A forging die in a 250-ton press producing brass valves began to show signs of fatigue after a few thousand hits. By the time it reached 30,000 hits, the die was badly damaged and was submitted for analysis along with one of the last forgings produced. The investigation included visual and macroscopic inspection, metallographic and chemical analysis, SEM imaging, optical profilometry, mechanical property testing, and EDX analysis. The die was made of chromium hot-work tool steel and the forgings were made of CuZn39Pb3 heated to an initial working temperature 700 deg C. The entire surface of the die was covered with fatigue cracks and many fillets had been plastically deformed. Several other types of damage were also observed, including areas of oxidation, corrosion pits, voids, abrasive wear, die adhesion, and thermal fatigue. Fatigue cracking was the primary cause of failure with significant contributions from the other damage mechanisms.

Despite extensive aircraft landing gear design analyses and tests performed by designers and manufacturers, and the large number of trouble-free landings, aircraft users have experienced problems with and failures of landing gear components. Different data banks and over 200 failure analysis reports were surveyed to provide an overview of structural landing gear component failures as experienced by the Canadian Forces over the last 20 years on more than 20 aircraft types, and to assess trends in failure mechanisms and causes. Case histories were selected to illustrate typical problems, troublesome failure mechanisms, the role of high strength aluminum alloys and steels, and situations where fracture mechanics analyses provided insight into the failures. The two main failure mechanisms were: fatigue occurring mainly in steel components, and corrosion related problems with aluminum alloys. Very few overload failures were noted. A number of causes were identified: design deficiencies and manufacturing defects leading mainly to fatigue failures, and poor materials selection and improper maintenance as the principal causes of corrosion-related failures. The survey showed that a proper understanding of the failure mechanisms and causes, by thorough failure analysis, provides valuable feedback information to designers, operators and maintenance personnel for appropriate corrective actions to be taken.

Engineering component and structure failures manifest through many mechanisms but are most often associated with fracture in one or more forms. This article introduces the subject of fractography and aspects of how it is used in failure analysis. The basic types of fracture processes (ductile, brittle, fatigue, and creep) are described briefly, principally in terms of fracture appearances. A description of the surface, structure, and behavior of each fracture process is also included. The article provides a framework from which a prospective analyst can begin to study the fracture of a component of interest in a failure investigation. Details on the mechanisms of deformation, brittle transgranular fracture, intergranular fracture, fatigue fracture, and environmentally affected fracture are also provided.

This article provides an overview of fractography and explains how it is used in failure analysis. It reviews the basic types of fracture processes, namely, ductile, brittle, fatigue, and creep, principally in terms of fracture appearances, such as microstructure. The article also describes the general features of fatigue fractures in terms of crack initiation and fatigue crack propagation.

This article provides a description of the microscale models and mechanisms for deformation and fracture. Macroscale and microscale appearances of ductile and brittle fracture are discussed for various specimen geometries and loading conditions. The article reviews the general geometric factors and materials aspects that influence the stress-strain behavior and fracture of ductile metals. It highlights fractures arising from manufacturing imperfections and stress raisers. The article presents a root cause failure analysis case history to illustrate some of the fractography concepts.

This article focuses on characterizing the fracture-surface appearance at the microscale and contains some discussion on both crack nucleation and propagation mechanisms that cause the fracture appearance. It begins with a discussion on microscale models and mechanisms for deformation and fracture. Next, the mechanisms of void nucleation and void coalescence are briefly described. Macroscale and microscale appearances of ductile and brittle fracture are then discussed for various specimen geometries (smooth cylindrical and prismatic) and loading conditions (e.g., tension compression, bending, torsion). Finally, the factors influencing the appearance of a fracture surface and various imperfections or stress raisers are described, followed by a root-cause failure analysis case history to illustrate some of these fractography concepts.

Critical heat exchanger components are usually manufactured from durable steels, such as stainless steel, which exhibit good strength and corrosion resistance. Failure of a heat exchanger occurred due to specification of a plain carbon steel that did not survive service in the SO2 vapor environment. However, failure analysis showed that cavitation erosion was the responsible failure mechanism, not corrosion as might be expected.

A spoon that was twisted and broken by a person claiming to possess parapsychic powers was submitted for failure analysis. Exemplar tests were conducted on material taken from the bowl region of the same spoon. In addition, tests on other unbroken samples of spoons were evaluated in order to establish both macroscopic and microscopic comparative behavior. These controlled tests produced known failure mechanisms and their respective fracture morphology in this material. A direct comparison could then be made with the unknown failure. The paper identifies a method of analysis that should be applied when analyzing failures of unknown origin.

Thermomechanical fatigue (TMF) is the general term given to the material damage accumulation process that occurs with simultaneous changes in temperature and mechanical loading. TMF may couple cyclic inelastic deformation accumulation, temperature-assisted diffusion within the material, temperature-assisted grain-boundary evolution, and temperature-driven surface oxidation, among other things. This article discusses some of the major aspects and challenges of dealing with TMF life prediction. It describes the damage mechanisms of TMF and covers various experimental techniques to promote TMF damage mechanisms and elucidate mechanism coupling interactions. In addition, life modeling in TMF conditions and a practical application of TMF life prediction are presented.

Thermomechanical fatigue (TMF) refers to the process of fatigue damage under simultaneous changes in temperature and mechanical strain. This article reviews the process of TMF with a practical example of life assessment. It describes TMF damages caused due to two possible types of loading: in-phase and out-of-phase cycling. The article illustrates the ways in which damage can interact at high and low temperatures and the development of microstructurally based models in parametric form. It presents a case study of the prediction of residual life in a turbine casing of a ship through stress analysis and fracture mechanics analyses of the casing.

Cold cracking of structural steel weldments is a well-documented failure mechanism, and extensive work has been done to recognize welding and materials selection parameters associated with it. These efforts, however, have not fully eliminated the occurrence of such failures. This article examines a case of cold cracking failure in the construction industry. Fortunately, the failure was identified prior to final erection of the structural members and the weld was successfully reworked. The article explains how various welding parameters, such as electrode/wire selection, joint design, and pre/postheating, played a role in the failure. Human factors and fabrication practices that contributed to the problem are covered as well.

A type 304 stainless steel tube that failed in a boiler stack economizer was analyzed to determine the cause. The investigation consisted of visual, SEM/EDS, and metallographic analysis. Several degradation mechanisms appeared to be at work, including pitting corrosion, chloride stress corrosion cracking, and fatigue fracture. Investigators concluded that the primary failure mechanism was fatigue fracture, although either of the other mechanisms may have eventually caused the tube to fail in the absence of fatigue.

A root cause failure analysis was performed on a vaporizer coil removed from a horizontal forced circulation vaporizer. The carbon steel coil was wound in a right-hand helix with a coil centerline diameter of about 2 m. The vaporizer was gas fired and used Dowtherm A as the heat transfer fluid. Design conditions are based on annular fluid flow to cool the coil wall. NDE, metallographic and fractographic examinations were performed. Numerous, circumferentially oriented, OD initiating cracks were found near the crown for two coils near the non-fired end of the vaporizer. The cracking was confined to the inner diameter of the vaporizer coil at positions from 4:00 to 7:00. The cracking was characterized as transgranular and the fracture surface had beach marks. The failure mechanism was thermal fatigue. The heat transfer calculation predicted that dryout of the coil would occur for coils at the non-fired end of the vaporizer during low flow transients. Dryout results in rapid increase in the tube wall temperature. Thermal cycling of the coil is completed by liquid quenching resulting from resumption of normal flow rates and the return to annular flow. The probable root cause of failure was low flow transient operation.

A 25 mm (1 in.) diam carrier shaft failed suddenly during operation. The shaft failed near the toe of the 4.8 mm (316 in.) frame-to-shaft 60 deg and 120 deg submerged metal arc (SMA) tack welds after an unknown time in service. Material specifications called for the shaft to be made from SAE 1018 cold-rolled carbon steel. Carrier assembly components were made from type 300 stainless steel, and all nuts, spacers, and washers were to be SMA tack welded to the stainless steel frame. Chemical analyses (OES, SEM/EDS) showed the shaft to actually be made from SAE 1050 high-carbon steel and that a low-carbon steel welding procedure had been used. This resulted in incipient cracks in the stainless steel weld metal near the toes of the component-to-shaft welds. The hardnesses of the heat-affected zones were as high as 58 HRC, and they were grain coarsened. The parting of the shaft was determined to have been caused by an impact failure mechanism, with the origin at the incipient cracks in the weld metal. Additionally, the coarsened heat-affected zones were found to be hydrogen embrittled. The primary cause of the failure was the use of an unspecified material.

The fatigue failure of a wire rope used on a skip hoist in an underground mine has been studied as part of the ongoing research by the Bureau of Mines into haulage and materials handling hazards in mines. Macroscopic correlation of individual wire failures with wear patterns, fractography, and microhardness testing were used to gain an understanding of the failure mechanism. Wire failures occurred predominantly at characteristic wear sites between strands. These wear sites are identifiable by a large reduction in diameter; however, reduction in area was not responsible for the location of failure. Fractography revealed multiple crack initiation sites to be located at other less noticeable wear sites or opposite the characteristic wear site. Microhardness testing revealed hardening, and some softening, at wear sites.

Material samples collected from failed booster pumps were analyzed to determine the cause of failure and assess the adequacy of the materials used in the design. The pumps had been in service at a power plant, transporting feedwater from a deaerator to a main turbine boiler. Samples from critical areas of the pump were examined using optical and scanning electron microscopy, electrochemical analysis, and tensile testing. Based on microstructure and morphology, estimated corrosion rates, and particle concentrations in the feedwater, it was concluded that cavitation and erosion were the dominant failure mechanisms and that the materials and processes used to make the pumps were largely unsuited for the application.

Metallurgical SEM analysis provides many insights into the failure of biomedical materials and devices. The results of several such investigations are reported here, including findings and conclusions from the examination a total hip prosthesis, stainless steel and titanium compression plates, and hollow spinal rods. Some of the failure mechanisms that were identified include corrosive attack, corrosion plus erosion-corrosion, inclusions and stress gaps, production impurities, design flaws, and manufacturing defects. Failure prevention and mitigation strategies are also discussed.

A pressure vessel failed causing an external fire on a nine-story coke gasifier in a refinery power plant. An investigation revealed that the failure began as cracking in the gasifier internals, which led to bulging and stress rupture of the vessel shell, and the escape of hot syngas, setting off the fire. The failure mechanisms include stress relaxation cracking of a large diameter Incoloy 825 tube, stress rupture of a 4.65 in. thick chromium steel shell wall, and the oxidation of chromium steel exposed to hot syngas. The gasifier process and operating conditions that contributed to the high-temperature degradation were also analyzed and are discussed.

A fire in a storage yard engulfed several propane delivery trucks, causing one of them to explode. A series of elevated-temperature stress-rupture tears developed along the top of the truck-mounted tank as it was heated by the fire. Unstable fracture then occurred suddenly along the length of the tank and around both end caps, following the girth welds that connect them to the center portion of the tank. The remaining contents of the tank were suddenly released, aerosolized, and combusted, creating a powerful boiling liquid expanding vapor explosion (BLEVE). Based on the metallography of the tank pieces, the approximate tank temperature at the onset of explosion was determined. Metallurgical analysis provided additional insights as well as a framework for making tanks less susceptible to this destructive failure mechanism.