life of the pipe significantly by facilitating corrosion and introducing sharp cracks into the microstructure of the wire. A few failures were attributed to general corrosion, where the cross section of the wire is reduced until the strength of the wire is exceeded. Most of the failures evaluated were attributed to stress-corrosion cracking.
Book Chapter
Failure of a Laminated-Paper Food Cooking Tray
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001274
EISBN: 978-1-62708-215-0
... Microwaves Paper products Laminated paper (Other, miscellaneous, or unspecified) failure Background A claim was made that a microwave food tray made of laminated paper was defective and collapsed, spilling hot food on the user. Circumstances Leading to Failure A laminated-paper tray...
Abstract
A laminated-paper microwave food tray collapsed with hot food in it. Microscopic examination of the failed tray revealed no structural or material defects. Five additional trays of like construction were also tested to determine the conditions necessary to simulate the permanent deflection of the tray handles that had occurred in the failed tray. Full distortion of the handles was obtained experimentally only by dropping a full hot tray on its end onto the floor. The test results indicated that the tray had slipped from the hand of the user.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.matlhand.c9001527
EISBN: 978-1-62708-224-2
... examination, the rope, strand, and wire diameters should all be measured. Examination should also address the presence or absence of lubricant, corrosion evidence, and gross mechanical damage. Failed wires can exhibit classic cup-and-cone ductile features, flat fatigue features, and various appearances...
Abstract
Mechanical properties of wire ropes, their chemical composition, and the failure analysis process for them are described. The wires are manufactured from high-carbon, plain carbon steel, with high-strength ropes most often manufactured from AISI Grade 1074. During visual failure examination, the rope, strand, and wire diameters should all be measured. Examination should also address the presence or absence of lubricant, corrosion evidence, and gross mechanical damage. Failed wires can exhibit classic cup-and-cone ductile features, flat fatigue features, and various appearances in-between. However, wires are often mechanically damaged after failure. Most nondestructive evaluation (NDE) techniques are not applicable to wire rope failures. Electron microscope fractography of fracture surfaces is essential in failure analysis. Fatigue is the most important fracture mode in wire ropes. Metallographic features of wire ropes that failed because of ductile overload and fatigue are described.
Book Chapter
Optical Testing and Characterization
Available to PurchaseSeries: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006937
EISBN: 978-1-62708-395-9
... Transmission is one of the most obvious characteristics of a transparent plastic. It is measured using a spectrophotometer or a hazemeter in accordance with ASTM D 1003. This method uses a collimated light source, an integrating sphere, and a detector. Measurements are taken on a flat, dust-free test specimen...
Abstract
Optical testing of plastics includes the characterization of materials and the analysis of optical components. If a material is tested for transmission, haze, yellowness, and refractive index, the knowledge of its optical properties is nearly complete. For optical components, surface irregularity, birefringence, and internal contamination must also be considered. These characteristics are a function of the material and the fabrication method. Gloss and color also are affected by the base material and measured as optical properties.
Book Chapter
Failure Analysis of a Fractured Wrench Socket
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001784
EISBN: 978-1-62708-241-9
... section of the flat surface inside socket drum as shown in Figs. 1a , b and 2 . Geometry of the hexagonal grip may help a better screw grip, but it adds regions with high stress concentration that are vulnerable to failure [ 1 ]. Fig. 1 ( a , b ) Fractured wrench socket showing a large...
Abstract
A 13/16-in. hex socket failed while in use. Analysis (hardness testing, optical and scanning electron microscopy, and EDS) revealed that the socket was made of low carbon steel formed in a powder metallurgy process. A number of flaws were found including nonuniform wall thickness, poor geometric design with sharp corners as stress raisers, and incomplete sintering evidenced by unsintered particles. These were determined to be the primary cause of failure, although inclusions on the fracture surface containing S and Al may have played a role as well.
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