In a steel foundry, tensile and bend specimens of castings made in a 2-ton basic arc furnace showed, at irregular intervals, regions with coarse-grained fractures where the specimens broke prematurely, so that the specified strength and toughness values could not be reached. Several cast tensile specimens and some forcibly-broken pieces of the flanges of armature yokes made of cast steel GS C 25 according to DIN 17 245 were investigated. Microscopic examination showed that the cause of damage was the superabundant use of aluminum as deoxidizer. According to recommendations, the aluminum addition was reduced by one-half. Since then, there have been no additional rejects due to insufficient tensile and bend values.

An investigation of wear and failure of babbitt bushes was completed in this study. The results showed that wear at dry sliding of babbitt obtained by plasma spraying was less than that of babbitt in the as-cast state and after a deformation heat treatment. The failure of babbitt bushes was caused by a simultaneous and interrelated exhibition of fatigue and wear processes that depend considerably on cohesion strength between the bush and the bearing base and accumulation of defects on the contact surface between the bush and the shaft.

Two cases of failure of centrifuge baskets were investigated. The first involved a centrifuge running at approximately 1000 rpm. The basket was constructed from a perforated sheet of stainless steel rolled into a cylinder and joined by a single vee longitudinal weld. Detailed examination showed the weld had not completely penetrated the full depth of the section. The fracture faces showed a gradually progressing fatigue crack developing from a notch, formed by the lack of penetration, at the root of the weld. Microscopic examination of the parent plate showed it was a typical titanium stabilized austenitic steel. It is probable that had the basket been subjected to a periodic inspection by a competent person, this failure would not have occurred. The second case concerned a continuous duty centrifuge operating at 2200 rpm. Fracture had occurred at the circumferential weld attaching the stainless steel skirt to the basket rim and also in the region of the vertical weld which was made when the skirt was formed into a cone. Stress-corrosion cracking of the skirt material, which contained residual stresses due to cold-rolling, had been caused by the presence of sodium chloride.

This article describes the visual, fractographic, and metallographic evidence typically encountered when analyzing stress rupture of turbine airfoils. Stress-rupture fractures are generally heavily oxidized, tend to be rough in texture, and are primarily intergranular and/or interdendritic in appearance compared to smoother, transgranular fatigue type fractures. Often, gross plastic yielding is visible on a macroscopic scale. Commonly observed microstructural characteristics include creep voiding along grain boundaries and/or interdendritic regions. Internal voids can also nucleate at carbides and other microconstituents, especially in single crystal castings that do not possess grain boundaries.

After several years' use, an eyebolt suffered brittle fracture in the first turn of the thread. The fracture started at the notch at the root of the thread. Neither localized material defect nor an old crack were present. The investigation showed that instead of the specified steel quality St 37-2 N, a steel with about 0.5% C had been used. The microstructure with the coarse ferrite network indicated that the forged eye bolt had been normalized either at too high a temperature or not at all. In any case the anneal at 900 deg C produced a considerably more finely grained structure. In addition, the nature of the fracture and the results of the notched bar impact tests showed that in spite of the high C-content, the eye bolt had become brittle as a result of aging.

This article provides a description of the microscale models and mechanisms for deformation and fracture. Macroscale and microscale appearances of ductile and brittle fracture are discussed for various specimen geometries and loading conditions. The article reviews the general geometric factors and materials aspects that influence the stress-strain behavior and fracture of ductile metals. It highlights fractures arising from manufacturing imperfections and stress raisers. The article presents a root cause failure analysis case history to illustrate some of the fractography concepts.

This article focuses on characterizing the fracture-surface appearance at the microscale and contains some discussion on both crack nucleation and propagation mechanisms that cause the fracture appearance. It begins with a discussion on microscale models and mechanisms for deformation and fracture. Next, the mechanisms of void nucleation and void coalescence are briefly described. Macroscale and microscale appearances of ductile and brittle fracture are then discussed for various specimen geometries (smooth cylindrical and prismatic) and loading conditions (e.g., tension compression, bending, torsion). Finally, the factors influencing the appearance of a fracture surface and various imperfections or stress raisers are described, followed by a root-cause failure analysis case history to illustrate some of these fractography concepts.

This study examines the role of calcium-precipitating bacteria (CPB) in heat exchanger tube failures. Several types of bacteria, including Serratia sp. (FJ973548), Enterobacter sp. (FJ973549, FJ973550), and Enterococcus sp. (FJ973551), were found in scale collected from heat exchanger tubes taken out of service at a gas turbine power station. The corrosive effect of each type of bacteria on mild steel was investigated using electrochemical (polarization and impedance) techniques, and the biogenic calcium scale formations analyzed by XRD. It was shown that the bacteria contribute directly to the formation of calcium carbonate, a critical factor in the buildup of scale and pitting corrosion on heat exchanger tubes.

Cluster bomb tailcone assemblies each containing two aluminum die-cast components were rejected because of the poor surface condition of the die castings. Numerous heat checks were found on the surfaces of the tailcones and radiographic inspection revealed inclusions, gas holes, and shrinkage defects in the castings. Most of the components failed to meet required mechanical properties because of these casting defects.

Various aluminum bronze valves and fittings on the essential cooling water system at a nuclear plant were found to be leaking. The leakage was limited to small-bore socket-welded components. Four specimens were examined: three castings (an ASME SB-148 CA 952 elbow from a small-bore fitting and two ASME SB-148 CA 954 valve bodies) and an entire valve assembly. The leaks were found to be in the socket-weld crevice area and had resulted from dealloying. It was recommended that the weld joint geometry be modified.

A locomotive type boiler was fitted with a copper firebox of orthodox construction. Flanged tube- and firehole-plates were attached to a wrapper plate by means of copper rivets. Shortly after it was put into service the fireside heads of a number of rivets broke off at different parts of the seams. By the time the investigation was begun a total of fifty heads had broken off. Repairs had been effected from time to time by fitting screwed rivets, none of which gave trouble in service. Microscopic examination confirmed the fracture path to be wholly intergranular. In the region of the fracture the grain boundaries were delineated as a near-continuous network of cavities and films of oxide. It was evident that the failure of the rivets in service was attributable to intergranular weakness in the material due to gassing.

X-ray spectroscopy is generally accepted as the most useful ancillary technique that can be added to any scanning electron microscope (SEM), even to the point of being considered a necessity by most operators. While “stand-alone” x-ray detection systems are used less frequently in failure analysis than the more exact instrumentation employed in SEMs, the technology is advancing and is worthy of note due to its capability for nondestructive analysis and application in the field. This article begins with information on the basis of the x-ray signal. This is followed by information on the operating principles and applications of detectors for x-ray spectroscopy, namely energy-dispersive spectrometers, wavelength-dispersive spectrometers, and handheld x-ray fluorescence systems. The processes involved in x-ray analysis in the SEM and handheld x-ray fluorescence analysis are then covered. The article ends with a discussion on the applications of x-ray spectroscopy in failure analysis.

During the lifting of a piece of machinery by means of an overhead travelling crane the hook fractured suddenly. The load was attached to the hook by means of fiber rope slings and rupture occurred in a plane which appeared to coincide with the sling loop nearest to the back of the hook. The rated capacity of the crane was 15 tons. At the time of the mishap it was being used to lift one end of a hydraulic cylinder with a total weight of about 27 tons. Fracture was of the cleavage type throughout. There was no evidence of any prior deformation of the material in the vicinity, nor was there any indication of a pre-existing crack or major discontinuity at the point of origin. A sulfur print suggested the hook had been forged from a billet cogged down from an ingot of semi-killed steel. Failure of this hook was attributed to strain-age embrittlement of the material at the surface of the intrados.

Fundamentals of fatigue failure are outlined. Addressed are fatigue crack characteristics, basic crack types, unidirectional bending, alternate bending, rotary bending, torsion, direct stress, and combined stress. Stress cycle, endurance limits, under and overstressing, stress concentration, and surface condition are discussed. Sections are devoted to fatigue crack assessment, corrosion relation to fatigue failure, and the micro-mechanisms of fatigue failure. Materials considered include steels. Photographs of service failures are used to illustrate features alluded to in the text.

Following disruption of the austenitic stainless steel basket of a hydro-extractor used for the separation of crystals of salt (sodium chloride) from glycerin, samples of the broken parts were analyzed. Examination revealed that the fish-plates joining the reinforcing hoops had broken, the shell had split from top to bottom adjacent to the weld, the top and bottom cover plates had become loose, all the rivets having pulled out, and the shaft was also found to be bent. Fracture took place in an irregular manner and was of the shear type towards both ends; it occurred immediately adjacent to the weld or a short distance from it and on alternate sides. Microscopical examination did not reveal any intergranular carbide precipitation, such as is well known to result in the weld-decay mode of failure. It was concluded that the primary cause of failure was stress-corrosion cracking arising from the combined effect of residual stresses and the corrosive effect of the material being centrifuged. If the shell had been stress-relieved after fabrication, the failure likely would not have occurred.

An octagonal steel ingot weighing 13 tons made of manganese-molybdenum steel developed gaping cross-cracks on all eight sides in the forging press during initial pressure application. It was reported that the steel had been melted in a basic 12-ton arc furnace, oxygenated, furnished with 42 kg of 75% ferrosilicon and 12 kg aluminum additions, alloyed with 160 kg of 80% ferromanganese, and finally deoxidized in the ladle with 42 kg calcium silicon. For metallographic examination a plate approximately 100 mm thick was cut parallel to one of the eight planes. Platelet-like particles could be discerned on the conchoidal fracture planes with the SEM. The precipitates proved to be thin and partially transparent platelets of a hexagonal crystal lattice whose parameters resemble those of AIN. The precipitates were at least in part still undissolved in spite of the long holding period at high initial forging temperature. Another block melted under the same conditions and immediately after the defective one, was forged into a gear ring without any trouble. This ring was free of grain boundary precipitates, but it contained only 0.012 % AI and 0.0102 % N.

Several of the aluminum alloy 6061-T6 drawn seamless tubes (ASTM B 234, 2.5 cm (1.0 in.) OD with wall thickness of 1.7 mm (0.065 in.)) connecting an array of headers to a system of water-cooling pipes failed. The tubes were supplied in the O temper. They were bent to the desired curvature, preheated, then solution treated, water quenched, and then aged for 8 to 10 h. Analysis (visual inspection, slow-bend testing, 65x macrographic analysis, macroetching, spectrographic analysis, hardness tests, microhardness tests, tension tests, and microscopic examination) supported the conclusions that bending of the connector tubes in the annealed condition induced critical strain near the neutral axis of the tube, which resulted in excessive growth of individual grains during the subsequent solution treatment. Recommendations included bending the connector tubes in the T4 temper as early as possible after being quenched from the solution temperature. The tubes should be stored in dry ice after the quench until bending can be done. The tubes should be aged immediately after being formed. Flattening and slow-bend tests should be specified to ensure that the connector tubes had satisfactory ductility.

Thermomechanical fatigue (TMF) is the general term given to the material damage accumulation process that occurs with simultaneous changes in temperature and mechanical loading. TMF may couple cyclic inelastic deformation accumulation, temperature-assisted diffusion within the material, temperature-assisted grain-boundary evolution, and temperature-driven surface oxidation, among other things. This article discusses some of the major aspects and challenges of dealing with TMF life prediction. It describes the damage mechanisms of TMF and covers various experimental techniques to promote TMF damage mechanisms and elucidate mechanism coupling interactions. In addition, life modeling in TMF conditions and a practical application of TMF life prediction are presented.

A drawing plant which processed steel wire of designation 105 Cr 2 for ball bearings had losses due to crack formation and wire breakage during drawing. To establish the reason for the breakage, seven fractures were submitted for investigation with contiguous wire segments on both sides of the fracture of 300 mm each. Missing in the lamellar surface structure, with the exception of the remnants of a coarse network, were the pre-eutectically precipitated carbides to be expected in this steel. Surrounding the ferritic region in the surface structure, a ring of lamellar pearlite is seen, which turns into the granular annealed structure towards the core. The described structural phenomena were noted in all of the seven fracture regions. Their intensity always decreased with increasing distance from the fracture. Surface decarburization caused the formation of lamellar pearlite during annealing. This investigation further revealed that the localized decarburization and pearlite formation was present already in the rolled wire in uneven distribution over the entire coil length.

Cracking occurred within the plastic jacket (injection molded from an impact-modified, 15% glass-fiber-reinforced PET resin.) of several assemblies used in a transportation application during an engineering testing regimen which involved cyclic thermal shock (exposing the parts to alternating temperatures of -40 and 180 deg C (-40 and 360 deg F)). Prior to molding, the resin had reportedly been dried at 135 deg C (275 deg F). The drying process usually lasted 6 h, but occasionally, the material was dried overnight. Comparison investigation (visual inspection, 20x SEM views, micro-FTIR, and analysis using DSC and TGA) with non-failed parts supported the conclusion that that the failure was via brittle fracture associated with the exertion of stresses that exceeded the strength of the resin as-molded caused by the disparity in the CTEs of the PET jacket and the mating steel sleeve. The drying process had exposed the resin to relatively high temperatures, which caused substantial molecular degradation, thus limiting the part's ability to withstand the stresses. The drying temperature was found to be significantly higher than the recommendation for the PET resin, and the testing itself exposed the parts to temperatures above the recognized limits for PET.