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Current density needed to sustain a set cathodic protection potential as a ...
Available to PurchasePublished: 15 January 2021
Fig. 16 Current density needed to sustain a set cathodic protection potential as a function of iron sulfide present in biologically active soil box experiments under anaerobic conditions
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Scatter in Ir, the minimum current density, for service embrittled and de-e...
Available to Purchase
in Failure Analysis of a Set of 1CrMoV Studs From a Steam Turbine and Techniques for Its Assessment
> ASM Failure Analysis Case Histories: Power Generating Equipment
Published: 01 June 2019
Fig. 11 Scatter in Ir, the minimum current density, for service embrittled and de-embrittled stud.
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Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001624
EISBN: 978-1-62708-218-1
.... The findings suggested salt or salt water had leaked into the sensor and caused localized corrosion to the wire, possibly at an area where preexisting damage was present in the coating. Separation occurred in the wire when the current density at the reduced cross section caused excessive localized heating...
Abstract
An electronic sensor coil failed continuity testing, indicating that a break was present in the polymer-coated wire. An area of the wire showed a green discoloration and the break in the wire was located in this same region. The discoloration was suspected to be an indicator of what caused the failure. SEM/EDS and FTIR results showed the break in the coil wire was associated with corrosion. The corrosion debris contained relatively high levels of sodium and chlorine, which were likely in the form of salt. Some salt deposits were noted also in other areas along the wire surface. The findings suggested salt or salt water had leaked into the sensor and caused localized corrosion to the wire, possibly at an area where preexisting damage was present in the coating. Separation occurred in the wire when the current density at the reduced cross section caused excessive localized heating, which led to melting of the wire.
Book Chapter
Failure Analysis of a Set of 1CrMoV Studs From a Steam Turbine and Techniques for Its Assessment
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.power.c9001004
EISBN: 978-1-62708-229-7
... of grain boundary phosphorus segregation exhibited a good relationship with ambient temperature Charpy data. The electrochemical polarization kinetic reactivation, EPR, approach, however, proved disappointing in that the overlapping scatter in the minimum current density, Ir, for an embrittled and a non...
Abstract
The results of a failure analysis of a series of Cr-Mo-V steel turbine studs which had experienced a service lifetime of some 50,000 h are described. It was observed that certain studs suffered complete fracture while others showed significant defects located at the first stress bearing thread. Crack extension was the result of marked creep embrittlement and reverse temper embrittlement (RTE). Selected approaches were examined to assess the effects of RTE on the material toughness of selected studs. It was observed that Auger electron microscopy results which indicated the extent of grain boundary phosphorus segregation exhibited a good relationship with ambient temperature Charpy data. The electrochemical polarization kinetic reactivation, EPR, approach, however, proved disappointing in that the overlapping scatter in the minimum current density, Ir, for an embrittled and a non-embrittled material was such that no clear decision of the toughness properties was possible by this approach. The initial results obtained from small punch testing showed good agreement with other reported data and could be related to the FATT. Indeed, this small punch test, combined with a miniature sample sampling method, represents an attractive approach to the toughness assessment of critical power plant components.
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Schematic of the failure of spot welds to join a bracket to a baseplate ass...
Available to PurchasePublished: 01 January 2002
Fig. 56 Schematic of the failure of spot welds to join a bracket to a baseplate assembly. The failure was caused by inadequate welding current density resulting from extension of the electrode beyond the edge of the bracket flange.
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Book Chapter
Electrical Fluting Failure of a Tri-Lobe Roller Bearing
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001796
EISBN: 978-1-62708-241-9
... in bearings to minimize the effects of orbital slippage and rolling-contact fatigue. The damaged areas were examined under a scanning electron microscope, which revealed a high density of microcraters, characteristic of local melting and material removal associated with bearing currents. Investigators also...
Abstract
A tri-lobe cylindrical roller bearing was submitted for investigation to determine the cause of uniformly spaced axial fluting damages on its rollers and outer raceway surfaces. The rollers and raceways were made from premium-melted M50 and M50NiL, aircraft quality steels often used in bearings to minimize the effects of orbital slippage and rolling-contact fatigue. The damaged areas were examined under a scanning electron microscope, which revealed a high density of microcraters, characteristic of local melting and material removal associated with bearing currents. Investigators also examined the effect of electrical discharge on crater dimensions and density and the role that thermoelectric voltage potentials may have played.
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001514
EISBN: 978-1-62708-218-1
... in a visual inspection of the welds themselves. The defective welds were formed due to inadequate current density (possibly in conjunction with inadequate welding time). This is consistent with the microstructure in Figure 9 . It is not known whether the lack of appropriate current density was due...
Abstract
A front-wheel drive hatchback automobile was involved in a severe front end impact. Failure analysis of the automobile revealed only a single sound spot weld in each of two 66 cm (26 in.) sections of both upper and lower floor sill flanges. Consequently, upon impact, the floor pan separated from the rocker panel, buckled and rotated upward and forward. This introduced slack in the seat belts since their retractors, being anchored to the floor pan, also rotated forward. Although not contributory to the accident itself, the faulty welds were responsible in part for the severity of the injuries sustained by the driver. The faulty welds in the unit body were apparently a consequence of improper settings of parameters on a multihead electrical resistance spot welding machine. Lack of appreciation of the hazard associated with failure of this weldment may have contributed to the low frequency of their physical inspection during production. A similar case involving faulty welds in a fuel delivery truck is also discussed.
Book Chapter
Failure of a Squeeze-Clamped Polyethylene Natural Gas Pipeline
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001275
EISBN: 978-1-62708-215-0
... Abstract A high-density polyethylene (HDPE) natural gas distribution pipe (Grade PE 3306) failed by slow, stable crack growth while in residential service. The leak occurred at a location where a squeeze clamp had been used to close the pipe during maintenance. Failure analysis showed...
Abstract
A high-density polyethylene (HDPE) natural gas distribution pipe (Grade PE 3306) failed by slow, stable crack growth while in residential service. The leak occurred at a location where a squeeze clamp had been used to close the pipe during maintenance. Failure analysis showed that the origin of the failure was a small surface crack in the inner pipe wall produced by the clamping. Fracture mechanics calculations confirmed that the suspected failure process would result in a failure time close to the actual time to failure. It was recommended that: materials be screened for susceptibility to the formation of the inner wall cracks since it was not found to occur in pipe typical of that currently being placed in service; pipes be re-rounded after clamp removal to minimize residual stresses which caused failure; and a metal reinforcing collar be placed around the squeeze location after clamp removal.
Book Chapter
Catastrophic Failure of a Fan in a Diesel Engine Cooler
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.auto.c9001612
EISBN: 978-1-62708-218-1
... of the nugget indicated that the weld penetration is non-uniform across the section and is higher at the top electrode when compared to the lower electrode ( Fig. 2b ). The inadequate penetration may result from too low a current density in the weld or other improper weld process variables...
Abstract
The fan used to cool a diesel engine fractured catastrophically after approximately 100 h of operation. The fan failed at a spider, which was resistance spot welded to a shim placed between two circular spiders of 3 mm thickness. The detailed analysis of the fracture indicated that the premature failure of the fan was due to inadequate bonding between the sheets at the weld nugget. The fracture was initiated from the nugget-plate interface. The inadequate penetration and lack of fusion between the steel sheets during resistance spot welding led to poor weld strength and the fracture during operation. The propensity to crack initiation and failure was accentuated by improper cleaning of the surfaces prior to welding and to inadequate nugget-to-sheet edge distance.
Series: ASM Failure Analysis Case Histories
Volume: 2
Publisher: ASM International
Published: 01 December 1993
DOI: 10.31399/asm.fach.v02.c9001296
EISBN: 978-1-62708-215-0
... current density. It was also possible that short circuiting led to high-temperature melting. Conclusion and Recommendations Most Probable Cause The brittle cracking of the valve guide was caused by low-cycle fatigue, which was attributed to the presence of a pre-existing crack in the outer...
Abstract
A 52000 bearing steel valve guide component operating in the fuel supply system of a transport aircraft broke into two pieces after 26 h of flight. The valve guide fractured through a set of elongated holes that had been electrodischarge machined into the component. Analysis indicated that the part failed by low cycle fatigue. The fracture was brittle in nature and had originated at a severely eroded zone of craters in a hard, deep white layer that was the result of remelting during electrodischarge machining. It was recommended that the remaining parts be inspected using a stereoscopic microscope and/or a borescope.
Book Chapter
Series: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c0048791
EISBN: 978-1-62708-234-1
...-improvement treatment, the oxalic acid etch test, Practice A of ASTM A 262 ( Ref 2 ), was implemented. The polished specimen was etched at a current density of 1 A/cm 2 (6.5 A/in. 2 ) for 1.5 min in 10% oxalic acid-demineralized water, using a piece of type 304 stainless steel as the anode...
Abstract
Linear indications on the outer surface of a cross in a piping system were revealed by dye-penetrant examination. The cross was specified to be SA403 type WP 304 stainless steel. The cross had been subjected to induction-heating stress improvement. The linear indications on the cross were located in wide bands running circumferentially below the cross-to-cap weld and above the cap-to-discharge-pipe weld. The material was found to conform to the requirements both in terms of hardness and strength. Intergranular cracks filled with oxide were observed on metallographic analysis of a sectioned and oxalic acid etched sample. The grain size was found to exceed the ASTM standard. No indications of sensitization were observed during testing with practice A of ASTM A 262. Definitive evidence of contaminants to support SCC as the failure mechanism was not disclosed during analysis. It was concluded that overheating or burning of the forging, which classically results in large grain size, intergranular fractures, and fine oxide particles dispersed throughout the grains was the possible reason for the failure.
Book Chapter
Corrosion Failure of Stainless Steel Tanks
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 1
Publisher: ASM International
Published: 01 December 1992
DOI: 10.31399/asm.fach.v01.c9001068
EISBN: 978-1-62708-214-3
... from the cut section of the dished end and from the parent metal of the shell plate. Both showed a typical solution-annealed structure ( Fig. 5 ) after electrolytic etching in 10% ammonium persulfate at a current density of 1 A/cm 2 (6.45 A/in. 2 ) for 5 min. Fig. 5 Typical microstructure...
Abstract
Four tanks made from type 304L stainless steel were removed from storage. Atmospheric corrosion on the outside of the tanks and pitting and crevice corrosion on the inside were visible. Metallographic examination revealed that the internal corrosion had been caused by crevices related to weld spatter and uneven weld deposit and by service water that had not been drained after hydrostatic testing. External corrosion was attributed to improper passivation. It was recommended that the surfaces be properly passivated and that, before storage, the interiors be rinsed with demineralized water and dried.
Book Chapter
Failure Analysis of Welded Low-Carbon Steel Storage Tank
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.chem.c9001525
EISBN: 978-1-62708-220-4
... to the surface. After the potential has been raised well above the OCP, it is again decreased until the test is finally terminated. The resulting test curve shows the range of potentials and the resulting current density at each potential. This curve provides the overall corrosion rate, and can be used...
Abstract
Welded steel storage vessels used to hold mildly alkaline solution were produced in exactly the same manner from deep-drawn aluminum-killed SAE 1006 low-carbon steel sheet. After the cylindrical shell was drawn, a top low-carbon steel closure was welded to the inside diameter. The containers were then filled with the slightly alkaline solution, pressurized, and allowed to stand under ambient conditions. A small number, less than 1%, were returned because they began to leak in service. Inspection revealed general corrosion and pitting on the inner surfaces. However, other tanks that experienced the same service conditions developed no corrosion. Corrosion was linked to forming defects that provided sites for localized corrosion, and to lack of steam drying after cleaning, which increased susceptibility to general corrosion.
Book Chapter
Failure of Stainless Steel Piping in Stagnant Seawater
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.marine.c0091394
EISBN: 978-1-62708-227-3
... forces and identical regarding the corrosion reactions. Macroscopic geometry determines the category. These austenitic stainless steels can be active or passive in adjacent areas on the same part or pipe. Because of the relatively large surface area of the cathode and hence the low current density...
Abstract
An austenitic stainless steel (type 316/316L stainless steel, schedule 40, 64 mm (2.5 in.) diam and larger) piping network used in the fire-sprinkler system in a large saltwater passenger and car ferry failed by rapid leaking. Operating conditions involved stagnant seawater at ambient temperatures. The pipe was in service for four weeks when three leaks appeared. Investigation (visual inspection and photographic images) supported the conclusion that the failure was caused by attack and corrosion damage of Cl ions in conditions that were ideal for three modes of highly accelerated pitting of austenitic stainless steel: the bottom surface, weld or HAZ pits, and crevices. Recommendations included proper material selection for piping, flanges, and weld rods with greater corrosion resistance. Proper filtering to prevent entrained abrasives and timely breakdown inspections were also advised.
Book Chapter
Failure Analysis of Computer Data Storage Disc Drive Systems
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Publisher: ASM International
Published: 01 June 2019
DOI: 10.31399/asm.fach.modes.c9001516
EISBN: 978-1-62708-234-1
.... These trends are shown in Fig. 1 . Fig. 1 Trends in flying heights and recording densities Current flying heights in high-density drives are as small as 6 micro inches (0.15 micron) and attempts are now being made to further reduce it to 2–4 microins (0.05–0.1 micron) since high densities demand...
Abstract
This paper deals with disk drive failures that occur in the interface area between the head and disk. The failures often lead to the loss of stored data and are characterized by circumferential microscratches that are usually visible to the unaided eye. The recording media in disk drives consists of a metal, glass, ceramic, or plastic substrate coated with a magnetic material. Data errors are classified as ‘soft’ or ‘hard’ depending on their correctability. Examination has shown that hard errors are the result of an abrasive wear process that begins with contact between head and disk asperities. The contact generates debris that, as it accumulates, increases contact pressure between the read-write head and the surface of the disk. Under sufficient pressure, the magnetic coating material begins wearing away, resulting in data loss.
Book Chapter
Nondestructive Testing in Failure Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006764
EISBN: 978-1-62708-295-2
... of detecting surface discontinuities by magnetic-particle inspection, liquid penetrant inspection, and eddy-current testing. The major NDE methods for internal (volumetric) inspection in failure analysis also are described. eddy-current testing liquid penetrant inspection magnetic-particle inspection...
Abstract
Nondestructive testing (NDT), also known as nondestructive evaluation (NDE), includes various techniques to characterize materials without damage. This article focuses on the typical NDE techniques that may be considered when conducting a failure investigation. The article begins with discussion about the concept of the probability of detection (POD), on which the statistical reliability of crack detection is based. The coverage includes the various methods of surface inspection, including visual-examination tools, scanning technology in dimensional metrology, and the common methods of detecting surface discontinuities by magnetic-particle inspection, liquid penetrant inspection, and eddy-current testing. The major NDE methods for internal (volumetric) inspection in failure analysis also are described.
Book Chapter
Failure Analysis of a Crimping Mechanism
Available to PurchaseSeries: ASM Failure Analysis Case Histories
Volume: 3
Publisher: ASM International
Published: 01 December 2019
DOI: 10.31399/asm.fach.v03.c9001783
EISBN: 978-1-62708-241-9
.... While the tip cracking no longer took place, the square roller as mentioned above was wearing out at a rate that was very unsatisfactory. At this point there were several material changes and one design change to remediate current issues; however, because of their interdependence this caused a new set...
Abstract
An aluminum bronze bushing that serves as a guide in a crimping machine began to fail after 50,000 cycles or approximately two weeks of operation. Until then, typical run times had been on the order of months. Although the bushings are replaceable and relatively inexpensive, the cost of downtime adds up quickly while operators troubleshoot and swap out worn components. Initially, the quality of the bushings came into question, but after a detailed analysis of the entire crimping mechanism, several other issues emerged that were not previously considered. As a result, the investigation provides information on not only better materials, but also design changes intended to reduce wear and increase service life.
Book Chapter
Corrosive Wear Failures
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003567
EISBN: 978-1-62708-180-1
... impart two-body wear damage to component parts. They are not constrained by another solid, as distinguished from grinding, which is discussed later. Abrasive Particle Characteristics Abrasive particle characteristics, such as shape, density, size, hardness, and their relation to wear rate...
Abstract
This article focuses on the corrosion-wear synergism in aqueous slurry and grinding environments. It describes the effects of environmental factors on corrosive wear and provides information on the impact and three-body abrasive-corrosive wear. The article also discusses the various means for combating corrosive wear, namely, materials selection, surface treatments, and handling-environment modifications.
Book Chapter
Electrical Testing and Characterization of Plastics
Available to PurchaseSeries: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006913
EISBN: 978-1-62708-395-9
... 15 mm (0.6 in.) inside the edges of the electrodes. (h) The Type 7 electrodes, as described in the table and in Note (g), are those given in IEC Publication 243-1 for making tests parallel to the surface. Using Alternating Current A commonly used test method is ASTM D149 for measuring...
Abstract
This article addresses electrical testing and characterization of plastics and presents a number of techniques for evaluating the electrical properties of insulating materials, with a special focus on plastics, accompanied by a list of the electrical properties of different types of plastics. It provides the reader with sufficient information to select the appropriate electrical test(s) for a specific application. The tests covered in this article are widely used in industry to determine the electrical properties of insulating materials, particularly plastics. The article lists and defines terms used in connection with testing and specification of plastics for electrical applications.
Book Chapter
Failures Related to Welding
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003509
EISBN: 978-1-62708-180-1
... requirements of a particular welded structure as well as on the properties of the material involved. A number of different fitness-for-service assessment methodologies for calculating allowable or critical flaw sizes are currently in use, as described in the section “Fitness-for-Service Codes...
Abstract
This article briefly reviews the general causes of weldment failures, which may arise from rejection after inspection or failure to pass mechanical testing as well as loss of function in service. It focuses on the general discontinuities observed in welds, and shows how some imperfections may be tolerable and how the other may be root-cause defects in service failures. The article explains the effects of joint design on weldment integrity. It outlines the origins of failure associated with the inherent discontinuity of welds and the imperfections that might be introduced from arc welding processes. The article also describes failure origins in other welding processes, such as electroslag welds, electrogas welds, flash welds, upset butt welds, flash welds, electron and laser beam weld, and high-frequency induction welds.
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