A missile detached from a Navy fighter jet during a routine landing on an aircraft carrier deck because of a faulty missile launcher detent spring. Visual inspection of Inconel 718 detent spring assembly revealed that four of the nine spring leafs comprising the assembly were plastically deformed while two of the deformed leafs did not meet minimal hardness or tensile requirements. Liquid penetrant testing revealed no cracks or other surface discontinuities on the leaf springs. Material sectioned from the soft spring leafs was heat-treated according to specifications in the laboratory. The resultant increase in mechanical properties of the re-heat-treated material indicated that the original heat treatment was not performed correctly. The failure was attributed to improper heat treatment. Recommendations focused on more stringent quality control of the heat-treat operations.

This paper describes the superplastic characteristics of shipbuilding steel deformed at 800 °C and a strain rate less than 0.001/s. After the superplastic deformation, the steel presents mixed fractures: by decohesion of the hard (pearlite and carbides) and ductile (ferrite) phases and by intergranular sliding of ferrite/ferrite and ferrite/pearlite, just as it occurs in stage III creep behavior. The behavior is confirmed through the Ashby-Verrall model, according to which the dislocation creep (power-law creep) and diffusion creep (linear-viscous creep) occur simultaneously.

Several stainless steel coils cracked during a routine unwinding procedure, prompting an investigation to determine the cause. The analysis included optical and scanning electron microscopy, energy-dispersive x-ray spectrometry, and tensile testing. An examination of the fracture surfaces revealed a brittle intercrystalline mode of fracture with typical manifestations of clear grain facets. Branched and discrete stepwise microcracks were also found along with unusually high levels of residual hydrogen. Mechanical tests revealed a marked loss of tensile ductility in the defective steel with elongations barely approaching 8%, compared to 50% at the time of delivery weeks earlier. Based on the timing interval and the fact that failure occurred at operating stresses well below the yield point of the material, the failure is being attributed to hydrogen-induced damage. Potential sources of hydrogen are considered as are remedial measures for controlling hydrogen content in steels.

The failure during use of a seat on a heavy-duty swing set at an elementary school was investigated. The seat contained a perforated reinforcing sheet metal (galvanized type 430 stainless steel) insert covered by an elastomeric material. Specimens of the reinforcing sheet from the failed seat were examined using SEM fractography, tensile and ductility tests, and spectrographic chemical analysis. The test results showed that the steel used did not meet the manufacturer's specifications for ductility (elongation). In addition, the small-diameter punched holes caused a stress concentration factor that aggravated the brittleness of the steel.

A 52000 bearing steel valve guide component operating in the fuel supply system of a transport aircraft broke into two pieces after 26 h of flight. The valve guide fractured through a set of elongated holes that had been electrodischarge machined into the component. Analysis indicated that the part failed by low cycle fatigue. The fracture was brittle in nature and had originated at a severely eroded zone of craters in a hard, deep white layer that was the result of remelting during electrodischarge machining. It was recommended that the remaining parts be inspected using a stereoscopic microscope and/or a borescope.

A 75 cm OD x 33 mm thick pipe in a horizontal section of a hot steam reheat line ruptured after 15 years in service. The failed section was manufactured from rolled plate of material specification SA387, grade C. The longitudinal seam weld was a double butt-weld that was V-welded from both sides and failure was found to propagate along the longitudinal seam and its HAZ. The fracture surface near the inner wall of the pipe was found to have a bluish gray appearance, while the fracture surface near the outer wall was rust colored (oxides). The transverse-to-the-weld specimen from the longitudinal seam weld was revealed to have lower elongation and a shear type failure rather than the cup-cone failures. It was concluded that the welded longitudinal seam exhibited embrittlement. A low-ductility intergranular fracture that progressed through the weld metal was revealed by scanning electron microscopy. The cracks were revealed to be in existence for some time before the final failure which was indicated by the extent and amount of corrosion products. It was concluded that low ductility was responsible for the original initiation of cracks in the pipe.

A spindle made of hardenable 13% chromium steel X40 Cr13 (Material No. 1.4034) that was fastened to a superheated steam push rod made of high temperature structural steel 13Cr-Mo44 (Material No. 1.7335) by means of a convex fillet weld, fractured at the first operation of the rod directly next to the weld bead. Investigation showed that the fracture of the superheated steam push rod spindle was caused by hardening and hardening crack formation in the weld seams and adjoining areas. It would have been preferable to avoid welding near the cross sectional transitions altogether in consideration of the crack sensitivity of high hardenability steels. If for some reason this was not possible, then all precautions should have been taken that are applicable to the particular steel, such as preheating, slow cooling and stress relief tempering after welding. The selection of an austenitic additive material should have been considered because it could have equalized stresses due to its high elongation. Most probably, however, a material of lower hardenability should have been selected for the spindle if high operating properties were of paramount importance.

Microstructural examinations on transverse cross sections of a steam reformer tube, showed the presence of large macrovoids elongated in the radial direction and emanating from the internal surface of the tube. The macrovoids were located at the interdendritic regions, and were partially filled by a Mn-Fe bearing chromium oxide film. The areas adjacent to the oxide film were chemically depleted in C, Cr and Mn and rich in Fe and Ni. Associated with this depletion were a large concentration of microvoids. It was suggested that the dissolution of carbides in areas surrounding the macrovoids and the concentration of stresses at their tips, caused extensive localized plastic deformation which led to the formation of microvoids and subsequently to the spalling of the oxide film. The non-protective character of the film induced a progressive deterioration of the grain boundaries properties. Grain boundary sliding and dislocation motion were enhanced, causing a local increase in the steady state strain rate and the premature failure of the tube.

Several wires in aluminum conductor cables fractured within 5 to 8 years of, service in Alaskan tundra. The cables were comprised of 19-wire strands; the wires were aluminum alloy 6201-T81. Visual and metallographic examinations of the cold-upset pressure weld joints in the wires established that the fractures were caused by fatigue loading attributable to wind/thermal factors at the joints. The grain flow at the joints was transverse to the wire axis, rendering the notches of the joints sensitive to fatigue loading. An additional contributory factor was intergranular corrosion, which assisted fatigue crack initiation/propagation. The failure was attributed to the departure of conductor quality from the requirements of ASTM B 398 and B 399, which specify that “no joints shall be made during final drawing or in the finished wire” and that the joints should not be closer than 15 m (50 ft). The failed cable did not meet either criterion. It was recommended that the replacement cable be inspected for strict compliance to ASTM requirements.

A sprinkler head unit that was installed in a smoking lounge of a multi story office building in 1975 failed, causing substantial water damage. There was no fire in the building. A set of four sprinkler heads -- three that had been installed in 1975 (the failed unit, an unfailed unit from the same room, and an unfailed unit from another room) and an unused 1991 unit -- were examined. casting revealed no material defects or mechanical damage. Because of several environmental factors, it was suspected that the failed unit was exposed to temperatures much above the normal office environment. On this basis, it was concluded that creep of the solder alloy was the most probable cause of failure.

A number of failures involving carbon and alloy steels were analyzed to assess the effects of inclusions and their influence on mechanical properties. Inclusions, including brittle oxides and more ductile manganese sulfides (MnS), affect fatigue endurance limit, fatigue crack propagation rates, fracture toughness, notch toughness, and transverse tensile properties, and do so in an anisotropic manner with respect to rolling direction. Significant property anisotropy has been documented in the failures investigated, providing evidence that designers failed to account for it. Typical fracture morphologies observed in such cases and metallographic appearances of MnS-containing materials are illustrated.

During a planned shut-down in 1990 it appeared that the bottom manifold parts made of wrought Incoloy 800H had undergone diametrical expansion of up to 2% due to creep. Further, cracking at the outer diam was found. It was decided to replace these parts. Microscopical investigations showed that the cracking could not be caused by creep. It was found that the cracking was confined to a 4-mm deep coarse-grained zone (ASTM 0-1) at the outer diameter. The cracking appeared to be caused by strain-induced intergranular oxidation. When the cracks reached the fine-grained material, the oxidation-cracks stopped. To determine the residual creep life of the sound (non-cracked) bottom manifold material, iso-stress creep tests were performed. It was found that tertiary creep started at 7% strain. The time-to-rupture was greater than 100,000 h. It was concluded that the bottom manifold (and thus the furnace) could be used safely during the foreseen production period.

An 1100 aluminum alloy connector of a high-tension aluminum conductor steel-reinforced (ACSR) transmission cable failed after more than 20 years in service, in a region of consider able industrial pollution. The steel core was spliced with a galvanized 1020 carbon steel sheath. Visual examination showed that the connector had undergone considerable plastic deformation and necking before fracture. The steel sheath was severely corroded, and the steel splice was pressed off-center in the axial direction inside the connector. Examination of the fracture surface and micro-structural analysis indicated that the failure was caused by mechanical overload, which occurred because of weakening of the steel support cable by corrosion inside the fitting. The corrosion was ascribed to defective assembly of the connector which allowed moisture penetration.

A sand-cast LM6M aluminum alloy sprocket drive wheel in an all-terrain vehicle failed. Extensive cracking had occurred around each of the six bolt holes in the wheel. Evidence of considerable deformation in this area was also noted. Examination indicated that the part failed because of gross overload. Use of an alloy with a much higher yield strength and improvement in design were recommended.

Galvanized A36 steel unsleeved shear-type anchor bolts failed during installation. The galvanized steel bolts were approximately 18 mm (0.7 in.) in diameter with a 90 deg bend between the long and short legs. As-fractured, sawcut, and unfractured specimens were examined. Failure analysis revealed dark thumbnail regions at the fracture origins and a very narrow and uniform shear lip. The thumbnail region exhibited zinc deposits with no apparent fracture detail, indicating preexisting cracks that had occurred before galvanizing. The balance of the fracture exhibited a transgranular mode with cleavage and ductile, dimpled shear. Hardness values as high as 35 HRC were measured in the bend area. The as-galvanized bolts fractured in a brittle manner. Failure was attributed to improper bending of the bolts, which provided a severely cold-worked bend area susceptible to strain-age embrittlement.

Failure occurred in a steel superheater tube in a power plant. The tube was specified as ASTM A 213 grade T 22, and the reported operating conditions were 13 MPa (1900 psi) at 482 deg C (900 deg F). The tube carried superheated steam and was coal fired. Investigation (visual inspection, 2% nital etched 297x images, chemical analysis, and SEM fractographs) supported the conclusion that the superheater tube failed as a result of long-term overheating. Substantial creep damage reduced the strength of the tube to the point that overload failure occurred. No recommendations were made.

Failed portions of a 4140 steel axle from a prototype urban transit vehicle were examined to determine the cause of failure. The testing procedures included visual examination, macrofractography, metallography, chemical analysis, and hardness and tensile testing. The analysis showed that a salvage welding repair had resulted in the formation of martensite that developed cracks, leading to fatigue failure of the axle. It was recommended that no weld buildup or repair be permitted on the axles.

Two sections of a galvanized cable 10.5 A 160 GR +NORM M 9533 (round stranded cable of normal type, h + 6, Langslay, right-handed) were examined. One had a 100 mm long blackish-brown tarnished zone obviously caused by localized heating at one end, inside which the hemp core was missing, and the other corresponded to the original condition of the cable. The cause of the damage was unknown. About a third of the wires had fractured and the rest had been cut. All were tensile fractures with a relatively high degree of necking. The cause of the localized heating was unknown. It can only be concluded from the investigation that the temperature did not exceed the Ac3 point of the wire material, which should be about 750 deg C, and that the heating lasted a fairly long time.

A mild steel hook that was part of the auxiliary hoist of an electric overhead crane used in a foundry was of the shank type and the rated safe working load was 15 tons. Failure took place in a wholly brittle manner, and occurred transversely through the back of the hook. From the direction in which the fracture developed, as indicated by the radial lines on its surface, it was evident that a preexisting defect served to initiate the brittle fracture. Material adjacent to the fracture was decarburized and contained numerous globules of oxide and slag. It was evident, therefore that a fissure was formed during the manufacture of the hook and had not developed in service. The failure was associated with a surface defect, and it was recommended that the other similar hooks at the establishment be crack detected and any similar discontinuities eliminated.

The shafts on two centrifugal pumps failed during use in a petroleum refinery. Light optical microscopy and scanning electron microscopy were used to analyze the damaged materials to determine the cause of failure. The results showed that one shaft, made of duplex stainless steel, failed by fatigue fracture, and the other, made of 316 austenitic stainless steel, experienced a similar fracture, which was promoted by the presence of nonmetallic inclusion particles.