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differential scanning calorimetry

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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001593
EISBN: 978-1-62708-234-1
.... The techniques utilized included scanning electron microscopy, Fourier transform infrared spectroscopy, differential scanning calorimetry, thermomechanical analysis, and melt flow rate determination. It was the conclusion of the investigation that the part failed via brittle fracture, with evidence also...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003525
EISBN: 978-1-62708-180-1
..., contamination, degradation, chemical contact Differential scanning calorimetry (DSC) Heat of fusion, melting point, glass transition temperature, heat capacity Material identification, level of crystallinity, aging/degradation, thermal history Thermogravimetric analysis (TGA) Weight loss over...
Series: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001798
EISBN: 978-1-62708-241-9
...Abstract Abstract The crosslinked epoxy resin encapsulant protecting an electromagnetic valve coil failed during long-term storage and was examined to determine the cause. The investigation included fault-tree analysis, FTIR and EDX spectroscopy, and differential scanning calorimetry...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001901
EISBN: 978-1-62708-218-1
...Abstract Abstract Thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) were used to analyze an automotive polyoxymethylene (POM) sensor housing that was depolymerizing during service. It was found that a combination of heat, oxygen, and sulfuric acid attacked and caused...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c0090442
EISBN: 978-1-62708-218-1
... apparent in the results, suggestive of degradation of the failed part material. Differential scanning calorimetry was performed on the sleeve materials using a heat/cool/heat methodology. Testing of the reference material produced initial heating results indicative of a PBT resin, as illustrated...
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.homegoods.c0090457
EISBN: 978-1-62708-222-8
..., and the obtained spectrum exhibited absorption bands characteristic of a polyacetal resin. It is significant to note that polyacetal copolymers and homopolymers cannot be differentiated spectrally, and a melting point determination is often used to distinguish between these materials. Differential scanning...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.9781627081801
EISBN: 978-1-62708-180-1
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006759
EISBN: 978-1-62708-295-2
... Thermal analysis of polymeric materials can be used in conjunction with FTIR or Raman spectroscopy to confirm the chemistry of a polymeric material. Although methods such as differential scanning calorimetry and thermogravimetric analysis are used for ascertaining the mechanical and physical properties...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006757
EISBN: 978-1-62708-295-2
... Inherent viscosity, reduced viscosity, intrinsic viscosity Quasi-elastic light scattering (QELS) Macromolecular particle diameter, diffusion coefficient Differential thermal analysis (DTA) Transition temperature, T g ; melt/crystallization temperatures, T m Differential scanning calorimetry...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003522
EISBN: 978-1-62708-180-1
... methods Methods of thermal analysis Differential scanning calorimetry (DSC) and differential thermal analysis (DTA) Thermomechanical analysis Dynamic mechanical analysis Thermogravimetric analysis X-ray diffraction (XRD) analysis Further details of polymer characterization...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006782
EISBN: 978-1-62708-295-2
... Temperatures and Enthalpies of Fusion and Crystallization of Polymers by Differential Scanning Calorimetry ,” D 3418, Annual Book of ASTM Standards , ASTM International , 2019 5. Annual Book of ASTM Standards , ASTM International , 2019 6. Corrosion: Materials , Vol 13B , ASM Handbook...