The center portions of two adjacent low-carbon steel boiler tubes (made to ASME SA-192 specifications) ruptured during a start-up period after seven months in service. It was indicated by reports that there had been sufficient water in the boiler two hours before start-up. The microstructure near the rupture edge was revealed by metallographic examination to consist of ferrite and acicular martensite or bainite. The microstructure and the observed lack of cold work indicated a temperature above the transformation temperature of 727 deg C had been reached. Swelling of the tubes was disclosed by the wall thickness and OD of the tubing. The tubes were concluded to have failed due to rapid overheating.

Compound bow handle risers that had failed in service and during assembly along with an unassembled riser were submitted for analysis. The risers were die cast from magnesium-base alloy AM60A. Inspection of the failed risers and metallurgical investigations conducted on the stock riser revealed the presence of cold shuts at the same site in all specimens. It was recommended that all risers be thoroughly inspected and that the bow company work with their die casting shop to design a mold with acceptable filling characteristics.

This article describes the general root causes of failure associated with wrought metals and metalworking. This includes a brief review of the discontinuities or imperfections that may be the common sources of failure-inducing defects in bulk working of wrought products. The article discusses the types of imperfections that can be traced to the original ingot product. These include chemical segregation; ingot pipe, porosity, and centerline shrinkage; high hydrogen content; nonmetallic inclusions; unmelted electrodes and shelf; and cracks, laminations, seams, pits, blisters, and scabs. The article provides a discussion on the imperfections found in steel forgings. The problems encountered in sheet metal forming are also discussed. The article concludes with information on the causes of failure in cold formed parts.

A clamp used for securing the hot-air ducting system on fighter aircraft fractured in an area adjacent to a slot near the end of the strap after two or three years of service. The strap was 0.8 mm (0.032 in.) thick, and the V-section was 1.3 mm (0.050 in.) thick; both were made of 19-9 DL heat-resisting alloy. The operating temperature of the duct surrounded by the clamp was 425 to 540 deg C (800 to 1000 deg F). The life of the clamp was expected to equal that of the aircraft. Investigation (visual inspection, chemical analysis, hardness testing, and 540x/2700x images etched with oxalic acid) supported the conclusion that the clamp fractured by SCC because the work metal was sensitized. Sensitization occurred during long-term exposure to the service temperature; the effects of sensitization were intensified as a result of cold forming. Recommendations included using a work metal that is less susceptible to intergranular carbide precipitation.

An integral coupling and gear (Cr-Mo steel), used on a turbine-driven main boiler-feed pump, was removed from service after one year of operation because of excessive vibration. Spectrographic analysis and metallographic examination revealed the fact that gritty material in the gear teeth (found at visual inspection) was composed of the same material as the metal in the coupling. Beach marks and evidence of cold work, typical of fatigue failure, were found on the fracture surface. Chips remaining in the analysis cut were difficult to remove, indicating a strong magnetic field in the part. Evidence found supports the conclusions that failure of the coupling was by fatigue and that incomplete demagnetization of the coupling following magnetic-particle inspection caused retention of metal chips in the roots of the teeth. Improper lubrication caused gear teeth to overheat and spall, producing chips that eventually overstressed the gear, causing failure. Because the oil circulation system was not operating properly, metal chips were not removed from the coupling. Recommendations included checking the replacement coupling for residual magnetism and changing or filtering the pump oil to remove any debris.

A cold-formed Grade TP 304 stainless steel swaged region of a reheater tube in service for about 8000 hours cracked because of sulfur-induced stress-corrosion cracking (SCC). Cracking initiated from the external surface and a high sulfur content was detected in the outer diameter and crack deposits. Comparison of the microstructure and hardness of the swaged region and unswaged Grade TP 304 stainless steel tube metal indicated that the swaged section was not annealed to reduce the effects of cold working. The high hardness created during swaging increased the stainless steel's susceptibility to sulfur-induced SCC. Because SCC requires water to be present, cracking most likely occurred during downtime or startups. To prevent future failures, the boiler should be kept dry during downtime to avoid formation of sulfur acids, and the swaged sections of the tubes should be heat treated after swaging to reduce or eliminate strain hardening of the metal.

A heavily worked 304 stainless steel wire basket recrystallized and distorted while in service at 650 deg C (1200 deg F). This case study demonstrates that heavily cold worked austenitic stainless steel components can experience large losses in creep strength, and potentially structural collapse, under elevated temperature service, even at temperatures more than 300 deg C (540 deg F) below the normal solution annealing temperature. The creep strength of the recrystallized 304/304L steel was more than 1000 times less than that achievable with solution annealed 304H. These observations are consistent with limitations (2000 Addendum to ASME Boiler and Pressure Vessel Code) on the use of cold worked austenitic stainless steels for elevated temperature service.

Two tanks made of AISI type 304 stainless steel exhibited cracking in the heat-affected zone (HAZ) of the weld that joined the dished end and the shell. The dished ends had been produced by cold deformation. Hardness measurement and simulation tests showed that the deformation was equivalent to a 30% reduction in thickness. Residual stresses were measured at about 135 MPa (20 ksi). The HAZ was found to be sensitized. The tanks had been stored in a coastal atmosphere for about 4 years before installation. The failure was attributed to intergranular stress-corrosion cracking in a sensitized HAZ due to chloride from the environment. Use of low-carbon type AISI 304L was recommended. Minimization of fit-up stresses and covering with polyethylene sheets during storage were also suggested.

Several type 316L stainless steel wires in an electrostatic precipitator at a paper plant fractured in an unexpectedly short time. Failed wires were examined using optical and scanning electron microscope, and hardness tests were conducted. Fractography clearly established that fracture was caused by fatigue originating at corrosion pits on the surface of the wire. It was recommended that higher-molybdenum steel in the annealed condition be used to combat pitting corrosion.

Forged austenitic steel rings used on rotor shafts in two 100,000 kW generators burst from overstressing in a region of ventilation holes. A variety of causes contributed to the brittle fractures in the ductile austenitic alloy, including stress concentration by holes, work hardened metal in the bores, and a variable pattern of residual stress.

A blade from the engine cooling fan of a pickup truck fractured unexpectedly. The blade was made from type 301 stainless steel in the extra full hard tempered condition with a hardness of 47 HRC. Failure analysis indicated that the blade fractured in three modes: crack initiation, fatigue crack propagation, and final rapid fracture in a ductile manner The fatigue crack originated near a rivet hole.

Leakage which developed from two storage vessels handling a mixture of trimethyl formate and chloroform took place from the dished head at the edge of the circumferential weld to the shell which incorporated a backing ring. Some shallow pitting had occurred under the backing ring on the shell side behind the tack welds securing the backing strip to the shell. Intermittent pitting had also occurred along the head side of the weld at the other end the vessel. There was no pitting along the main longitudinal weld of the shells in any vessel nor around any of the branches set into the shells. The material of the original vessels was specified as BS 970 - 1966. En 58J. Sections taken through pitted areas from both head welds showed preferential attack along the grain-boundaries, some grains becoming completely detached. The location of the pitting and preferential attack was at such a distance from the weld that the heat of welding could have raised the metal temperature to 550 to 700 deg C (1292 deg F). The corrosion of the shell material which occurred at the shell side of the weld under the backing ring is also an example of crevice corrosion.

Two water pumps were taken out of service because of reduced output. Visual inspection revealed considerable material loss in both impellers, which were 25.4 cm (10 in.) in diam x 1.3 cm (0.5 in.) wide and made from a cast bronze alloy. Several similar water pumps operating under nearly identical conditions, drawing water from an open tank through a standpipe, had no observable failures. Etched micrographs 100x of samples taken from the impellers showed clean, pockmarked, severely eroded surfaces, characteristic of cavitation damage. Investigation also revealed that considerable quantities of air were being drawn into the system when water in the supply tank dropped below a certain level. It was concluded that cavitation erosion (due to the uptake of air) caused metal removal and microstructural damage in the impellers. Recommendations included adding a water-level control to the piping system and excluding air from the pump inlet.

Two of four adjustable Moore pins, which had been used to stabilize a proximal femur fracture, were found to be broken and deformed at their threads. The pins were made from a cobalt-chromium alloy and were not in the same condition. Brittle precipitates in the grains and grain boundaries were seen in one of the pins and hence the fracture was revealed to have occurred along the grain boundaries. The other pin made from cold-worked cobalt-chromium alloy was observed to have randomly lines of primary inclusions. Intermingled dimples and fatigue striations were exhibited on the fracture surface of this pin. Thus, the effect of different conditions of cobalt-chromium alloys on failure behavior was demonstrated as a result of this study.

Two type 316L stainless steel orthopedic screws broke approximately 6 weeks after surgical implant. The screws had been used to fasten a seven-hole narrow dynamic compression plate to a patient's spine. The broken screws and screws of the same vintage and source were examined using macrofractography, SEM fractography, and hardness testing. Fractography established that fracture was by fatigue and that the fatigue cracking originated at corrosion pits. Hardness while below specification, still indicated that the screws were in the cold-worked condition and notch sensitive during fatigue loading. Use of a steel with a higher molybdenum content (317L) in the annealed condition was recommended.

Following disruption of the austenitic stainless steel basket of a hydro-extractor used for the separation of crystals of salt (sodium chloride) from glycerin, samples of the broken parts were analyzed. Examination revealed that the fish-plates joining the reinforcing hoops had broken, the shell had split from top to bottom adjacent to the weld, the top and bottom cover plates had become loose, all the rivets having pulled out, and the shaft was also found to be bent. Fracture took place in an irregular manner and was of the shear type towards both ends; it occurred immediately adjacent to the weld or a short distance from it and on alternate sides. Microscopical examination did not reveal any intergranular carbide precipitation, such as is well known to result in the weld-decay mode of failure. It was concluded that the primary cause of failure was stress-corrosion cracking arising from the combined effect of residual stresses and the corrosive effect of the material being centrifuged. If the shell had been stress-relieved after fabrication, the failure likely would not have occurred.

Several surgical tool failures were analyzed to understand why they occur and how to prevent them. The study included drills, catheters, and needles subjected to the rigors of biomedical applications such as corrosive environments, high stresses, sterilization, and improper cleaning procedures. Given the extreme conditions to which surgical tools can be exposed, and the potential for misuse, failures are inevitable and systematic methods for analyzing them are necessary to keep them in check.

A spoon that was twisted and broken by a person claiming to possess parapsychic powers was submitted for failure analysis. Exemplar tests were conducted on material taken from the bowl region of the same spoon. In addition, tests on other unbroken samples of spoons were evaluated in order to establish both macroscopic and microscopic comparative behavior. These controlled tests produced known failure mechanisms and their respective fracture morphology in this material. A direct comparison could then be made with the unknown failure. The paper identifies a method of analysis that should be applied when analyzing failures of unknown origin.

A portable propane container with a name-plate soldered onto it exploded in service. When the vessel was inspected afterwards, it was found to have developed a crack in the top end plate. A portion of the end plate cut out to include the midlength and one termination of the crack was examined microscopically. This revealed that the crack was associated with intergranular penetration by molten metal. The microstructure in general was indicative of a good-quality mild steel. It was evident from that solder that was responsible for the penetration and that fused brass from the hand wheel had not played any part. Tensile stress was present at the time of the failure sufficiently high to enable solder penetration to take place. The use of soft solder as a medium for attaching name-plates directly on to stressed steel parts is not recommended. It would be preferable to use a welded-on patch plate or to employ one of the high-strength, non-metallic adhesives.

A 2.3 mm diam steel wire broke during cable twisting. The fracture occurred obliquely to the longitudinal axis of the wire and showed a constriction at the end. Therefore it was a ductile fracture. File mark type work defects were noticeable on the wire surface at both sides of the fracture, but they had no effect on the breakage of the wire. Away from the fracture area, the wire had a normal structure of hyperfine lamellar pearlite (sorbite) of a “patented” and cold drawn steel wire. In the vicinity of the fracture, the cementite of the pearlite was partially spheroidized, while at the fracture itself it was completely spheroidized. Therefore the wire was locally annealed at this point. It was likely that the wire cracked at this point during the last drawing and then broke during twisting due to its lower strength in the weakened cross section after prior deformation.