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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001594
EISBN: 978-1-62708-229-7
... to detect a crack prior to the component leaking would involve frequent inspections at a given location and that the cost of the inspection program would far exceed the benefits of avoiding a leak. Instead, TU Electric locates these cracks by visually monitoring for leaks. Field experience with fatigue...
Abstract
Nuclear power plants typically experience two or three high-cycle fatigue failures of stainless steel socket-welded connections in small bore piping during each plant-year of operation. This paper discusses fatigue-induced failure in socket-welded joints and the strategy Texas Utilities Electric Company (TU Electric) has implemented in response to these failures. High-cycle fatigue is invisible to proven commercial nondestructive evaluation (NDE) methods during crack initiation and the initial phases of crack growth. Under a constant applied stress, cracks grow at accelerating rates, which means cracks extend from a detectable size to a through-wall crack in a relatively short time. When fatigue cracks grow large enough to be visible to NDE, it is likely that the component is near the end of its useful life. TU Electric has determined that an inspection program designed to detect a crack prior to the component leaking would involve frequent inspections at a given location and that the cost of the inspection program would far exceed the benefits of avoiding a leak. Instead, TU Electric locates these cracks by visually monitoring for leaks. Field experience with fatigue-induced cracks in socket-welded joints has confirmed that visual monitoring does detect cracks in a timely manner, that these cracks do not result in catastrophic failures, and that the plant can be safely shut down in spite of a leaking socket-welded joint in a small bore pipe. Historical data from TU Electric and Southwest Research Institute are presented regarding the frequency of failures, failure locations, and the potential causes. The topics addressed include 1) metallurgical and fractographic features of fatigue cracks at the weld toe and weld root; 2) factors that are associated with fatigue, such as mechanical vibration, internal pulsation, joint design, and welding workmanship; and 3) implications of a leaking crack on plant safety. TU Electric has implemented the use of modified welding techniques for the fabrication of socket-welded joints that are expected to improve their ability to tolerate fatigue.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006913
EISBN: 978-1-62708-395-9
... where an electrical field is present, the dielectric breakdown property is an important factor. The dielectric strength of a material is, in many situations, the deciding factor in the nature of the system in which it is to be used. Results obtained using this test provide part of the information...
Abstract
This article addresses electrical testing and characterization of plastics and presents a number of techniques for evaluating the electrical properties of insulating materials, with a special focus on plastics, accompanied by a list of the electrical properties of different types of plastics. It provides the reader with sufficient information to select the appropriate electrical test(s) for a specific application. The tests covered in this article are widely used in industry to determine the electrical properties of insulating materials, particularly plastics. The article lists and defines terms used in connection with testing and specification of plastics for electrical applications.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.process.c9001443
EISBN: 978-1-62708-235-8
... Abstract Following the fusing of one of the copper leads in the choke circuit of an electric welder, a piece of the affected lead was obtained for examination. The sample had large internal cavities and surface bulges. It is remarkable that a wire containing defects of the magnitude present...
Abstract
Following the fusing of one of the copper leads in the choke circuit of an electric welder, a piece of the affected lead was obtained for examination. The sample had large internal cavities and surface bulges. It is remarkable that a wire containing defects of the magnitude present in this case could have been drawn without failure. Failure in service was due to overheating resulting from the inability of the conductor to carry the current where its cross section was reduced by the presence of a cavity. Another failure of a conductor occurred in one of the field coils of a direct-current motor. The mode of failure and the changes in the microstructure showed that fracture was due to a defective resistance butt-weld which had been made when the wire was in process of drawing. A further example of a conductor failure occurred in a 12 SWG copper connection between the rotor contactor and the resistance in a starter. A transverse section through the zone of failure showed an oxide layer extended almost completely across the plane of a weld, and also the grain growth that had occurred in this region.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006769
EISBN: 978-1-62708-295-2
... a heated filament to produce electrons. These thermionic sources use tungsten or lanthanum hexaboride (LaB 6 ) as the filament material, with tungsten being less expensive and more robust, while LaB 6 is brighter and lasts longer. Scanning electron microscopes that use a strong electric field to remove...
Abstract
The scanning electron microscope (SEM) is one of the most versatile instruments for investigating the microscopic features of most solid materials. The SEM provides the user with an unparalleled ability to observe and quantify the surface of a sample. This article discusses the development of SEM technology and operating principles of basic systems of SEM. The basic systems covered include the electron optical column, signal detection and display equipment, and the vacuum system. The processes involved in the preparation of samples for observation using an SEM are described, and the application of SEM in fractography is discussed. The article covers the failure mechanisms of ductile failure, brittle failure, mixed-mode failure, and fatigue failure. Lastly, image dependence on microscope type and operating parameters is also discussed.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003533
EISBN: 978-1-62708-180-1
... being less expensive and more robust while LaB 6 is brighter and lasts longer. Scanning electron microscopes that use a high electric field to remove electrons from a tungsten filament are termed cold-field-emission SEMs or high-resolution SEMs and have the highest resolution capabilities of all SEMs...
Abstract
The scanning electron microscopy (SEM) is one of the most versatile instruments for investigating the microstructure of metallic materials. This article highlights the development of SEM technology and describes the operation of basic systems in an SEM, including the electron optical column, signal detection and display equipment, and vacuum system. It discusses the preparation of samples for observation using an SEM and describes the application of SEM in fractography. If the surface remains unaffected and undamaged by events subsequent to the actual failure, it is often a simple matter to determine the failure mode by the use of an SEM. In cases where the surface is altered after the initial failure, the case may not be so straightforward. The article presents typical examples that illustrate these points. Image dependence on the microscope type and operating parameters is also discussed.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001120
EISBN: 978-1-62708-214-3
... Abstract A segment from a premium-quality H13 tool steel die for die casting of aluminum failed after only 700 shots. The segment was subjected to visual, macroscopic, hardness, and metallographic testing. The investigation revealed that failure occurred as a result of fatigue at an electrical...
Abstract
A segment from a premium-quality H13 tool steel die for die casting of aluminum failed after only 700 shots. The segment was subjected to visual, macroscopic, hardness, and metallographic testing. The investigation revealed that failure occurred as a result of fatigue at an electrical-discharge-machined surface where the resulting rehardened layer had not been removed. This rehardened layer had cracked, providing a source for fatigue initiation.
Series: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001076
EISBN: 978-1-62708-214-3
... system at appropriate locations were recommended. Electrostatic fields Gas pipelines Static electricity Thrust bearings Turbogenerators Silver (Other, miscellaneous, or unspecified) failure Background The silver layer on a thrust bearing face in a power turbine experienced...
Abstract
The silver layer on a thrust bearing face experienced electrostatic discharge attack (the bombardment of an in-line series of individual sparks onto the soft bearing face), which destroyed the integrity of the bearing surface. The electrical attack appeared as scratches to the naked eye. Macrophotography showed that the attack was more severe at one edge of each pad, resulting in deeper grooving and a buildup of deposits, mostly silver sulfides. Microstructural analysis of a cross section indicated that the interface between the silver overlay and the substrate (beryllium copper) was sound and free of voids and foreign material. Corrosion products contained a large quantity of sulfur. The probable cause of the attack was the presence of electrical current within the system, with sulfides a possible contributing factor. Elimination of residual magnetism and grounding of the rotating system at appropriate locations were recommended.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.usage.c0046242
EISBN: 978-1-62708-236-5
... for steel (for comparison, magnetic steels have a flux density of about 9000 G). A field test around the boiler-feed pump indicated virtually no electric forces that could induce magnetism in the gears. Therefore, the gear must have been magnetized before being put into service. A logical source...
Abstract
An integral coupling and gear (Cr-Mo steel), used on a turbine-driven main boiler-feed pump, was removed from service after one year of operation because of excessive vibration. Spectrographic analysis and metallographic examination revealed the fact that gritty material in the gear teeth (found at visual inspection) was composed of the same material as the metal in the coupling. Beach marks and evidence of cold work, typical of fatigue failure, were found on the fracture surface. Chips remaining in the analysis cut were difficult to remove, indicating a strong magnetic field in the part. Evidence found supports the conclusions that failure of the coupling was by fatigue and that incomplete demagnetization of the coupling following magnetic-particle inspection caused retention of metal chips in the roots of the teeth. Improper lubrication caused gear teeth to overheat and spall, producing chips that eventually overstressed the gear, causing failure. Because the oil circulation system was not operating properly, metal chips were not removed from the coupling. Recommendations included checking the replacement coupling for residual magnetism and changing or filtering the pump oil to remove any debris.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001725
EISBN: 978-1-62708-229-7
....) On the day of the failure, when the electrical load was lost and the rotating field oversped, the ring was subjected to a much higher stress than normal. It was calculated that during this period of overspeeding the stress in the retaining ring was about 35,000 psi. This is considerably lower than the yield...
Abstract
Another failure in a turbogenerator, similar to the accidents in Toronto described in Metal Progress in July 1956, was due to the presence of fatigue cracks at ventilating holes. These acted as stress-raisers during temporary and minor overspeeding, inducing an almost instantaneous brittle failure which wrecked the machine, fortunately without human casualty.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.bldgs.c0089752
EISBN: 978-1-62708-219-8
...-fabricated in 12 m (40 ft) lengths, then shop welded into 24 m (80 ft) lengths. Field assembly was with bell-and-spigot joints. Investigation (visual inspection and Charpy V-notch testing) supported the conclusion that brittle fracture of the aqueduct pipe was attributed to a combination of stress...
Abstract
A 208 cm (82 in.) ID steel aqueduct (ASTM A572, grade 42, type 2 steel) fractured circumferentially at two points 152 m (500 ft) apart in a section above ground. A year later, another fracture occurred in a buried section 6.4 km (4 mi) away. Both pipes fractured during Jan at similar temperatures and pressures. The pipe had a 24 mm wall thickness, and the hydrostatic head was 331 m (1085 ft). The air temperature was approximately -13 deg C (9 deg F), the water temperature approximately 0.6 deg C (33 deg F), and the steel temperature approximately -4 deg C (25 deg F). The pipe had been shop-fabricated in 12 m (40 ft) lengths, then shop welded into 24 m (80 ft) lengths. Field assembly was with bell-and-spigot joints. Investigation (visual inspection and Charpy V-notch testing) supported the conclusion that brittle fracture of the aqueduct pipe was attributed to a combination of stress concentrations at the toes of the fillet welds due to poor welding technique, including shop welds made without preheat, and a brittle condition of the steel at winter temperatures. Recommendations included revised welding techniques, installation of expansion joints, and the use of steel plate rolled from fully killed ingots.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001691
EISBN: 978-1-62708-234-1
... low strength. When heat-treated for strength, AlCu 2 forms and the strength is increased. Over-heating during welding can sensitize these materials for corrosion. Manganese is the major alloying element of 3003. Tests Testing can be in a laboratory or a pilot-plant. Pilot-plant or field tests...
Abstract
The Advanced Photon Source (APS) is a state-of-the-art synchrotron light source. The storage ring vacuum chamber is fabricated from 6061 extruded aluminum. Water connections to the vacuum chambers that were fabricated from 3003 aluminum had developed water leaks, which were subsequently remedied after considerable investigations.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006788
EISBN: 978-1-62708-295-2
... controlled conditions, consistent with high corrosion rates seen in the field. Fig. 6 Electrical microbiologically influenced corrosion mechanism for sulfate-reducing bacteria (SRB) Not all microorganisms are capable of accepting electrons directly from the surface of conductive materials...
Abstract
This article focuses on the mechanisms of microbiologically influenced corrosion as a basis for discussion on the diagnosis, management, and prevention of biological corrosion failures in piping, tanks, heat exchangers, and cooling towers. It begins with an overview of the scope of microbial activity and the corrosion process. Then, various mechanisms that influence corrosion in microorganisms are discussed. The focus is on the incremental activities needed to assess the role played by microorganisms, if any, in the overall scenario. The article presents a case study that illustrates opportunities to improve operating processes and procedures related to the management of system integrity. Industry experience with corrosion-resistant alloys of steel, copper, and aluminum is reviewed. The article ends with a discussion on monitoring and preventing microbiologically influenced corrosion failures.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001661
EISBN: 978-1-62708-229-7
.... The NDT inspections, evaluations, method of field metallography, analysis and conclusions are discussed with recommendations for corrective actions in the following report. Cracking (fracturing) Electric power generation Field metallography Plates (structural members) Welded joints 610Steel...
Abstract
An evaluation of indications in the main turbine building column horizontal plate welds was conducted by the joint efforts of field metallography and nondestructive examinations. The turbine building main column horizontal plate welds were selected at random and were inspected to find discontinuities, metallurgical evaluation of the discontinuities, analysis of any failure modes, and determination of the best repair techniques. The welds were made with prequalified joints in accordance with AWS D1.1-77 and required only visual inspection. More sensitive inspection methods were applied to the welds in order to better define the indications found with the visual inspections. Cracks were found in 17 field welds and in two test plate welds. The causes of the cracking are related to the weld design and installation procedure. Three field welds were rejected because of the depth of the cracks. The NDT inspections, evaluations, method of field metallography, analysis and conclusions are discussed with recommendations for corrective actions in the following report.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006827
EISBN: 978-1-62708-329-4
... at the assembly level. This article covers the properties of solder alloys and the corresponding intermetallic compounds. It includes the dominant failure modes introduced during the solder joint manufacturing process and in field-use applications. The corresponding failure mechanism and root-cause analysis...
Abstract
Due to the recent requirement of higher integration density, solder joints are getting smaller in electronic product assemblies, which makes the joints more vulnerable to failure. Thus, the root-cause failure analysis for the solder joints becomes important to prevent failure at the assembly level. This article covers the properties of solder alloys and the corresponding intermetallic compounds. It includes the dominant failure modes introduced during the solder joint manufacturing process and in field-use applications. The corresponding failure mechanism and root-cause analysis are also presented. The article introduces several frequently used methods for solder joint failure detection, prevention, and isolation (identification for the failed location).
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001666
EISBN: 978-1-62708-229-7
... Abstract Stress-corrosion cracking of low-alloy steel turbine discs has emerged as a generic concern in nuclear generating stations. An investigation that made extensive use of field metallographic techniques to examine suspected cracking in such a component is described. The crack position...
Abstract
Stress-corrosion cracking of low-alloy steel turbine discs has emerged as a generic concern in nuclear generating stations. An investigation that made extensive use of field metallographic techniques to examine suspected cracking in such a component is described. The crack position, and its relationship to surface topographic features, were examined and recorded by magnetic rubber and high-resolution dental rubber replicating materials. Corrosion deposits on keyway surfaces and within the crack were collected with acetate foil replicas applied and then stripped from the keyway surfaces. Microstructural details were revealed by the use of field metallographic preparation techniques and replicated by acetate foil for examination with optical and scanning electron microscopes. It was possible by these techniques to establish the cracking mechanism as stress corrosion possibly related to chloride or sulphate ion steam contaminants. Subsequent sectioning and conventional metallography confirmed both the validity of the conclusions and the replication techniques.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.steel.c9001645
EISBN: 978-1-62708-232-7
... or multiple interactions among several factors. The important factors that contribute to premature service failure include improper fitting, inadequate lubrication, overloading, vibration, impact loading, debris ingress, contamination, high operating temperatures, and stray electrical fields. Bearings subject...
Abstract
An extensive metallurgical investigation was carried out on samples of a failed roller bearing from the support and tilting system of a basic oxygen furnace converter used in the steel melting shop of an integrated steel plant. The converter bearing was fabricated from low-carbon, carburizing grade steel and had failed in service within a year of fitting to a repaired shaft. Microscopic observations of both the broken roller and inner-race samples revealed subsurface cracking and preponderance of brittle oxide and other macroinclusions. Electron probe microanalysis studies confirmed that the brittle oxides that formed stringers were alumina, and the other macroinclusions were complex silicates. Both the alumina and silicate inclusions were deleterious to contact-fatigue properties. Microstructurally, the carburized regions of the broken roller and of inner-race samples contained high-carbon tempered martensite. Microhardness measurements revealed that. Although the core hardness of the roller and the inner-race samples were similar, the surface hardness of the roller was approximately 8.5 HRC units harder than that of the inner-race. SEM observations of the roller fracture surface revealed striations indicative of fatigue, and EDS analyses corroborated a high incidence of silicate inclusions at crack sites. The study suggests that the failure of the bearing occurred because the hardness difference between the roller bearing and the inner-race surfaces resulted in wear of the inner-race. The wear led to shaft misalignment and play during service. The misalignment, coupled with the presence of inclusions, caused fatigue failure of the roller bearing.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003556
EISBN: 978-1-62708-180-1
... intergranular pitting of 304L stainless steel condenser tubes in a geothermal electrical power plant operating at >100 °C (> 210 °F) has been reported ( Ref 16 ). In another example, microbiological activity and chloride concentrated under scale deposits were blamed for the wormhole pitting of carbon...
Abstract
This article focuses on the mechanisms of microbially induced or influenced corrosion (MIC) of metallic materials as an introduction to the recognition, management, and prevention of microbiological corrosion failures in piping, tanks, heat exchangers, and cooling towers. It discusses the degradation of various protective systems, such as corrosion inhibitors and lubricants. The article describes the failure analysis of steel, iron, copper, aluminum, and their alloys. It also discusses the probes available to monitor conditions relevant to MIC in industrial systems and the sampling and analysis of conditions usually achieved by the installation of removable coupons in the target system. The article also explains the prevention and control strategies of MIC in industrial systems.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006822
EISBN: 978-1-62708-329-4
.... If possible, a field investigation should be performed soon after the incident, and prior to any further analysis, to document the layout of the pipe in the ground, to gather field-specific information such as coating condition, and to gather samples of corrosion products (if present), samples of liquids...
Abstract
This article discusses the failure analysis of several steel transmission pipeline failures, describes the causes and characteristics of specific pipeline failure modes, and introduces pipeline failure prevention and integrity management practices and methodologies. In addition, it covers the use of transmission pipeline in North America, discusses the procedures in pipeline failure analysis investigation, and provides a brief background on the most commonly observed pipeline flaws and degradation mechanisms. A case study related to hydrogen cracking and a hard spot is also presented.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006764
EISBN: 978-1-62708-295-2
... comparison with reference sample. Part edges complicate results, and a skilled operator is required. No fluid coupling required. Can adapt to high-speed production lines Metals only Potential drop Measures electrical resistance between/among probes contacting material surface Online monitoring...
Abstract
Nondestructive testing (NDT), also known as nondestructive evaluation (NDE), includes various techniques to characterize materials without damage. This article focuses on the typical NDE techniques that may be considered when conducting a failure investigation. The article begins with discussion about the concept of the probability of detection (POD), on which the statistical reliability of crack detection is based. The coverage includes the various methods of surface inspection, including visual-examination tools, scanning technology in dimensional metrology, and the common methods of detecting surface discontinuities by magnetic-particle inspection, liquid penetrant inspection, and eddy-current testing. The major NDE methods for internal (volumetric) inspection in failure analysis also are described.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0001820
EISBN: 978-1-62708-180-1
... penetration Electric welds (a) Upturned fiber cracks Weld-line inclusions Cold weld Excessive trim Contact burns Field weld defects Causes of service failures Defects in the pipe body Mechanical damage Environmental causes Corrosion (external or internal...
Abstract
This article describes the failure characteristics of high-pressure long-distance pipelines. It discusses the causes of pipeline failures and the procedures used to investigate them. The use of fracture mechanics in failure investigations and in developing remedial measures is also reviewed.
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