A case of continual product refinement stimulated by product failures was described. Brittle fracture of gas transmission line pipe steels occurred demonstrating a poor combination of materials, environment, manufacturing and installation problems, and loads. Initial efforts were concentrated towards decreasing the Charpy ductile-to-brittle transition temperature to avoid brittle fracture. It was subsequently revealed that the absorbed energy on the upper shelf of the Charpy energy-temperature curve was critical for arresting a moving crack. Both fracture initiation and fracture propagation were needed be controlled. It was concluded that improved steel processing procedures, chiefly hot-working temperature and deformation control, were also required to optimize microstructure and properties.

On 23 Dec 1997, a portion of the main ore conveyor at a large mine collapsed onto a highway and shut down mine operations. The conveyor structure that collapsed was supported by a steel truss spanning 185 ft. Truss failure occurred just as the conveyor transport rate was increased to 8,260 tph. Under this total loading, which was only slightly above the regular operating condition, a poorly designed and fabricated transition joint in the west lower chord failed, thereby overloading other key structural members and causing the entire truss to collapse. Another contributing cause of the collapse was the transition joint welds, where the fracture originated. They were made with undersized fillet welds, 20% smaller than specified on the original fabrication drawing. Because of the poorly designed joint detail and the deficient welds, both of which concentrated stress and strain in the low ductility direction of the transition joint plate, lamellar tearing of plate material occurred at the boxed I-beam fillet weld attachment. Brittle fracture of this joint precipitated global collapse of the truss structure.

A support arm on a front-end loader failed in a brittle manner while lifting a load. The arm had a cross section of 50 x 200 mm (2 x 8 in.). Material used for the arm was hot-rolled ASTM A572, grade 42 (type 1), steel, which exhibited poor impact properties in the as-rolled condition and had a ductile-to-brittle transition temperature exceeding 93 deg C (200 deg F). This transition temperature was much too high for the application. It was recommended that a modified ASTM A572, grade 42 (0.15% C max), type 1 or 2, steel be used (type 1, which contains niobium, may be needed to meet strength requirements). The steel should be specified to be killed, fine-grained, and normalized, with Charpy V-notch impact-energy values of 20 J (15 ft·lbf) at -46 deg C (-50 deg F) in the longitudinal direction and 20 J (15 ft·lbf) at -29 deg C (-20 deg F) in the transverse direction.

Cracks initiating from the tip of the cloverleaf pattern in steel cargo tiedown sockets were observed by the builder following installation aboard several cargo vessels in various stages of construction. Testing of finite element models and measurements performed in the field on cargo ships with the cracking problem supported the conclusion that the failure was caused by overload. Additional testing showed that the overload failure and the transition from ductile to brittle fracture were facilitated by a combination of high brittleness due to flame cutting, increased hardness due to the cold-working coining process, and high residual stresses created by welding. Recommendations included the removal of the brittle, carbon-rich transformed martensite layer introduced by flame cutting and the application of a localized stress-relief heat treatment process. X-ray diffraction residual-stress measurements were then performed on heat treated tiedown sockets to verify the effectiveness of the localized heat treatment process applied.

A 208 cm (82 in.) ID steel aqueduct (ASTM A572, grade 42, type 2 steel) fractured circumferentially at two points 152 m (500 ft) apart in a section above ground. A year later, another fracture occurred in a buried section 6.4 km (4 mi) away. Both pipes fractured during Jan at similar temperatures and pressures. The pipe had a 24 mm wall thickness, and the hydrostatic head was 331 m (1085 ft). The air temperature was approximately -13 deg C (9 deg F), the water temperature approximately 0.6 deg C (33 deg F), and the steel temperature approximately -4 deg C (25 deg F). The pipe had been shop-fabricated in 12 m (40 ft) lengths, then shop welded into 24 m (80 ft) lengths. Field assembly was with bell-and-spigot joints. Investigation (visual inspection and Charpy V-notch testing) supported the conclusion that brittle fracture of the aqueduct pipe was attributed to a combination of stress concentrations at the toes of the fillet welds due to poor welding technique, including shop welds made without preheat, and a brittle condition of the steel at winter temperatures. Recommendations included revised welding techniques, installation of expansion joints, and the use of steel plate rolled from fully killed ingots.

The splined shaft (1040 steel, heat treated to a hardness of 44 to 46 HRC and a tensile strength of approximately 1448 MPa, or 210 ksi) from a front-end loader used in a salt-handling area broke after being in service approximately two weeks while operating at temperatures near -18 deg C (0 deg F). During the summer, similar shafts had a service life of 5 to eight months. Examination of the fracture surface showed brittle fatigue cracks, and visual examination of the splines disclosed heavy chatter marks at the root of the spline, with burrs and tears at the fillet area. Evidence found supports the conclusion that the shaft failed as the result of stress in the sharp fillets and rough surfaces at the root of the splines. Cold weather failure occurred sooner than in hot weather because ductile-to-brittle transition temperature of the 1040 steel shaft was too high. Recommendations include redesign of the fillet radius to a minimum of 1.6 mm (0.06 in.) and a maximum surface finish in the spline area of 0.8 microns. Material for the shafts should be modified to a nickel alloy steel, heat treated to a hardness of 28 to 32 HRC before machining.

A metallurgical failure analysis was performed on pieces of the cracked vent header pipe from the Edwin I. Hatch Unit 2 Nuclear power plant. The analysis consisted of optical microscopy, chemical analysis, mechanical Charpy impact testing, and fractography. It was found that the material of the vent header met the mechanical and chemical properties of ASTM A516 Grade 70 carbon-manganese steel material and microstructures were consistent with this material. Fracture faces of the cracked pipe were predominantly brittle in appearance with no evidence of fatigue contribution. The NDTT (Nil ductility Transition Temperature) for this material was approximately -51 deg C (-60 deg F). The fact that the material's NDTT was significantly out of the normal operating range of the pipe suggested an impingement of low temperature nitrogen (caused by a faulty torus inerting system) induced a thermal shock in the pipe which, when cooled below its NDTT, cracked in a brittle manner.

The discussion on the fracture of solid materials, both metals and polymers, customarily begins with a presentation of the stress-strain behavior and of how various conditions such as temperature and strain-rate affect the mechanisms of deformation and fracture. This article describes crazing and fracture in polymeric materials, with a review of the behavior of the elastic modulus as a function of temperature or time parameters, emphasizing the importance of the viscoelastic nature of their deformation and fracture. The discussion covers the behavior of polymers under stress, provides information on ductile and brittle behaviors, and describes craze initiation in polymers and crack formation and fracture by crazing. Macroscopic permanent deformation of polymeric materials caused by shear-yielding and crazing, which eventually can result in fracture and failure, is also covered.

An anchorage plate which fractured was one of a pair used as intermediate members through which the boom suspension ropes were attached to the jury-mast of an excavator. Failure of the plate released the ropes on one side of the boom, resulting in extensive damage to the latter and also bending of the other anchorage plate. The anchorage plates were 23 x 9 in. and had been flame-cut from mild steel plate. Collars were fillet-welded on each side at both ends to provide extra bearing area for the pins. Holes had then been flame-cut slightly under size and bored to final dimensions. The plates were given a slight set after flame-cutting to provide a more direct line of pull for the ropes. The fracture surface was bounded by narrow lips, indicative of shear failure. Failure of the anchorage plate was attributed to cracks present at the junctions of the fillet welds, and deficient notch-ductility of the material from which the plates were made.

A cast steel bracket manufactured in accordance with ASTM A 148 grade 135/125 steel failed in railroad maintenance service. Ancillary property requirements included a 285 to 331 HB hardness range and minimum impact energy of 27 J (20 ft·lbf) at -40 deg C (-40 deg F). The conditions at the time of failure were characterized as relatively cold. Investigation (visual inspection, chemical analysis, and unetched 119x and 2% nital etched 119x SEM images) supported the conclusion that the bracket failed through brittle overload fracture due to a number of synergistic factors. The quenched-and-tempered microstructure contained solidification shrinkage, inherently poor ductility, and type II Mn-S inclusions that are known to reduce ductility. The macro and microscale fracture features confirmed that the casting was likely in low-temperature service at the time of failure. The composition and mechanical properties of the casting did not satisfy the design requirements. Recommendations included exerting better composition control, primarily with regard to melting, deoxidation, and nitrogen control. Better deoxidation practice was recommended to generate the more desirable Mn-S inclusion morphology, and reevaluation of the casting design was suggested to minimize shrinkage.

Overload failures refer to the ductile or brittle fracture of a material when stresses exceed the load-bearing capacity of a material. This article reviews some mechanistic aspects of ductile and brittle crack propagation, including a discussion on mixed-mode cracking, which may also occur when an overload failure is caused by a combination of ductile and brittle cracking mechanisms. It describes the general aspects of fracture modes and mechanisms. The article discusses some of the material, mechanical, and environmental factors that may be involved in determining the root cause of an overload failure. It also presents examples of thermally and environmentally induced embrittlement effects that can alter the overload fracture behavior of metals.

This article aims to identify and illustrate the types of overload failures, which are categorized as failures due to insufficient material strength and underdesign, failures due to stress concentration and material defects, and failures due to material alteration. It describes the general aspects of fracture modes and mechanisms. The article briefly reviews some mechanistic aspects of ductile and brittle crack propagation, including discussion on mixed-mode cracking. Factors associated with overload failures are discussed, and, where appropriate, preventive steps for reducing the likelihood of overload fractures are included. The article focuses primarily on the contribution of embrittlement to overload failure. The embrittling phenomena are described and differentiated by their causes, effects, and remedial methods, so that failure characteristics can be directly compared during practical failure investigation. The article describes the effects of mechanical loading on a part in service and provides information on laboratory fracture examination.

A housing used in conjunction with an electrical switch failed shortly after being placed into service. A relatively high failure rate had been encountered, corresponding to a recent production lot of the housings, and the failed part was representative of the problem. The housing had been injection molded from a commercially available, medium-viscosity grade of PC, formulated with an ultraviolet stabilizer. In addition to the PC housing, the design of the switch included an external protective zinc component installed with a snap-fit and two retained copper press-fit contact inserts. Investigation supported the conclusion that the switch housings failed via brittle fracture, likely through a creep mechanism. The failure was caused by severe embrittlement of the housing resin associated with massive molecular degradation produced during the molding process. A potential contributing factor was the design of the part, which produced significant interference stresses between the contact and a mating retaining tab.

The 8620 steel latch tip, carburized and then induction hardened to a minimum surface hardness of 62 HRC, on the main-clutch stop arm on a business machine fractured during normal operation when the latch tip was subjected to intermittent impact loading. Fractographic examination 9x showed a brittle appearance at the fractures. Micrograph examination of an etched section disclosed several small cracks. Fracture of the parts may have occurred through similar cracks. Also observed was a burned layer approximately 0.075 mm (0.003 in.) deep on the latch surface, and hardness at a depth of 0.025 mm (0.001 in.) in this layer was 52 HRC (a minimum of 55 HRC was specified). Thus, the failure was caused by brittle fracture in the hardness-transition zone as the result of excessive impact loading. The burned layer indicated that the cracks had been caused by improper grinding after hardening. Redesign was recommended to include reinforcing the backing web of the tip, increasing the radius at the relief step to 1.5 x 0.5 mm (0.06 x 0.02 in.), the use of proper grinding techniques, and a requirement that the hardened zone extend a minimum of 1.5 mm (0.06 in.) beyond the step.

A 150 cm ID boiler drum made form ASTM A515, grade 70, steel failed during final hydrotesting at a pressure of approximately 26 MPa. Brittle fractures were revealed in between two SA-106C nozzles and remainder was found to involve tearing. Short, flat segments of fracture area, indicative of pre-existing cracks, were revealed by examination of the fracture surface at the drain grooves arc gouged at the nozzle sites. A thin layer of material with a dendritic structure was observed at the groove surface. The dendritic layer was revealed by qualitative microprobe analysis to contain over 1% C, higher than the carbon content of the base metal. The cracks in the drain groove surface could have occurred after arc gouging, during subsequent stress-relieving, or during the hydrostatic test. Flame cutting is not recommended for the type of steel used in the boiler drum because it can lead to local embrittlement and stress raisers, potentially initiating major failures.

A detailed fracture mechanics evaluation is the most accurate and reliable prediction of process equipment susceptibility to brittle fracture. This article provides an overview and discussion on brittle fracture. The discussion covers the reasons to evaluate brittle fracture, provides a brief summary of historical failures that were found to be a result of brittle fracture, and describes key components that drive susceptibility to a brittle fracture failure, namely stress, material toughness, and cracklike defect. It also presents industry codes and standards that assess susceptibility to brittle fracture. Additionally, a series of case study examples are presented that demonstrate assessment procedures used to mitigate the risk of brittle fracture in process equipment.

This article reviews the impact response of plastic components and the various methods used to evaluate it.. It describes the effects of loading rate on polymer deformation and the influence of temperature and strain rate on failure mode. It discusses the advantages and limitations of standard impact tests, the use of puncture tests for assessing material behavior under extreme strain, and the application of fracture mechanics for analyzing impact failures. It also develops and demonstrates the theory involved in the design and analysis of thin-walled, injection-molded plastic components.

The upper frame from a large cone crusher failed in severe service after an unspecified service duration. The ductile iron casting was identified as grade 80-55-06, signifying minimum properties of 552 MPa (80 ksi) tensile strength, 379 MPa (55 ksi) yield strength, and 6% elongation. Investigation (visual inspection, chemical analysis, unetched 30x images, and 2% nital etched 30x images) was difficult because the fracture surface of the frame section was obliterated by postfracture corrosion. Repeated attempts at cleaning using progressively stronger chemicals revealed that no telltale fracture morphology remained. However, the investigation supported the conclusion that the crusher frame failed via brittle overload fracture, likely due to excessive service stresses and substandard mechanical properties. Recommendations included additional quality-control measures to provide better spheroidal graphite morphology at the frame surface.

In TAKR 300 (Bob Hope) Class transport ships, the builder observed cracking of steel cloverleaf vehicle tie-down deck sockets following installation. Sockets were made from AH36 steel plate by flame cutting and cold coining, then submerged-arc welded to the shop deck. Cracks initiated from the tip of the cloverleaf pattern in >300 cases aboard several cargo vessels in various stages of construction. Consultants who analyzed the situation concluded that the problem may have been corrosion and hydrogen embrittlement. Three possible mechanisms of failure were considered: overload failure; fatigue fracture; and, environmentally-assisted cracking. Testing indicated overload failure was the cause. Remedial actions were taken to improve the fracture properties of the deck socket. A modified manufacturing process was developed involving milling and cutting instead of coining to round the comers of the flame-cut cloverleaf lobe. This new manufacturing process solved the problem.